JPH11319535A - Throttling disk for particle-coating apparatus, apparatus for coating particle comprising throttling disk, and method for coating particle - Google Patents

Throttling disk for particle-coating apparatus, apparatus for coating particle comprising throttling disk, and method for coating particle

Info

Publication number
JPH11319535A
JPH11319535A JP10153955A JP15395598A JPH11319535A JP H11319535 A JPH11319535 A JP H11319535A JP 10153955 A JP10153955 A JP 10153955A JP 15395598 A JP15395598 A JP 15395598A JP H11319535 A JPH11319535 A JP H11319535A
Authority
JP
Japan
Prior art keywords
coating
disk
jet
tower
granules
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP10153955A
Other languages
Japanese (ja)
Other versions
JP3921813B2 (en
Inventor
Tadao Sato
忠夫 佐藤
Susumu Tamura
進 田村
Shigeo Fujii
重雄 藤井
武彦 ▲高▼橋
Takehiko Takahashi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JNC Corp
Original Assignee
Chisso Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chisso Corp filed Critical Chisso Corp
Priority to JP15395598A priority Critical patent/JP3921813B2/en
Publication of JPH11319535A publication Critical patent/JPH11319535A/en
Application granted granted Critical
Publication of JP3921813B2 publication Critical patent/JP3921813B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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  • Application Of Or Painting With Fluid Materials (AREA)
  • Spray Control Apparatus (AREA)
  • Glanulating (AREA)
  • Fertilizers (AREA)
  • Medical Preparation Storing Or Oral Administration Devices (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide a throttling disk for a particle-coating apparatus capable of preventing pulsation of a jet gas and a particle, evenly forming a coating on the surface of the particle, inhibiting the particle from aggregating in throttling parts, and possible to be manufactured by industrial mass production and to provide an apparatus for coating a particle and a method for coating a particle. SOLUTION: This throttling disk 52 for a particle-coating apparatus and produced by evenly forming a prescribed number of jetting holes 56 in a disk 54 as to control the aperture ratio of 10-70% is employed for a throttling part of a jetting tower. The throttling disk 52 is fitted to a lower part of a jetting tower while a coating liquid-jetting nozzle 26 being inserted into at least one of the jetting holes 56.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は粒体の被覆装置用絞
り円盤、同絞り円盤を備えた粒体の被覆装置、及び同装
置を用いる粒体の被覆方法に関する。更に詳述すれば、
槽内で粒体の噴流層を形成すると共に、これに被覆液を
噴霧して粒体を被膜で被覆する粒体の被覆装置用絞り円
盤、同被覆装置、及び同装置を用いる粒体の被覆方法に
関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a drawing disk for a particle coating apparatus, a particle coating apparatus provided with the drawing disk, and a method for coating particles using the apparatus. More specifically,
Forming a spouted bed of granules in a tank, spraying a coating liquid on the spouted bed, and coating the granules with a film; a drawing disk for a granule coating device; a coating device using the same; and a granule coating using the same device About the method.

【0002】[0002]

【従来の技術】噴流方式を用いた粒体の被覆方法は、例
えば特公昭38ー13896号に記載されているよう
に、円筒状の槽の下部を逆円錐形とし、その下端側を水
平方向に切断して気体噴流用の絞り部となし、該絞り部
を通して高速気体流を該槽内に垂直上方向に噴流せしめ
て槽内の被覆すべき粒体を吹き上げ、同時に被覆液を吹
き付けて粒体に被膜を被覆する方法である。特公昭38
ー2294号は、粒体を噴流塔内の中央噴流部に設けた
案内管を通して粒体を吹き上げ、該管内に設けた噴霧ノ
ズルから被覆液を噴霧する方法を開示している。更に特
公昭50ー1355号には、噴流部に案内管を設け、そ
の周辺部にも気体を通すことにより、粒体を流動状態、
或いはそれに近い無重力の状態におき、粒体同士の付着
等のトラブルを回避している。
2. Description of the Related Art As a method of coating particles using a jet flow method, for example, as described in Japanese Patent Publication No. 38-13896, the lower part of a cylindrical tank is formed in an inverted conical shape, and the lower end side is horizontally oriented. Into a narrowed portion for gas jetting, and a high-speed gas stream is jetted vertically upward into the tank through the narrowed portion to blow up particles to be coated in the tank, and simultaneously spray particles with the coating liquid. This is a method of coating the body with a coating. Tokiko 38
No. 2294 discloses a method in which the particles are blown up through a guide tube provided in a central jet portion in a jet tower, and a coating liquid is sprayed from a spray nozzle provided in the tube. In Japanese Patent Publication No. 50-1355, a guide tube is provided in the jet part, and gas is also passed around the jet part, so that the granules can be flowed.
Alternatively, it is placed in a weightless state close to the above, thereby avoiding troubles such as adhesion of the particles.

