JPS5735526A - Preparation of organopolysiloxane - Google Patents
Preparation of organopolysiloxaneInfo
- Publication number
- JPS5735526A JPS5735526A JP11148580A JP11148580A JPS5735526A JP S5735526 A JPS5735526 A JP S5735526A JP 11148580 A JP11148580 A JP 11148580A JP 11148580 A JP11148580 A JP 11148580A JP S5735526 A JPS5735526 A JP S5735526A
- Authority
- JP
- Japan
- Prior art keywords
- trimethylsilanol
- reaction
- hydrochloric acid
- compound shown
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Silicon Polymers (AREA)
Abstract
PURPOSE: To obtain the titled substance with its terminal groups blocked with trimethylsilyl groups in high purity, in high yield, and at low cost, by subjecting a trimethylsilanol- or OH-containing organopolysiloxane and a Cl-containing organic silicon compound to a reaction through removal of hydrochloric acid.
CONSTITUTION: A compound shown by the formula I (R is hydrocarbon group; l is positive integer ≤4) synthesized from trimethylsilanol or trimethylsilanol and organodichlorosilane as starting mterials and a compound shown by the formula II (where c is 1, a=b=3, m=1W4; when c is 2, a=b=1, m=0) are subjected to a reaction through removal of hydrochloric acid, to give a compound shown by the formula III (n is positive integer of 1W9). The reaction is carried out at -50W 120°C, a trapping agent (e.g., triethylamine) for hydrochloric acid, organic solvent, etc. may be used.
USE: Lubricant, antifoaming agent, parting agent, additive for coating compound, and polish.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11148580A JPS5735526A (en) | 1980-08-13 | 1980-08-13 | Preparation of organopolysiloxane |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11148580A JPS5735526A (en) | 1980-08-13 | 1980-08-13 | Preparation of organopolysiloxane |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5735526A true JPS5735526A (en) | 1982-02-26 |
JPS6228956B2 JPS6228956B2 (en) | 1987-06-23 |
Family
ID=14562452
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP11148580A Granted JPS5735526A (en) | 1980-08-13 | 1980-08-13 | Preparation of organopolysiloxane |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5735526A (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5002762A (en) * | 1988-03-16 | 1991-03-26 | The Procter & Gamble Company | Volatile silicons in household and cosmetic products |
US5084577A (en) * | 1988-03-16 | 1992-01-28 | The Procter & Gamble Company | Volatile silicon compounds |
EP0639576A1 (en) * | 1993-08-18 | 1995-02-22 | Shin-Etsu Chemical Co., Ltd. | Organopolysiloxanes having a silanol group and process of making them |
JP2013520429A (en) * | 2010-02-19 | 2013-06-06 | ボード・オブ・リージエンツ,ザ・ユニバーシテイ・オブ・テキサス・システム | Branched siloxanes and methods for synthesis |
JP2018533562A (en) * | 2015-11-04 | 2018-11-15 | ダウ シリコーンズ コーポレーション | Method of preparing organosiloxane |
JP2020519700A (en) * | 2017-06-06 | 2020-07-02 | ダウ シリコーンズ コーポレーション | Method for producing halosiloxane |
-
1980
- 1980-08-13 JP JP11148580A patent/JPS5735526A/en active Granted
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5002762A (en) * | 1988-03-16 | 1991-03-26 | The Procter & Gamble Company | Volatile silicons in household and cosmetic products |
US5084577A (en) * | 1988-03-16 | 1992-01-28 | The Procter & Gamble Company | Volatile silicon compounds |
EP0639576A1 (en) * | 1993-08-18 | 1995-02-22 | Shin-Etsu Chemical Co., Ltd. | Organopolysiloxanes having a silanol group and process of making them |
JP2013520429A (en) * | 2010-02-19 | 2013-06-06 | ボード・オブ・リージエンツ,ザ・ユニバーシテイ・オブ・テキサス・システム | Branched siloxanes and methods for synthesis |
JP2018533562A (en) * | 2015-11-04 | 2018-11-15 | ダウ シリコーンズ コーポレーション | Method of preparing organosiloxane |
JP2020519700A (en) * | 2017-06-06 | 2020-07-02 | ダウ シリコーンズ コーポレーション | Method for producing halosiloxane |
US11098068B2 (en) | 2017-06-06 | 2021-08-24 | Dow Silicones Corporation | Method of making a halosiloxane |
Also Published As
Publication number | Publication date |
---|---|
JPS6228956B2 (en) | 1987-06-23 |
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