JPS4848448A - - Google Patents

Info

Publication number
JPS4848448A
JPS4848448A JP47102618A JP10261872A JPS4848448A JP S4848448 A JPS4848448 A JP S4848448A JP 47102618 A JP47102618 A JP 47102618A JP 10261872 A JP10261872 A JP 10261872A JP S4848448 A JPS4848448 A JP S4848448A
Authority
JP
Japan
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP47102618A
Other languages
Japanese (ja)
Other versions
JPS5336457B2 (cg-RX-API-DMAC7.html
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Publication of JPS4848448A publication Critical patent/JPS4848448A/ja
Publication of JPS5336457B2 publication Critical patent/JPS5336457B2/ja
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/002—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by dehydrogenation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/79—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C07C45/84—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation by azeotropic distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP10261872A 1971-10-14 1972-10-13 Expired JPS5336457B2 (cg-RX-API-DMAC7.html)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7114111A NL7114111A (cg-RX-API-DMAC7.html) 1971-10-14 1971-10-14

Publications (2)

Publication Number Publication Date
JPS4848448A true JPS4848448A (cg-RX-API-DMAC7.html) 1973-07-09
JPS5336457B2 JPS5336457B2 (cg-RX-API-DMAC7.html) 1978-10-03

Family

ID=19814252

Family Applications (1)

Application Number Title Priority Date Filing Date
JP10261872A Expired JPS5336457B2 (cg-RX-API-DMAC7.html) 1971-10-14 1972-10-13

Country Status (8)

Country Link
US (1) US3946076A (cg-RX-API-DMAC7.html)
JP (1) JPS5336457B2 (cg-RX-API-DMAC7.html)
BE (1) BE790104A (cg-RX-API-DMAC7.html)
DE (1) DE2250088C2 (cg-RX-API-DMAC7.html)
FR (1) FR2156332B1 (cg-RX-API-DMAC7.html)
GB (1) GB1353437A (cg-RX-API-DMAC7.html)
IT (1) IT968292B (cg-RX-API-DMAC7.html)
NL (1) NL7114111A (cg-RX-API-DMAC7.html)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58194834A (ja) * 1982-06-17 1983-11-12 Tokyo Ohka Kogyo Co Ltd シクロヘキサノンの精製方法
US4588829A (en) * 1984-07-27 1986-05-13 Exxon Research & Engineering Company (Disulfido)tris(N,N-substituted dithiocarbamato)Mo(V) complexes