【0003】これらの被覆方法は、何れも医薬品を被覆
対象にしたもので、小規模、且つ丁重に被覆する場合に
は好ましい方法である。しかし、例えば肥料等を被覆対
象とする場合のように、安価に、大量に被覆する必要が
ある場合には、この方法は適切な方法とは言い難い。大
量の粒体を被覆する場合は、大きな径の噴流塔を用いる
必要があるが、噴流塔の径が大きくなると粒体全体が流
動状態となり、噴流層が形成できない問題がある。
[0003] All of these coating methods are intended for coating pharmaceuticals, and are preferable methods for small-scale and gentle coating. However, when it is necessary to coat a large amount at low cost, for example, when a fertilizer or the like is to be coated, this method is not an appropriate method. When coating a large amount of particles, it is necessary to use a jet tower having a large diameter. However, when the diameter of the jet tower is large, the whole particles are in a flowing state, and there is a problem that a spouted bed cannot be formed.

【0004】この問題点に対し、特公平2ー31939
号は、噴流槽が大型化しても噴流状態が得られる技術を
開示している。即ち、肥料の様に、大量に生産し、供給
するために、大きな径の噴流塔を用いた噴流装置内にガ
イド管をオリフィス上部に垂直に設けた被覆装置を用
い、オリフィスから装置内に不活性気体を導入する際
に、オリフィスにおける気体の流速を20m/sec〜
70m/secとし、ガイド管内の流速を20m/se
c以下に調節して被覆を行なうものである。
To solve this problem, Japanese Patent Publication No. 2-3939
Discloses a technique in which a jet state can be obtained even when a jet tank becomes large. In other words, in order to produce and supply a large amount like fertilizer, a coating device in which a guide tube is provided vertically above an orifice in a jet device using a large-diameter jet tower is used. When introducing the active gas, the flow velocity of the gas at the orifice is set to 20 m / sec or more.
70 m / sec, and the flow velocity in the guide tube is 20 m / sec.
The coating is performed by adjusting the value to c or less.

【0005】一方、近頃では特開平6ー9303号、特
開平6ー9304号、特開平6ー72805号、特開平
6ー80514号、特開平5ー29634号、特開平4
ー202078号、特開平4ー202079号、特開平
6ー87684号に開示されているような、施肥後一定
期間は活性成分が溶出されないか、若しくは溶出が極端
に抑制された期間(この期間を以後初期溶出期間と称
す)を有する、いわゆる時限溶出型のパターンを有する
被膜を肥料粒体の表面に被覆した被覆粒体肥料が開示さ
れている。
On the other hand, recently, JP-A-6-9303, JP-A-6-9304, JP-A-6-72805, JP-A-6-80514, JP-A-5-29634 and JP-A-5-29634 have recently been disclosed.
As disclosed in JP-A-202078, JP-A-4-202079 and JP-A-6-87684, the active ingredient is not eluted for a certain period after fertilization or the period in which the elution is extremely suppressed (this period is referred to as A coated granular fertilizer in which the surface of a fertilizer granule is coated with a coating having a so-called timed elution type pattern having an initial dissolution period) is disclosed.

