JPS5673031A - Preparation of tetrafluoromethane - Google Patents
Preparation of tetrafluoromethaneInfo
- Publication number
- JPS5673031A JPS5673031A JP15032779A JP15032779A JPS5673031A JP S5673031 A JPS5673031 A JP S5673031A JP 15032779 A JP15032779 A JP 15032779A JP 15032779 A JP15032779 A JP 15032779A JP S5673031 A JPS5673031 A JP S5673031A
- Authority
- JP
- Japan
- Prior art keywords
- temperature
- reaction
- tetrafluoromethane
- monochlorotrifluoromethane
- tetrachloromethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare tetrafluoromethane in high conversion, with long catalytic life, by reacting tetrachloromethane with HF at a relatively low temperature to produce monochlorotrifluoromethane, and then raising the temperature to continue the reaction.
CONSTITUTION: Tetrafluoromethane is prepared by reacting (A) a mixture of a partly chlorinated and fluorinated methane derivative and chlorine gas, (B) tetrachloromethane, and/or (C) chlorofluoromethane containing two or more chlorine atoms, with HF using a solid catalyst (e.g. activated chromium oxide). The reaction with HF is carried out first at a temperature sufficiently low to produce mainly monochlorotrifluoromethane (≤380°C, pref. ≤350°C), and then after the purification of the reaction product gas, at a temperature higher than the first stage reaction temperature (i.e. ≥350°C, pref. ≥380°C).
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15032779A JPS5673031A (en) | 1979-11-20 | 1979-11-20 | Preparation of tetrafluoromethane |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15032779A JPS5673031A (en) | 1979-11-20 | 1979-11-20 | Preparation of tetrafluoromethane |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5673031A true JPS5673031A (en) | 1981-06-17 |
JPS6210484B2 JPS6210484B2 (en) | 1987-03-06 |
Family
ID=15494587
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP15032779A Granted JPS5673031A (en) | 1979-11-20 | 1979-11-20 | Preparation of tetrafluoromethane |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5673031A (en) |
-
1979
- 1979-11-20 JP JP15032779A patent/JPS5673031A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS6210484B2 (en) | 1987-03-06 |
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