JPS567731A - Separation of methyl acetate, methanol, and water - Google Patents
Separation of methyl acetate, methanol, and waterInfo
- Publication number
- JPS567731A JPS567731A JP8211179A JP8211179A JPS567731A JP S567731 A JPS567731 A JP S567731A JP 8211179 A JP8211179 A JP 8211179A JP 8211179 A JP8211179 A JP 8211179A JP S567731 A JPS567731 A JP S567731A
- Authority
- JP
- Japan
- Prior art keywords
- methanol
- water
- column
- methyl acetate
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
PURPOSE: To minimize the energy required for the separation of the titled compounds, by subjecting a mixture of methyl acetate and methanol to the extraction distillation and the azeotropic distillation, and feeding the bottom liquid of the azeotropic distillation column to the top of the distillation column of methanol- water mixture.
CONSTITUTION: A mixture of methyl acetate and methanol containing smaller amount of water is fed to an azeotropic distillation column 9, and the one containing higher amount of water to an extraction distillation column 3, and distilled under reflux. A mixture of 80.5% of methyl acetate and 19.5% of methanol is distilled off from the top of the column 9, and a highly concentrated methyl acetate is obtained from the top of the column 3. A mixture of methanol and water is extracted from the bottom of the column 3 and sent to a water-methanol separator column 14. The bottom liquid (highly concentrated methanol) of the azeotropic distillation column 9 is fed to the top or between the top and the 15th stage (the higher the better) of the separator column 14, and distilled under reflux to separate methanol from water.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8211179A JPS567731A (en) | 1979-06-29 | 1979-06-29 | Separation of methyl acetate, methanol, and water |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8211179A JPS567731A (en) | 1979-06-29 | 1979-06-29 | Separation of methyl acetate, methanol, and water |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS567731A true JPS567731A (en) | 1981-01-27 |
| JPS615455B2 JPS615455B2 (en) | 1986-02-18 |
Family
ID=13765284
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP8211179A Granted JPS567731A (en) | 1979-06-29 | 1979-06-29 | Separation of methyl acetate, methanol, and water |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS567731A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0798284A2 (en) * | 1996-03-29 | 1997-10-01 | Kuraray Co., Ltd. | Method for treating a solution of organic compound |
| JP2010132667A (en) * | 2002-01-11 | 2010-06-17 | Celanese Internatl Corp | Integrated process for producing acetic acid and acetic anhydride or simultaneously producing them by carbonylation using methyl acetate by-product stream |
| CN105152855A (en) * | 2015-09-28 | 2015-12-16 | 中建安装工程有限公司 | Method and device for performing azeotropic distillation separation on methyl acetate and methyl alcohol mixture |
-
1979
- 1979-06-29 JP JP8211179A patent/JPS567731A/en active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0798284A2 (en) * | 1996-03-29 | 1997-10-01 | Kuraray Co., Ltd. | Method for treating a solution of organic compound |
| EP0798284A3 (en) * | 1996-03-29 | 1998-07-29 | Kuraray Co., Ltd. | Method for treating a solution of organic compound |
| CN1089260C (en) * | 1996-03-29 | 2002-08-21 | 可乐丽股份有限公司 | Method for treating solution of organic compound |
| JP2010132667A (en) * | 2002-01-11 | 2010-06-17 | Celanese Internatl Corp | Integrated process for producing acetic acid and acetic anhydride or simultaneously producing them by carbonylation using methyl acetate by-product stream |
| CN105152855A (en) * | 2015-09-28 | 2015-12-16 | 中建安装工程有限公司 | Method and device for performing azeotropic distillation separation on methyl acetate and methyl alcohol mixture |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS615455B2 (en) | 1986-02-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPS53116314A (en) | Separation of acetic acid and water | |
| KR960029310A (en) | (Meth) acrylic acid is isolated by rectifying a mixture containing (meth) acrylic acid as a main component and a lower aldehyde as a secondary component in a rectification column composed of a stripping region and a rectification region | |
| JPS5433279A (en) | Separating method for liquid mixture | |
| JPS5692228A (en) | Preparation of high-purity alkylene glycol | |
| JPS579740A (en) | Purification of methyl methacrylate | |
| JPS567731A (en) | Separation of methyl acetate, methanol, and water | |
| JPS55104244A (en) | Separation and incineration of crude olefinic unsaturated acetonitrile | |
| ES8303282A1 (en) | Esterification process of acetic acid by C2 to C5 alcohols. | |
| JPS5413474A (en) | Separator of tubular membrane type | |
| JPS56166131A (en) | Preparation of mixture of m-phenoxybenzyl alcohol with m-phenoxybenzaldehyde | |
| JPS56123926A (en) | Purification of methanol | |
| SU652169A1 (en) | Method of separating methyl-tert-butyl ester | |
| JPS55115833A (en) | Separation of ester and ketone | |
| JPS5585532A (en) | Separation of cresol | |
| JPS55143949A (en) | Recovery of purified acetonitrile | |
| DE2962595D1 (en) | Process for producing tetrahydrofuran and 1,4-butanediol | |
| JPS53114569A (en) | Apparatus for separating and dehydrating scale | |
| GB1199120A (en) | Process for Separating Methanol from a Mixture Thereof With Methyl Acetate | |
| JPS5387305A (en) | Preparation of 1,4-butanediol and tetrahydrofuran | |
| JPS53111001A (en) | Separation of mixture of hydrocarbons | |
| JPS53108909A (en) | Purification of ethylene glycol | |
| JPS53130654A (en) | Separation and purification of tetrahydrofuran | |
| JPS5293762A (en) | Preparation of cyclic ethers | |
| JPS5371006A (en) | Purification of hexafluoro-2-propanone | |
| JPS53119807A (en) | Separation of butanediol |