JPS5669230A - Preparation of hydrous iron oxide - Google Patents
Preparation of hydrous iron oxideInfo
- Publication number
- JPS5669230A JPS5669230A JP14606879A JP14606879A JPS5669230A JP S5669230 A JPS5669230 A JP S5669230A JP 14606879 A JP14606879 A JP 14606879A JP 14606879 A JP14606879 A JP 14606879A JP S5669230 A JPS5669230 A JP S5669230A
- Authority
- JP
- Japan
- Prior art keywords
- oxidizing agent
- suspension
- liquid
- reaction
- liquid oxidizing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 title abstract 4
- 239000007800 oxidant agent Substances 0.000 abstract 8
- 239000007788 liquid Substances 0.000 abstract 5
- 239000000725 suspension Substances 0.000 abstract 4
- 238000006243 chemical reaction Methods 0.000 abstract 3
- 229910052598 goethite Inorganic materials 0.000 abstract 2
- AEIXRCIKZIZYPM-UHFFFAOYSA-M hydroxy(oxo)iron Chemical compound [O][Fe]O AEIXRCIKZIZYPM-UHFFFAOYSA-M 0.000 abstract 2
- 229910021506 iron(II) hydroxide Inorganic materials 0.000 abstract 2
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 238000013019 agitation Methods 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
- C01G49/06—Ferric oxide [Fe2O3]
-
- G—PHYSICS
- G11—INFORMATION STORAGE
- G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
- G11B5/00—Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
- G11B5/62—Record carriers characterised by the selection of the material
- G11B5/68—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent
- G11B5/70—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer
- G11B5/706—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer characterised by the composition of the magnetic material
- G11B5/70626—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer characterised by the composition of the magnetic material containing non-metallic substances
- G11B5/70642—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer characterised by the composition of the magnetic material containing non-metallic substances iron oxides
- G11B5/70652—Record carriers characterised by the selection of the material comprising one or more layers of magnetisable material homogeneously mixed with a bonding agent on a base layer characterised by the composition of the magnetic material containing non-metallic substances iron oxides gamma - Fe2 O3
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/42—Magnetic properties
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Iron (AREA)
- Hard Magnetic Materials (AREA)
Abstract
PURPOSE: To synthesize hydrous iron oxide consisting of high-quality goethite essentially at a low cost, by oxidizing a suspension consisting of iron (II) hydroxide with a gaseous oxidizing agent and a liquid oxidizing agent together.
CONSTITUTION: A suspension consisting of iron (II) hydroxide is oxidized with a gaseous oxidizing agent, e.g. air, and a liquid oxidizing agent, e.g. NaClO3, together, and the liquid oxidizing agent is preferably used in the initial stage of the reaction and then changed over to the gaseous oxidizing agent to carry out the oxidation. In the process, the suspension is reacted at 30W60°C with agitation. After the suspension turns yellow completely and the reaction is completed, a formed precipitate is washed with water, filtered and dried to give goethite powder in the form of fine needlelike crystal. According to the method, the amount of the liquid oxidizing agent of comparatively high price is reduced to half or less that in the case of the liquid oxidizing agent used throughout the reaction period, and the raw material cost can be saved.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14606879A JPS5669230A (en) | 1979-11-13 | 1979-11-13 | Preparation of hydrous iron oxide |
DE19803042880 DE3042880A1 (en) | 1979-11-13 | 1980-11-13 | METHOD FOR PRODUCING HYDRATED IRON OXIDE |
GB8036437A GB2063233A (en) | 1979-11-13 | 1980-11-13 | Hydrated Iron Oxide Production |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14606879A JPS5669230A (en) | 1979-11-13 | 1979-11-13 | Preparation of hydrous iron oxide |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5669230A true JPS5669230A (en) | 1981-06-10 |
Family
ID=15399350
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP14606879A Pending JPS5669230A (en) | 1979-11-13 | 1979-11-13 | Preparation of hydrous iron oxide |
Country Status (3)
Country | Link |
---|---|
JP (1) | JPS5669230A (en) |
DE (1) | DE3042880A1 (en) |
GB (1) | GB2063233A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102015215736A1 (en) | 2015-08-18 | 2017-02-23 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Process for the preparation of stably dispersible magnetic iron oxide monoparticle nanoparticles, stably dispersible magnetic iron oxide monoparticle nanoparticles and uses thereof |
-
1979
- 1979-11-13 JP JP14606879A patent/JPS5669230A/en active Pending
-
1980
- 1980-11-13 GB GB8036437A patent/GB2063233A/en not_active Withdrawn
- 1980-11-13 DE DE19803042880 patent/DE3042880A1/en not_active Withdrawn
Also Published As
Publication number | Publication date |
---|---|
GB2063233A (en) | 1981-06-03 |
DE3042880A1 (en) | 1981-05-21 |
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