JPS5671089A - 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate - Google Patents

1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate

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Publication number
JPS5671089A
JPS5671089A JP14704979A JP14704979A JPS5671089A JP S5671089 A JPS5671089 A JP S5671089A JP 14704979 A JP14704979 A JP 14704979A JP 14704979 A JP14704979 A JP 14704979A JP S5671089 A JPS5671089 A JP S5671089A
Authority
JP
Japan
Prior art keywords
methyl
compound
cyclohexyl
phenyl
piperidinium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP14704979A
Other languages
Japanese (ja)
Other versions
JPS6241514B2 (en
Inventor
Kazuo Kikazawa
Mineji Hiiragi
Haruhide Ishimaru
Toshihisa Nakamura
Keiko Shiroyama
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Aska Pharmaceutical Co Ltd
Original Assignee
Grelan Pharmaceutical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Grelan Pharmaceutical Co Ltd filed Critical Grelan Pharmaceutical Co Ltd
Priority to JP14704979A priority Critical patent/JPS5671089A/en
Publication of JPS5671089A publication Critical patent/JPS5671089A/en
Publication of JPS6241514B2 publication Critical patent/JPS6241514B2/ja
Granted legal-status Critical Current

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Abstract

NEW MATERIAL:1-Methyl-1-[ ( 2-cyclohexyl-r-2-phenyl-1, 3-dioxoran-t-4-yl )meth- yl ]-piperidinium p-toluenesulfonate.
USE: Synthetic intermediate of autonomic nerve blocker: they are very useful for synthesizing the trans isomer of the compound of formula II.
PREPARATION: The reaction of a compound of formula III with N-methylpiperidine affords the compound of formula I. The reaction is carried out in the absence or presence of a solvent such as methanol at room temperature to 250°C. The compound of formula III is obtained through, e.g., following steps the reaction of cyclohexyl phenyl ketone with glycerol or glycidol, the tosylation of the product and the fractionation recrystallization.
COPYRIGHT: (C)1981,JPO&Japio
JP14704979A 1979-11-15 1979-11-15 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate Granted JPS5671089A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP14704979A JPS5671089A (en) 1979-11-15 1979-11-15 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP14704979A JPS5671089A (en) 1979-11-15 1979-11-15 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate

Publications (2)

Publication Number Publication Date
JPS5671089A true JPS5671089A (en) 1981-06-13
JPS6241514B2 JPS6241514B2 (en) 1987-09-03

Family

ID=15421337

Family Applications (1)

Application Number Title Priority Date Filing Date
JP14704979A Granted JPS5671089A (en) 1979-11-15 1979-11-15 1-methyl-1-((2-cyclohexyl-r-2-phenyl-1,3-dioxorane-t-4-yl)- methyl)piperidinium p-toluenesulfonate

Country Status (1)

Country Link
JP (1) JPS5671089A (en)

Also Published As

Publication number Publication date
JPS6241514B2 (en) 1987-09-03

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