JPS54109919A - Preparation of guanidine salt - Google Patents
Preparation of guanidine saltInfo
- Publication number
- JPS54109919A JPS54109919A JP1494978A JP1494978A JPS54109919A JP S54109919 A JPS54109919 A JP S54109919A JP 1494978 A JP1494978 A JP 1494978A JP 1494978 A JP1494978 A JP 1494978A JP S54109919 A JPS54109919 A JP S54109919A
- Authority
- JP
- Japan
- Prior art keywords
- guanidine
- acid
- solution containing
- preparation
- urea
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain guanidine (G) economically, by combining the separation step of G formed as a by-product, through an ion exchanger and various steps of purification, concentration, and drying with the urea preparation step organically.
CONSTITUTION: NH3 is reacted with CO2 at high temperature and pressure to prepare urea, and the liquor in the process is brought into contact with a cation exchanger. The adsorbed guanidine (G) is eluted with an acid, e.g. sulfuric acid, to give a solution containing a salt of G, from which acid radicals are removed by ion exchange, precipitation, or electrodialysis to form a solution containing G.
EFFECT: Inexpensive raw materials used, safe and free from explosion, and low cost.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1494978A JPS54109919A (en) | 1978-02-14 | 1978-02-14 | Preparation of guanidine salt |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1494978A JPS54109919A (en) | 1978-02-14 | 1978-02-14 | Preparation of guanidine salt |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS54109919A true JPS54109919A (en) | 1979-08-29 |
JPS5749541B2 JPS5749541B2 (en) | 1982-10-22 |
Family
ID=11875219
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP1494978A Granted JPS54109919A (en) | 1978-02-14 | 1978-02-14 | Preparation of guanidine salt |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS54109919A (en) |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5017455A (en) * | 1973-06-16 | 1975-02-24 |
-
1978
- 1978-02-14 JP JP1494978A patent/JPS54109919A/en active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5017455A (en) * | 1973-06-16 | 1975-02-24 |
Also Published As
Publication number | Publication date |
---|---|
JPS5749541B2 (en) | 1982-10-22 |
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