【0006】このような時限溶出型の溶出パターンを持
つ被膜を肥料粒体の表面に被覆した被覆粒体肥料を、前
記特公平2ー31939号に記載されている様に、噴流
塔を用いて安価、大量に製造する場合、粒体への被覆樹
脂溶液の付着のさせ方、及び付着した樹脂溶液からの溶
剤の飛散、乾燥の状態が、生産効率及び得られる被覆粒
体肥料の活性成分の溶出パターンに大きく影響を及ぼす
と考えられる。
[0006] The coated granular fertilizer in which the surface of the fertilizer granules is coated with a coating having such a time-dissolved elution pattern is applied to the fertilizer granules by using a jet tower as described in JP-B-2-31939. In the case of inexpensive, large-scale production, the method of attaching the coating resin solution to the granules, the scattering of the solvent from the adhered resin solution, and the state of drying are affected by the production efficiency and the active ingredient of the obtained coated granule fertilizer. It is thought to have a significant effect on the elution pattern.

【0007】大型噴流塔を用いて被覆粒体肥料を大量に
製造する場合、経済的に生産効率を上げるためには、乾
燥時間を短縮することが重要と考えられ、従来も乾燥時
間を短縮するために、樹脂溶液の供給量を高め、更に粒
体表面に付着した樹脂溶液に含まれる溶剤を大量かつ高
温の噴流ガスを用いて飛散、乾燥させることがしばしば
試みられている。
When a large amount of coated granular fertilizer is produced using a large spout tower, it is considered important to shorten the drying time in order to economically increase the production efficiency, and the drying time is conventionally shortened. For this reason, it is often attempted to increase the supply amount of the resin solution and to scatter and dry the solvent contained in the resin solution attached to the surface of the granules using a large amount and high-temperature jet gas.

【0008】しかし、噴流塔を用いて、例えば尿素粒体
の様な比較的低融点の粒体を被覆する場合は、噴流ガス
温度を尿素粒体の融点以下に保たなければならず、この
ため高温の噴流ガスを用いて生産効率を高めることがで
きない。即ち、噴流ガスの温度を尿素粒体の融点以上に
して被覆を行うと、噴流塔内で不均一な溶剤の飛散や乾
燥が起こり、このためガイド管外側に存在する尿素粒体
からなる環状の尿素粒体堆積層(固定層)の一部が融解
固結したり、また塔下部の逆円錐型先端の気体噴流用絞
りへの尿素粒体の融解固結等が起こり、このため粒体の
均一な循環が出来なくなることがあり、実質的な操業が
出来なくなることがある。
However, when using a jet tower to coat particles having a relatively low melting point, such as urea particles, the temperature of the jet gas must be kept below the melting point of the urea particles. Therefore, the production efficiency cannot be increased by using a high-temperature jet gas. That is, when coating is performed with the temperature of the jet gas being equal to or higher than the melting point of the urea granules, uneven scattering and drying of the solvent occur in the jet tower, and therefore, the annular urea granules formed outside the guide tube are formed. A part of the urea particle deposition layer (fixed layer) is melted and solidified, and the urea particles are melted and solidified into the gas jet throttle at the inverted conical tip at the bottom of the tower. In some cases, uniform circulation cannot be performed, and substantial operation cannot be performed.

【0009】また、噴流ガスの温度を尿素粒体の融点以
下に保って噴流ガスの量を高めた場合は、噴流塔下部よ
りガイド管に送られる粒体の量が変動し、いわゆる脈動
現象を起こすので運転が不安定となる。この場合は、尿
素粒体の被覆被膜の損傷を生じ易く、得られる被覆肥料
は初期溶出抑制期間内の活性成分の溶出量が大きなもの
になる。即ち、得られる被覆肥料は、施肥直後から急激
に活性成分が溶出し始めるものが多くなる。従って、従
来の噴流方式により所望の溶出機能を有する時限溶出型
被覆肥料を大量に、生産効率良く製造することは極めて
困難なものである。
When the temperature of the jet gas is kept below the melting point of the urea particles to increase the amount of the jet gas, the amount of the particles sent from the lower part of the jet tower to the guide tube fluctuates, causing a so-called pulsation phenomenon. The operation becomes unstable. In this case, the coating film of the urea granules is liable to be damaged, and the obtained coated fertilizer has a large amount of active ingredient eluted during the initial elution suppression period. That is, many of the obtained coated fertilizers rapidly elute the active ingredient immediately after fertilization. Therefore, it is extremely difficult to produce a large amount of time-dissolved coated fertilizer having a desired dissolution function by a conventional jet method with high production efficiency.

