JPS56123963A - Preparation of 2,6-dioxyiminocyclohexanone - Google Patents

Preparation of 2,6-dioxyiminocyclohexanone

Info

Publication number
JPS56123963A
JPS56123963A JP11442780A JP11442780A JPS56123963A JP S56123963 A JPS56123963 A JP S56123963A JP 11442780 A JP11442780 A JP 11442780A JP 11442780 A JP11442780 A JP 11442780A JP S56123963 A JPS56123963 A JP S56123963A
Authority
JP
Japan
Prior art keywords
cyclohexanone
acidic catalyst
dinitrogen trioxide
cyclohexanol
titled compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP11442780A
Other languages
Japanese (ja)
Other versions
JPS5725541B2 (en
Inventor
Yasuo Hazama
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
Original Assignee
Sumitomo Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Co Ltd filed Critical Sumitomo Chemical Co Ltd
Priority to JP11442780A priority Critical patent/JPS56123963A/en
Publication of JPS56123963A publication Critical patent/JPS56123963A/en
Publication of JPS5725541B2 publication Critical patent/JPS5725541B2/ja
Granted legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To obtain the titled compound useful as a synthetic intermediate for lysine, etc. in high yield and industrially and advantageously, by reacting cyclohexanone with a readily available dinitrogen trioxide or nitrose gas in cyclohexanol in the presence of an acidic catalyst.
CONSTITUTION: Cyclohexanone is reacted with dinitrogen trioxide or nitrose gas in cyclohexanol in the presence of an acidic catalyst, e.g. a mineral acid, at 0W40°C to give the titled compound. The concentration of the acidic catalyst based on the cyclohexanone is preferably 0.1W100mol%, and the amount of the dinitrogen trioxide or nitrose gas is suitably 1W2 times the theoretical one of the cyclohexanone. In the range described above, the conversion of the cyclohexanone reaches about 100% without the necessity for taking the recovery thereof into consideration.
COPYRIGHT: (C)1981,JPO&Japio
JP11442780A 1980-08-19 1980-08-19 Preparation of 2,6-dioxyiminocyclohexanone Granted JPS56123963A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11442780A JPS56123963A (en) 1980-08-19 1980-08-19 Preparation of 2,6-dioxyiminocyclohexanone

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11442780A JPS56123963A (en) 1980-08-19 1980-08-19 Preparation of 2,6-dioxyiminocyclohexanone

Publications (2)

Publication Number Publication Date
JPS56123963A true JPS56123963A (en) 1981-09-29
JPS5725541B2 JPS5725541B2 (en) 1982-05-29

Family

ID=14637438

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11442780A Granted JPS56123963A (en) 1980-08-19 1980-08-19 Preparation of 2,6-dioxyiminocyclohexanone

Country Status (1)

Country Link
JP (1) JPS56123963A (en)

Also Published As

Publication number Publication date
JPS5725541B2 (en) 1982-05-29

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