JPS5671089A - 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate - Google Patents
1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonateInfo
- Publication number
- JPS5671089A JPS5671089A JP14704979A JP14704979A JPS5671089A JP S5671089 A JPS5671089 A JP S5671089A JP 14704979 A JP14704979 A JP 14704979A JP 14704979 A JP14704979 A JP 14704979A JP S5671089 A JPS5671089 A JP S5671089A
- Authority
- JP
- Japan
- Prior art keywords
- methyl
- compound
- cyclohexyl
- phenyl
- piperidinium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
NEW MATERIAL:1-Methyl-1-[ ( 2-cyclohexyl-r-2-phenyl-1, 3-dioxoran-t-4-yl )meth- yl ]-piperidinium p-toluenesulfonate.
USE: Synthetic intermediate of autonomic nerve blocker: they are very useful for synthesizing the trans isomer of the compound of formula II.
PREPARATION: The reaction of a compound of formula III with N-methylpiperidine affords the compound of formula I. The reaction is carried out in the absence or presence of a solvent such as methanol at room temperature to 250°C. The compound of formula III is obtained through, e.g., following steps the reaction of cyclohexyl phenyl ketone with glycerol or glycidol, the tosylation of the product and the fractionation recrystallization.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14704979A JPS5671089A (en) | 1979-11-15 | 1979-11-15 | 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14704979A JPS5671089A (en) | 1979-11-15 | 1979-11-15 | 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5671089A true JPS5671089A (en) | 1981-06-13 |
JPS6241514B2 JPS6241514B2 (en) | 1987-09-03 |
Family
ID=15421337
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP14704979A Granted JPS5671089A (en) | 1979-11-15 | 1979-11-15 | 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5671089A (en) |
-
1979
- 1979-11-15 JP JP14704979A patent/JPS5671089A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS6241514B2 (en) | 1987-09-03 |
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