【0010】更に、従来の絞りは、図4に示すような、
円盤80の中央部に穿設した噴出孔82を有する絞り盤
若しくはオリフィスと呼ばれる、いわゆるドーナツ型の
気体噴出体84を塔下部の逆円錐型先端に設けることに
より構成している。このような気体噴出体84上面に
は、塔内を降下してくる被覆粒体が堆積し、融解固結す
る問題もあった。
[0010] Further, the conventional diaphragm is as shown in FIG.
A so-called donut-shaped gas ejection body 84 called an orifice having an ejection hole 82 formed in the center of the disk 80 is provided at the tip of the inverted cone at the bottom of the tower. There is also a problem that the coated particles falling down in the tower are deposited on the upper surface of the gas ejector 84 and melted and solidified.

【0011】[0011]

【発明が解決しようとする課題】本発明者らは上記の従
来技術の問題に鑑み、その原因が何処にあるかの究明に
努めた。その結果、噴流方式において、噴流ガスの温度
を尿素粒体の融点以上にして尿素粒体の表面に被膜を被
覆する場合、尿素粒体を被覆する樹脂溶液の噴霧が均一
でも、噴流ガス及び尿素粒体の脈動が起こり、溶剤の気
化熱による噴流ガスの温度の低下が部分的に起きない個
所が生じ、このため高温の噴流ガスによる尿素粒体の融
解、固結を生じることを発見した。
SUMMARY OF THE INVENTION In view of the above-mentioned problems of the prior art, the present inventors have sought to find out where the cause is. As a result, in the jet method, when the temperature of the jet gas is set to be equal to or higher than the melting point of the urea granules to coat the surface of the urea granules, even if the spray of the resin solution covering the urea granules is uniform, the jet gas and urea It has been discovered that pulsation of the granules occurs, causing a portion where the temperature of the jet gas does not partially decrease due to the heat of vaporization of the solvent, thereby melting and consolidating the urea granules by the high-temperature jet gas.

【0012】更に、噴流ガスの温度を尿素粒体の融点以
下に保っていても、噴流ガスの噴出量を増加すると噴流
ガスに偏流が生じること、このためガイド管に送られる
粒体の量が変動する、いわゆる脈動現象が起こり、被覆
された尿素粒体が噴流塔上部の壁に衝突して被覆粒体の
被膜が損傷することを発見した。
Furthermore, even if the temperature of the jet gas is kept below the melting point of the urea granules, increasing the jet amount of the jet gas causes a drift in the jet gas, so that the amount of the granules sent to the guide tube is reduced. It was discovered that a fluctuating, so-called pulsation phenomenon occurred, and that the coated urea particles collided with the upper wall of the spout tower and damaged the coating of the coated particles.

【0013】また更に、絞り部に粒体が融着すること
が、上記問題が起きる原因の一つであることも発見し
た。
Further, it has been found that the fusion of the particles to the narrowed portion is one of the causes of the above-mentioned problem.

【0014】本発明は上記知見に基づきなされたもの
で、その目的とするところは、噴流ガス、及び粒体の脈
動を防止し、均一で、安定した噴流状態を保持し、従っ
て均一に粒体表面に被膜を被覆でき、更に絞り部に粒体
が融着する事を防止し、工業的に大量処理することので
きる、粒体の被覆装置用絞り円盤、同絞り円盤を具備し
た粒体の被覆装置、及び粒体の被覆方法を提供すること
にある。
The present invention has been made on the basis of the above findings, and has as its object to prevent the pulsation of the jet gas and the granules, to maintain a uniform and stable jet state, and thus to uniformly form the granules. It is possible to coat the surface with a coating, further prevent the particles from being fused to the drawn portion, and to industrially mass-process the drawn disk for a coating device for the granular material, the granular material provided with the drawn disk. An object of the present invention is to provide a coating apparatus and a method for coating granules.

