JPS5479243A - Method of continuous esterification - Google Patents
Method of continuous esterificationInfo
- Publication number
- JPS5479243A JPS5479243A JP14507977A JP14507977A JPS5479243A JP S5479243 A JPS5479243 A JP S5479243A JP 14507977 A JP14507977 A JP 14507977A JP 14507977 A JP14507977 A JP 14507977A JP S5479243 A JPS5479243 A JP S5479243A
- Authority
- JP
- Japan
- Prior art keywords
- esterification
- terephthalic acid
- dicarboxylic acids
- type reactor
- mainly consisting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: The continuous esterification reaction between dicarboxylic acids mainly containing terephthalic acid and glycols is effected through a specific two-stage process, thereby producing esterification products with less DEG content in high productivity even in large scale production.
CONSTITUTION: The continuous esterification reaction between dicarboxylic acids mainly consisting of terephthalic acid and gylcols mainly consisting of ethylene glycol is carried out to produce the glycol esters of carboxylic acids and/or their oligomers, wherein first the slurry is esterified in completely mixing type reactor 4 to an extent of 80W92% esterification degree, then the esterification is continued using horizontal multistage cascade type reacror 9. The horizontal multistage cascade type reactor is provided with stirring shafts in the longitudinal direction to lift the reaction mixture to renew surfaces always, thereby expanding the evaporation area.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14507977A JPS5479243A (en) | 1977-12-05 | 1977-12-05 | Method of continuous esterification |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14507977A JPS5479243A (en) | 1977-12-05 | 1977-12-05 | Method of continuous esterification |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5479243A true JPS5479243A (en) | 1979-06-25 |
Family
ID=15376887
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP14507977A Pending JPS5479243A (en) | 1977-12-05 | 1977-12-05 | Method of continuous esterification |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5479243A (en) |
-
1977
- 1977-12-05 JP JP14507977A patent/JPS5479243A/en active Pending
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