JPS5716893A - Production of organoiminoxysilane - Google Patents
Production of organoiminoxysilaneInfo
- Publication number
- JPS5716893A JPS5716893A JP9126980A JP9126980A JPS5716893A JP S5716893 A JPS5716893 A JP S5716893A JP 9126980 A JP9126980 A JP 9126980A JP 9126980 A JP9126980 A JP 9126980A JP S5716893 A JPS5716893 A JP S5716893A
- Authority
- JP
- Japan
- Prior art keywords
- product
- organic base
- water
- halogenosilane
- oxime
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
PURPOSE: The reaction of halogenosilane with oxime is conducted in the presence of an organic base containing a tertiary nitrogen to prevent the contamination with water and alcohol in the process of the neutralization and the recovery of by-products, thus producing the titled compound of high quality in high yield.
CONSTITUTION: The reaction between a halogenosilane of Rm 1SiX4-m (R1 is lower alkyl; X is halogen; m is 1W3) and an oxime of formula I (R2, R3 are lower alkyl) is conducted in a hydrocarbon solvent such as benzene or toluene in the presence of an organic base containing a tertiary nitrogen such as pyridine and the by-product, the hydrohalide salt of the organic base, is filtered off. The solvent is distilled off from the filtrate to give the titled compound of formula II. The by-product is neutralized with ammonia gas and the base is recovered for reuse. Since no water is formed in the process, the decomposition of the starting materials and product is prevented and the operation for eliminating water can be omitted.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9126980A JPS5716893A (en) | 1980-07-03 | 1980-07-03 | Production of organoiminoxysilane |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9126980A JPS5716893A (en) | 1980-07-03 | 1980-07-03 | Production of organoiminoxysilane |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5716893A true JPS5716893A (en) | 1982-01-28 |
JPH0222079B2 JPH0222079B2 (en) | 1990-05-17 |
Family
ID=14021715
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP9126980A Granted JPS5716893A (en) | 1980-07-03 | 1980-07-03 | Production of organoiminoxysilane |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5716893A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4705877A (en) * | 1987-02-25 | 1987-11-10 | Dow Corning Corporation | Novel aminohydrocarbyl-substituted ketoximosilanes |
US4705878A (en) * | 1987-02-25 | 1987-11-10 | Dow Corning Corporation | Method for preparing aminohydrocarbyl-substituted ketoximosilanes |
JPH06106657A (en) * | 1992-09-04 | 1994-04-19 | Futagami Tekkosho:Kk | Taper box making machine |
-
1980
- 1980-07-03 JP JP9126980A patent/JPS5716893A/en active Granted
Non-Patent Citations (1)
Title |
---|
1ND1AN JOURNAL OF CHEM1STRY * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4705877A (en) * | 1987-02-25 | 1987-11-10 | Dow Corning Corporation | Novel aminohydrocarbyl-substituted ketoximosilanes |
US4705878A (en) * | 1987-02-25 | 1987-11-10 | Dow Corning Corporation | Method for preparing aminohydrocarbyl-substituted ketoximosilanes |
JPH06106657A (en) * | 1992-09-04 | 1994-04-19 | Futagami Tekkosho:Kk | Taper box making machine |
Also Published As
Publication number | Publication date |
---|---|
JPH0222079B2 (en) | 1990-05-17 |
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