【0015】[0015]

【課題を解決するための手段】上記目的を達成するため
に本発明は、〔1〕 所定数の噴出孔を均一に円盤主
体に穿設してなり、その開口率が10〜70%である粒
体の被覆装置用絞り円盤であって、前記絞り円盤の噴出
孔の少なくとも1個に被覆液噴霧ノズルを挿入して噴流
塔の下部に取り付けられ、噴流塔の下部から前記噴出孔
を通して噴流塔内に気体を噴出させて前記噴流塔内に粒
体の噴流層を形成すると共に、前記噴流層を形成する粒
体に前記ノズルから被覆液を噴霧して前記粒体を被膜で
被覆する粒体の被覆装置の噴流塔の下部に取付けて気体
を噴流塔内に噴出させることを特徴とする粒体の被覆装
置用絞り円盤を提案するものである。
In order to achieve the above-mentioned object, the present invention provides: [1] A predetermined number of ejection holes are uniformly formed mainly in a disk, and the opening ratio is 10 to 70%. A throttle disk for a coating apparatus for a granular material, wherein a coating liquid spray nozzle is inserted into at least one of the ejection holes of the throttle disk and attached to a lower part of a jet tower, and a jet tower is provided from a lower part of the jet tower through the jet hole. A particle formed by spraying a gas into the spout tower to form a spouted layer of particles in the spout tower, and spraying a coating liquid from the nozzle onto the particles forming the spouted bed to coat the particles with a coating film The present invention proposes a throttle disk for a coating apparatus for granular material, which is attached to a lower portion of a jet tower of a coating apparatus and ejects gas into the jet tower.

【0016】また、本発明は〔2〕 上記〔1〕に記載
の絞り円盤が取り付けられていることを特徴とする粒体
の被覆装置であり、〔3〕 〔2〕の被覆装置は、噴流
塔内にその軸方向を垂直に取り付けたガイド管を有する
場合を含む。
The present invention also provides [2] a granule coating apparatus to which the drawing disk according to the above [1] is attached. [3] The coating apparatus according to [2], This includes the case where the tower has a guide tube whose axis is vertically mounted in the tower.

【0017】更に本発明は、〔4〕 所定数の噴出孔
を均一に円盤主体に穿設してなり、その開口率が10〜
70%である絞り円盤を噴流塔の下部に取り付けると共
に、前記絞り円盤の噴出孔の少なくとも1個に噴霧ノズ
ルを挿入し、前記噴霧ノズルの上方であって前記噴流塔
内に垂直にガイド管を設けてなる噴流塔を有する粒体の
被覆装置を用い、前記絞り円盤の噴出孔を通して噴流塔
内に気体を噴出させて前記噴流塔内に粒体の噴流層を形
成すると共に、前記噴流層を形成する粒体に噴霧ノズル
から被覆液を噴霧して前記粒体を被膜で被覆することを
特徴とする粒体の被覆方法である。
The present invention further provides: [4] A predetermined number of ejection holes are uniformly formed mainly in a disk, and the opening ratio thereof is 10 to 10.
A 70% throttle disk is attached to the lower part of the jet tower, and a spray nozzle is inserted into at least one of the ejection holes of the throttle disk, and a guide pipe is provided vertically above the spray nozzle and in the jet tower. Using a granule coating apparatus having a spout tower provided, a gas is spouted into the spout tower through the spout hole of the throttle disk to form a spouted bed of granules in the spout tower, and the spouted bed is formed. A method for coating granules, comprising spraying a coating liquid from a spray nozzle onto the granules to be formed, and coating the granules with a coating.

【0018】[0018]

【発明の実施の形態】以下、図面を参照しながら本発明
を詳細に説明する。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Hereinafter, the present invention will be described in detail with reference to the drawings.

【0019】図1は、本発明の粒体の被覆装置の構成の
一例を示すもので、図1中、2は垂直に設けた噴流塔で
ある。前記噴流塔2は、主要部を円筒状の槽主体4で構
成している。
FIG. 1 shows an example of the configuration of a granule coating apparatus according to the present invention. In FIG. 1, reference numeral 2 denotes a vertically installed jet tower. The main part of the jet tower 2 is constituted by a cylindrical tank main body 4.

【0020】前記槽主体4の形状には、特に制限が無
く、水平方向断面の形状が円形であっても、多角形のも
のであってもよい。しかし、粒体の槽主体4内における
循環の均一性の面から云えば、前記槽主体4の断面の形
状は円形であることが望ましい。
The shape of the tank main body 4 is not particularly limited, and the shape of the horizontal section may be circular or polygonal. However, from the aspect of uniformity of circulation of the particles in the tank main body 4, it is desirable that the cross section of the tank main body 4 is circular.

