JPS56103134A - Preparation of high-purity carboxylic acid chloride - Google Patents

Preparation of high-purity carboxylic acid chloride

Info

Publication number
JPS56103134A
JPS56103134A JP586280A JP586280A JPS56103134A JP S56103134 A JPS56103134 A JP S56103134A JP 586280 A JP586280 A JP 586280A JP 586280 A JP586280 A JP 586280A JP S56103134 A JPS56103134 A JP S56103134A
Authority
JP
Japan
Prior art keywords
carboxylic acid
acid chloride
phosgene
preparation
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP586280A
Other languages
Japanese (ja)
Other versions
JPS6313976B2 (en
Inventor
Teruyuki Nagata
Akihiro Tamaoki
Masaru Wada
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Priority to JP586280A priority Critical patent/JPS56103134A/en
Publication of JPS56103134A publication Critical patent/JPS56103134A/en
Publication of JPS6313976B2 publication Critical patent/JPS6313976B2/ja
Granted legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To obtain a high-purity carboxylic acid chloride readily without discoloration and change with time, by adding a metal, e.g. Zn, to the reaction product of an organic carboxylic acid with phosgene in the presence of a lower aliphatic amide as a catalyst, and heat-treating the reaction mixture.
CONSTITUTION: An organic carboxylic acid, e.g. acetic or propionic acid, is reacted with phosgene, in the presence (absence) of a solvent, e.g. benzene, and a lower aliphatic acid amide, e.g. dimethylformamide as a catalyst, at 30W100°C, especially 50W90°C. To the resultant solution, or concentrated solution or crude product prepared by the elimination of all of part or the solvent used, are added one or two or more metals selected from Zn, Ti, V, Cr, Mn, Fe, Co and Ni, or a compound thereof, and the mixture is then heat-treated at 70W200°C, preferably 120W180°C, in an inert gas atmosphere and distilled to give the aimed compound of high quality.
COPYRIGHT: (C)1981,JPO&Japio
JP586280A 1980-01-23 1980-01-23 Preparation of high-purity carboxylic acid chloride Granted JPS56103134A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP586280A JPS56103134A (en) 1980-01-23 1980-01-23 Preparation of high-purity carboxylic acid chloride

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP586280A JPS56103134A (en) 1980-01-23 1980-01-23 Preparation of high-purity carboxylic acid chloride

Publications (2)

Publication Number Publication Date
JPS56103134A true JPS56103134A (en) 1981-08-18
JPS6313976B2 JPS6313976B2 (en) 1988-03-29

Family

ID=11622765

Family Applications (1)

Application Number Title Priority Date Filing Date
JP586280A Granted JPS56103134A (en) 1980-01-23 1980-01-23 Preparation of high-purity carboxylic acid chloride

Country Status (1)

Country Link
JP (1) JPS56103134A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6429334B1 (en) 2000-06-07 2002-08-06 E. I. Du Pont De Nemours And Company Production of acid anhydrides and acid chlorides
US6730210B2 (en) 2000-03-28 2004-05-04 E. I. Du Pont De Nemours And Company Low temperature alkali metal electrolysis
CN114478300A (en) * 2021-07-16 2022-05-13 丰益表面活性材料（连云港）有限公司 Novel acyl chloride catalyst and preparation method and application thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6730210B2 (en) 2000-03-28 2004-05-04 E. I. Du Pont De Nemours And Company Low temperature alkali metal electrolysis
US6429334B1 (en) 2000-06-07 2002-08-06 E. I. Du Pont De Nemours And Company Production of acid anhydrides and acid chlorides
CN114478300A (en) * 2021-07-16 2022-05-13 丰益表面活性材料（连云港）有限公司 Novel acyl chloride catalyst and preparation method and application thereof

Also Published As

Publication number Publication date
JPS6313976B2 (en) 1988-03-29

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