JPS5463039A - Preparation of pyromellitic acid and/or pyromellitic anhydride - Google Patents
Preparation of pyromellitic acid and/or pyromellitic anhydrideInfo
- Publication number
- JPS5463039A JPS5463039A JP12958977A JP12958977A JPS5463039A JP S5463039 A JPS5463039 A JP S5463039A JP 12958977 A JP12958977 A JP 12958977A JP 12958977 A JP12958977 A JP 12958977A JP S5463039 A JPS5463039 A JP S5463039A
- Authority
- JP
- Japan
- Prior art keywords
- pyromellitic
- acid
- anhydride
- mixture
- carboxylic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Furan Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare the high purity title compound selectively and in high yield by dissolving an aromatic poly-valent carboxylic acid mixture containing pyromellitic acid in a specific medium, and adding benzene and/or an alkylbenzene to the solution, thereby precipitating the title compound.
CONSTITUTION: A mixture of aromatic poly-valent carboxylic acid and/or its anhydride containing pyromellitic acid and/or pyromellitic anhydride dissolved in a≥3C aliphatic carboxylic acid (e.g. acetic acid) and/or its anhydride. Then, benzene and/or alkylbenzene is added to this mixture to precipitate the objective compound selectively. Pyromellitic acid or pyromellitic anhydride can also be obtained from a mixture of aromatic poly-valent carboxylic acid containing a comparatively small amount of the compound, such as the distillation residue of anhydrous phtaoic acid obtained by the air oxidation of e.g. o-xylene.
USE: Starting material of heat-resistant resins, etc.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12958977A JPS5463039A (en) | 1977-10-31 | 1977-10-31 | Preparation of pyromellitic acid and/or pyromellitic anhydride |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12958977A JPS5463039A (en) | 1977-10-31 | 1977-10-31 | Preparation of pyromellitic acid and/or pyromellitic anhydride |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5463039A true JPS5463039A (en) | 1979-05-21 |
JPS6115864B2 JPS6115864B2 (en) | 1986-04-26 |
Family
ID=15013171
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP12958977A Granted JPS5463039A (en) | 1977-10-31 | 1977-10-31 | Preparation of pyromellitic acid and/or pyromellitic anhydride |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5463039A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004111026A1 (en) * | 2003-06-17 | 2004-12-23 | Nippon Shokubai Co., Ltd. | Bis (fluorine-containing phthalic anhydride) and method for production thereof |
JP2005029572A (en) * | 2003-06-17 | 2005-02-03 | Nippon Shokubai Co Ltd | Bis(fluorine-containing phthalic anhydride) and method for production thereof |
JP2010168395A (en) * | 2003-06-17 | 2010-08-05 | Nippon Shokubai Co Ltd | Intermediate raw material |
-
1977
- 1977-10-31 JP JP12958977A patent/JPS5463039A/en active Granted
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004111026A1 (en) * | 2003-06-17 | 2004-12-23 | Nippon Shokubai Co., Ltd. | Bis (fluorine-containing phthalic anhydride) and method for production thereof |
JP2005029572A (en) * | 2003-06-17 | 2005-02-03 | Nippon Shokubai Co Ltd | Bis(fluorine-containing phthalic anhydride) and method for production thereof |
US7700647B2 (en) | 2003-06-17 | 2010-04-20 | Nippon Shokubai Co., Ltd. | Fluorinated bis (phthalic anhydride) and method for producing the same |
JP2010168395A (en) * | 2003-06-17 | 2010-08-05 | Nippon Shokubai Co Ltd | Intermediate raw material |
Also Published As
Publication number | Publication date |
---|---|
JPS6115864B2 (en) | 1986-04-26 |
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