【0021】前記槽主体4の内部には、円筒状のガイド
管6を不図示の固定手段で取り付けてある。
A cylindrical guide tube 6 is attached to the inside of the tank main body 4 by fixing means (not shown).

【0022】前記ガイド管6の形状としては、円筒状の
他、パイプに穿孔したもの、或いは金網を筒状にしたも
の等が挙げられる。ガイド管6の形状や材質は特に限定
するものではないが、被覆時の被膜の損傷を最小限に抑
えたい場合には、孔や突起物の無い平滑なパイプ、或い
はパイプの内面にフッ素樹脂をライニングしたものを用
いることが好ましい。ガイド管6は前記絞り部10の上
方であって槽主体4内に、ガイド管6の軸方向を垂直に
して固定若しくは懸垂する。
The shape of the guide tube 6 is not limited to a cylindrical shape, but may be a hole formed in a pipe or a wire mesh formed in a cylindrical shape. The shape and material of the guide tube 6 are not particularly limited. However, if it is desired to minimize damage to the coating at the time of coating, a smooth pipe without holes or protrusions, or a fluororesin is applied to the inner surface of the pipe. It is preferable to use a lining. The guide tube 6 is fixed or suspended in the tank main body 4 above the throttle unit 10 with the axial direction of the guide tube 6 being vertical.

【0023】槽主体4の下部側は下方に向かうに従って
徐々に内径を小さく形成した逆錘状の底部8を有すると
共に、底部8の下端側を貫通して槽主体4よりも小径の
絞り部10を形成してある。絞り部10には別途種々の
オリフィス板やベンチュリを挿入できるように構成して
もよい。
The lower portion of the tank body 4 has an inverted conical bottom 8 whose inner diameter is gradually reduced toward the bottom, and a narrowed portion 10 having a smaller diameter than the tank body 4 penetrating through the lower end of the bottom 8. Is formed. The orifice section 10 may be configured so that various orifice plates or venturis can be inserted separately.

【0024】前記絞り部10には、抜き出し管12の一
端が連結してあり、またその他端側は開閉弁14を介し
て被覆粒体抜き出し口16になっている。前記抜き出し
管12には気体供給管18の一端が連結してあり、この
気体供給管18はその中間に気体加熱器20を介して他
端をブロアー22に連結している。これにより、ブロア
ー22から供給される気体は気体加熱器20で加熱され
た後、絞り部10を通って槽主体4内に噴出される。な
お、24は気体供給管に介装した流量計である。
One end of an extraction pipe 12 is connected to the restricting section 10, and the other end side is formed as a coating particle extraction port 16 through an on-off valve 14. One end of a gas supply pipe 18 is connected to the extraction pipe 12, and the other end of the gas supply pipe 18 is connected to a blower 22 via a gas heater 20 in the middle. As a result, the gas supplied from the blower 22 is heated by the gas heater 20 and then jetted into the tank main body 4 through the throttle unit 10. Reference numeral 24 denotes a flow meter interposed in the gas supply pipe.

【0025】本発明に用いる気体は粒体及び溶剤に対し
て不活性のものであれば良く、特に限定されるものでは
ない。具体的には、空気、窒素ガス、ヘリウムガス、又
は噴流塔出口ガスから被覆液中の有機溶剤を一部除去し
たリサイクルガス等が例示できる。
The gas used in the present invention is not particularly limited as long as it is inert to the particles and the solvent. Specific examples include air, nitrogen gas, helium gas, and a recycle gas in which the organic solvent in the coating liquid is partially removed from the outlet gas of the jet tower.

【0026】前記絞り部10の中心近傍には、噴霧ノズ
ル26が配設してある。噴霧ノズル26は前記絞り部1
0の中心軸方向に沿って絞り部10の近傍にあれば良
く、前記絞り部10よりも高い位置であっても、低い位
置であっても良い。噴霧ノズル10の位置、形状は噴霧
液体の性状、運転条件等によって適宜決定する。
A spray nozzle 26 is provided near the center of the throttle unit 10. The spray nozzle 26 is connected to the throttle unit 1.
It suffices if it is in the vicinity of the throttle unit 10 along the central axis direction of 0, and may be a position higher or lower than the throttle unit 10. The position and shape of the spray nozzle 10 are appropriately determined depending on the properties of the spray liquid, operating conditions, and the like.

