JPS54156822A - Manufacturing of graphite fiber with high strength - Google Patents
Manufacturing of graphite fiber with high strengthInfo
- Publication number
- JPS54156822A JPS54156822A JP6162078A JP6162078A JPS54156822A JP S54156822 A JPS54156822 A JP S54156822A JP 6162078 A JP6162078 A JP 6162078A JP 6162078 A JP6162078 A JP 6162078A JP S54156822 A JPS54156822 A JP S54156822A
- Authority
- JP
- Japan
- Prior art keywords
- fibers
- phosphorus
- high strength
- salt
- soaked
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000835 fiber Substances 0.000 title abstract 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract 2
- 229910002804 graphite Inorganic materials 0.000 title abstract 2
- 239000010439 graphite Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract 5
- 239000011574 phosphorus Substances 0.000 abstract 5
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- 239000011261 inert gas Substances 0.000 abstract 2
- -1 phosphorus compound Chemical class 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 229920002972 Acrylic fiber Polymers 0.000 abstract 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 150000001447 alkali salts Chemical class 0.000 abstract 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 238000010000 carbonizing Methods 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Inorganic Fibers (AREA)
Abstract
PURPOSE: Pretreated fibers made from acrylic fibers are soaked with phosphorus and heat treated under a specific tension in an inert gas atomsphere, thus manufacturing graphite fibers with high strength, high elasticity and excellent oxidation resistance.
CONSTITUTION: Pretreated fibers, which are made by oxidizing and carbonizing acrylonitrile fibers, are soaked with phosphorus to 0.001W0.1 wt% content and then graphitized by heating under a tension of 0.2W30 mg/d in an atmosphere of nitrogen or an inert gas to 1700W3500°C. A method of adding the phosphorus to the fibers is to soak the fibers into a solution or dispersion of a phosphorus compound such as phosphoric acid, or its ammonoium salt, alkali salt or alkaline earth salt, or a surface active agent containing phosphorus in water, or alcohol or acetone.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6162078A JPS54156822A (en) | 1978-05-25 | 1978-05-25 | Manufacturing of graphite fiber with high strength |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6162078A JPS54156822A (en) | 1978-05-25 | 1978-05-25 | Manufacturing of graphite fiber with high strength |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS54156822A true JPS54156822A (en) | 1979-12-11 |
| JPS5760448B2 JPS5760448B2 (en) | 1982-12-20 |
Family
ID=13176395
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP6162078A Granted JPS54156822A (en) | 1978-05-25 | 1978-05-25 | Manufacturing of graphite fiber with high strength |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS54156822A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58214524A (en) * | 1982-06-07 | 1983-12-13 | Toray Ind Inc | Continuous production of graphite fiber |
| JPS602711A (en) * | 1983-06-14 | 1985-01-09 | Mitsubishi Rayon Co Ltd | Preparation of graphite yarn |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5048227A (en) * | 1973-09-07 | 1975-04-30 | ||
| JPS52107328A (en) * | 1976-03-03 | 1977-09-08 | Toho Rayon Co Ltd | Production of carbon fiber from acrylic fiber |
-
1978
- 1978-05-25 JP JP6162078A patent/JPS54156822A/en active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5048227A (en) * | 1973-09-07 | 1975-04-30 | ||
| JPS52107328A (en) * | 1976-03-03 | 1977-09-08 | Toho Rayon Co Ltd | Production of carbon fiber from acrylic fiber |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58214524A (en) * | 1982-06-07 | 1983-12-13 | Toray Ind Inc | Continuous production of graphite fiber |
| JPS6224525B2 (en) * | 1982-06-07 | 1987-05-28 | Toray Industries | |
| JPS602711A (en) * | 1983-06-14 | 1985-01-09 | Mitsubishi Rayon Co Ltd | Preparation of graphite yarn |
| JPH0335406B2 (en) * | 1983-06-14 | 1991-05-28 | Mitsubishi Rayon Co |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5760448B2 (en) | 1982-12-20 |
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