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL7513664A (nl) * 1975-11-22 1977-05-24 Stamicarbon Werkwijze en inrichting voor het oxideren van cy- cloalkanen.
JPH06104637B2 (ja) * 1990-04-06 1994-12-21 三菱化成株式会社 シクロヘキサノン及びシクロヘキサノールの混合物から不純物を除去する方法
JPH0713146B2 (ja) * 1990-05-22 1995-02-15 信越化学工業株式会社 オルガノポリシロキサンの製造方法
US5883292A (en) * 1996-01-17 1999-03-16 Twenty-First Century Research Corporation Reaction control by regulating internal condensation inside a reactor
US6337051B1 (en) 1996-06-24 2002-01-08 Rpc Inc. Device for detecting formation of a second liquid phase
US6143927A (en) * 1996-06-24 2000-11-07 Rpc Inc. Methods for removing catalyst after oxidation of hydrocarbons
US6288270B1 (en) 1996-06-24 2001-09-11 Rpc Inc. Methods for controlling the reaction rate of a hydrocarbon to an acid by making phase-related adjustments
US6039902A (en) * 1996-06-24 2000-03-21 Rpc Inc. Methods of recycling catalyst in oxidations of hydrocarbons
US5922908A (en) * 1996-06-24 1999-07-13 Twenty-First Century Research Corporation Methods for preparing dibasic acids
WO1998007677A1 (en) 1996-08-21 1998-02-26 Twenty-First Century Research Corporation Methods and devices for controlling the reaction by adjusting the oxidant consumption rate
US5801273A (en) * 1996-08-21 1998-09-01 Twenty-First Century Research Corporation Methods and devices for controlling the reaction rate of a hydrocarbon to an intermediate oxidation product by pressure drop adjustments
US20010053864A1 (en) * 1996-08-21 2001-12-20 Decoster David C. Devices for controlling the reaction rate and/or reactivity of hydrocarbon to an intermediate oxidation product by adjusting the oxidant consumption rate
US6103933A (en) * 1996-11-07 2000-08-15 Rpc Inc. Methods for controlling the oxidation rate of a hydrocarbon by adjusting the ratio of the hydrocarbon to a rate-modulator
US5817868A (en) * 1996-11-12 1998-10-06 Twenty-First Century Research Corporation Method and devices for controlling the oxidation of a hydrocarbon to an acid by regulating temperature/conversion relationship in multi-stage arrangements
US5824819A (en) * 1996-12-18 1998-10-20 Twenty-First Century Research Corporation Methods of preparing an intermediate oxidation product from a hydrocarbon by utilizing an activated initiator
US6037491A (en) * 1997-07-25 2000-03-14 Rpc Inc. Methods and devices for controlling hydrocarbon oxidations to respective acids by adjusting the solvent to hydrocarbon ratio
US5929277A (en) 1997-09-19 1999-07-27 Twenty-First Century Research Corporation Methods of removing acetic acid from cyclohexane in the production of adipic acid
US5908589A (en) * 1997-12-08 1999-06-01 Twenty-First Century Research Corporation Methods for separating catalyst from oxidation mixtures containing dibasic acids
WO1999040058A1 (en) 1998-02-09 1999-08-12 Rpc, Inc. Process for treating cobalt catalyst in oxidation mixtures of hydrocarbons to dibasic acids
EP1056706A1 (en) * 1998-02-19 2000-12-06 RPC Inc. Methods and devices for separating catalyst from oxidation mixtures
US6433221B1 (en) 1998-07-02 2002-08-13 Rpc Inc. Methods of separating catalyst in solution from a reaction mixture produced by oxidation of cyclohexane to adipic acid
US6340420B1 (en) 1998-07-06 2002-01-22 Rpc Inc. Methods of treating the oxidation mixture of hydrocarbons to respective dibasic acids
JP2002542214A (ja) 1999-04-20 2002-12-10 アールピーシー インコーポレイテッド 触媒の水溶液中で水およびシクロヘキサノンを酢酸と置換する方法
US6255533B1 (en) 1999-11-09 2001-07-03 Basf Corporation Process for the recovery of cyclohexanone and cyclohexanol from cyclohexanone production distillation bottoms
RU2479564C1 (ru) * 2012-04-10 2013-04-20 Открытое акционерное общество "Щекиноазот" Способ омыления сложных эфиров в производстве капролактама, установка для его осуществления, способ утилизации натриевых солей органических кислот и установка для его осуществления

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2931834A (en) * 1960-04-05 Ctclohexane oxidation process
DE1233858B (de) * 1959-12-16 1967-02-09 Basf Ag Verfahren zur Gewinnung von reinem Cyclohexanon und Cyclohexanol
NL288272A (cg-RX-API-DMAC7.html) * 1963-01-28
DE1518255B1 (de) * 1965-01-30 1969-12-11 Vickers Zimmer Ag Verfahren zur Aufarbeitung des Reaktionsgemisches der Oxydation von Cyclohexan mit sauerstoffhaltigen Gasen in fluessiger Phase

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58194834A (ja) * 1982-06-17 1983-11-12 Tokyo Ohka Kogyo Co Ltd シクロヘキサノンの精製方法
US4588829A (en) * 1984-07-27 1986-05-13 Exxon Research & Engineering Company (Disulfido)tris(N,N-substituted dithiocarbamato)Mo(V) complexes

Also Published As

Publication number Publication date
BE790104A (fr) 1973-04-13
FR2156332A1 (cg-RX-API-DMAC7.html) 1973-05-25
DE2250088C2 (de) 1984-02-16
NL7114111A (cg-RX-API-DMAC7.html) 1973-04-17
US3946076A (en) 1976-03-23
GB1353437A (en) 1974-05-15
IT968292B (it) 1974-03-20
JPS5336457B2 (cg-RX-API-DMAC7.html) 1978-10-03
FR2156332B1 (cg-RX-API-DMAC7.html) 1977-12-23
DE2250088A1 (de) 1973-04-19

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