【0027】前記噴霧ノズル26には、被覆液供給ポン
プ28を介装した被覆液供給管30の一端が連結してあ
ると共に、被覆液供給管30の他端は被覆液調製槽32
に連結してある。被覆液調製槽32で調製された被覆液
は、被覆液供給ポンプ28によって、被覆液供給管30
を通って噴霧ノズル26に送られ、その後槽主体4内に
噴霧される。なお、34は蒸気加熱用ジャケットであ
る。
The spray nozzle 26 is connected to one end of a coating liquid supply pipe 30 provided with a coating liquid supply pump 28, and the other end of the coating liquid supply pipe 30 is connected to a coating liquid preparation tank 32.
Connected to. The coating liquid prepared in the coating liquid preparation tank 32 is supplied to the coating liquid supply pipe 30 by the coating liquid supply pump 28.
Through the spray nozzle 26 and then sprayed into the tank body 4. Reference numeral 34 denotes a steam heating jacket.

【0028】36は前記槽主体4に形成した粒体投入口
で、この投入口を通して粒体が槽主体4内に供給され、
噴流層37を形成し、粒体表面に被膜が被覆される。な
お、38は粒体投入口バルブ、39は粒体である。
Numeral 36 denotes a granule input port formed in the tank main body 4, through which the granules are supplied into the tank main body 4.
The spouted layer 37 is formed, and the film is coated on the surface of the granular material. In addition, 38 is a granule inlet valve and 39 is a granule.

【0029】また、40は槽主体4の上部壁42に取り
付けた排出管で、これを通して槽主体4内の気体が外部
に放出される。
Reference numeral 40 denotes a discharge pipe attached to the upper wall 42 of the tank main body 4, through which gas in the tank main body 4 is discharged to the outside.

【0030】なお、44は噴流部周縁部46を落下した
粒体が堆積して形成した粒体堆積層である。
Reference numeral 44 denotes a particle deposition layer formed by depositing particles that have fallen on the peripheral edge portion 46 of the jet part.

【0031】図2は、前記図1において、絞り部10に
取り付ける絞り円盤52の一例を示すものである。絞り
円盤52は、円盤主体54に、その中心を中心とする同
心円上に中心を持つ、互いにほぼ等間隔離れた所定数
(本図では4個)の噴出孔56を穿設してある。前記噴
出孔56を同心円上でほぼ等間隔離れて円盤主体54に
均一に穿設する事により、各噴出孔56を通過する気体
を均一に噴流塔内に噴出させることができるものであ
る。
FIG. 2 shows an example of the drawing disk 52 attached to the drawing section 10 in FIG. The aperture disk 52 is provided with a predetermined number (four in this figure) of ejection holes 56 having a center on a concentric circle centered on the center of the disk main body 54 and spaced substantially at equal intervals from each other. By uniformly piercing the jet holes 56 in the disk main body 54 at substantially equal intervals on a concentric circle, the gas passing through each jet hole 56 can be jetted uniformly into the jet tower.

【0032】なお、図2においては、噴出孔56を4個
穿設したが、これに限られず2個以上の任意の個数の噴
出個を穿設する事ができるものであるが、通常4〜10
個とすることが実用上好ましい。また、図2においては
噴出孔56を同心円上に形成したが、例えば碁盤目の格
子点状、千鳥状、その他任意の配列を採用することがで
き、要するに噴出孔56を円盤主体54に均一になるよ
うに穿設し、各噴出孔を通過する気体が均一に噴流塔内
に噴出できる様に配列にすれば良いものである。
In FIG. 2, four ejection holes 56 are formed. However, the invention is not limited to this, and any number of two or more ejection holes can be formed. 10
It is practically preferable to make the number. Further, in FIG. 2, the ejection holes 56 are formed on concentric circles. However, for example, a grid-like grid point, a staggered shape, or any other arrangement can be adopted, that is, the ejection holes 56 are uniformly formed on the disk main body 54. What is necessary is just to arrange | position so that the gas which passes through each ejection hole may be ejected uniformly into a jet tower.

