JPS5495546A - Production cis-4-tert-butylcyclohexanol - Google Patents
Production cis-4-tert-butylcyclohexanolInfo
- Publication number
- JPS5495546A JPS5495546A JP141178A JP141178A JPS5495546A JP S5495546 A JPS5495546 A JP S5495546A JP 141178 A JP141178 A JP 141178A JP 141178 A JP141178 A JP 141178A JP S5495546 A JPS5495546 A JP S5495546A
- Authority
- JP
- Japan
- Prior art keywords
- ruthenium
- tert
- alumina
- hydroxide
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Abstract
PURPOSE: The catalytic hydrogenation of 4-tert-butylphenol under pressure is conducted using a ruthenium catalyst prepared by the adsorption of a ruthenium salt on alumina in a strong alkali aqueous solution to produce economically high-quality title compound used for perfumery of cosmetics.
CONSTITUTION: Alumina is suspended in an alkali metal hydroxide as sodium hydroxide aqueous solution and a ruthenium salt, preferably ruthenium cloride, solution is added to above suspension to deposit the ruthenium salt on the alumina as ruthenium hydroxide. Then the ruthenium hydroxide is reduced with sodium borohydride and treated with hydrochloric acid to prepare ruthenium catalyst on alumina. The catalytic hydrogenation of 4-tert-burylphenol is effected using the resulting catalyst at 55W150°C to produce cis-4-tert-butyl-cyclohexanol.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP53001411A JPS6034526B2 (en) | 1978-01-10 | 1978-01-10 | Method for producing cis-4-tert-butylcyclohexanol |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP53001411A JPS6034526B2 (en) | 1978-01-10 | 1978-01-10 | Method for producing cis-4-tert-butylcyclohexanol |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5495546A true JPS5495546A (en) | 1979-07-28 |
JPS6034526B2 JPS6034526B2 (en) | 1985-08-09 |
Family
ID=11500735
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP53001411A Expired JPS6034526B2 (en) | 1978-01-10 | 1978-01-10 | Method for producing cis-4-tert-butylcyclohexanol |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6034526B2 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH03173842A (en) * | 1989-11-13 | 1991-07-29 | Firmenich Sa | Preparation of 4-t-butyl-cyclohexanol and catalyst for its preparation |
-
1978
- 1978-01-10 JP JP53001411A patent/JPS6034526B2/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH03173842A (en) * | 1989-11-13 | 1991-07-29 | Firmenich Sa | Preparation of 4-t-butyl-cyclohexanol and catalyst for its preparation |
JPH0764769B2 (en) * | 1989-11-13 | 1995-07-12 | フイルメニツヒ・ソシエテ・アノニム | Process for producing 4-t-butyl-cyclohexanol and catalyst for production |
Also Published As
Publication number | Publication date |
---|---|
JPS6034526B2 (en) | 1985-08-09 |
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