【0033】前記噴出孔56の円盤主体54に対する開
口率、即ち下記式(1) 開口率(%)=(噴出孔面積の合計/穿孔前の円盤主体の面積)×100 (1) で示される開口率は、10〜70%が好ましく、特に2
0〜60%が好ましい。開口率が10%未満の場合は、
絞り円盤の上面に粒体が堆積固結し易くなる。また、開
口率が70%を超える場合は、絞り部の絞り作用が不十
分になり、充分な気体の噴流速度を得難くなる傾向にあ
る。
The opening ratio of the ejection holes 56 with respect to the disk main body 54, that is, the following formula (1): Opening ratio (%) = (total area of injection holes / area of disk main body before perforation) × 100 (1) The aperture ratio is preferably from 10 to 70%, particularly preferably 2 to 70%.
0-60% is preferred. If the aperture ratio is less than 10%,
The particles are easily deposited and solidified on the upper surface of the drawing disk. On the other hand, if the aperture ratio exceeds 70%, the throttle effect of the throttle portion becomes insufficient, and it tends to be difficult to obtain a sufficient gas jet velocity.

【0034】前記絞り円盤52を噴流塔の絞り部10に
取り付ける場合は、図2に示すように、噴霧ノズル26
が噴出孔56の中心を通るように、絞り円盤52を水平
に絞り部10に取り付けるものである。絞り円盤52を
このように取り付けることにより、ブロアー22から供
給される気体は、円盤主体54と被覆液供給管30又は
噴霧ノズル26との間隙60を通って槽主体4内に噴出
するものである。
When the throttle disk 52 is attached to the throttle section 10 of the jet tower, as shown in FIG.
The diaphragm disk 52 is attached to the diaphragm unit 10 horizontally so that the hole passes through the center of the ejection hole 56. By attaching the throttle disk 52 in this manner, the gas supplied from the blower 22 is ejected into the tank main body 4 through the gap 60 between the disk main body 54 and the coating liquid supply pipe 30 or the spray nozzle 26. .

【0035】なお、図2においては各噴出孔毎に噴霧ノ
ズル26をそれぞれ設けているが、これに限られず、図
3に示すように噴霧ノズル26を設けない噴出孔56
a、56bがあっても良い。この場合も、噴霧ノズル2
6はなるべく円盤主体52内において、均一に配置する
ことが望ましい。
In FIG. 2, the spray nozzles 26 are provided for each of the ejection holes. However, the present invention is not limited to this. As shown in FIG.
a and 56b may be provided. Also in this case, the spray nozzle 2
6 are preferably arranged as uniformly as possible in the disk main body 52.

【0036】絞り部10における気体流速は、噴出気体
量と絞り口径とによって決まる。また、ガイド管6内の
気体流速も同じ手法で計算することが出来る。ガイド管
6と絞り部10との間隔は粒体の循環を妨げない範囲で
選定することが好ましい。ガイド管6の口径は、絞り円
盤52に穿設した噴出口56の合計面積に相当する口径
の1.2〜4倍が好ましく、特に1.5〜3倍がより好
ましい。本発明においては、絞り部10における気体の
流速、及びガイド管内における気体の流速は特に限定す
るものではないが、品質の安定のためには絞り部10か
ら装置内に不活性気体を送入する際の、絞り円盤52に
穿設した噴出口56における気体の流速を20〜から7
0m/secとし、ガイド管6内の気体の流速を循環粒
体の終端速度の0.5〜3倍に調節して被覆を行う方法
が推奨される。
The gas flow velocity in the throttle unit 10 is determined by the amount of gas ejected and the throttle diameter. Further, the gas flow velocity in the guide tube 6 can be calculated by the same method. It is preferable that the distance between the guide tube 6 and the constricted portion 10 be selected within a range that does not hinder the circulation of the particles. The diameter of the guide tube 6 is preferably 1.2 to 4 times, more preferably 1.5 to 3 times, the diameter corresponding to the total area of the ejection ports 56 formed in the throttle disk 52. In the present invention, the gas flow rate in the throttle unit 10 and the gas flow rate in the guide tube are not particularly limited, but in order to stabilize the quality, an inert gas is sent from the throttle unit 10 into the apparatus. At this time, the flow rate of gas at the jet port 56 formed in the throttle disk 52 is
A method is recommended in which the coating is performed by adjusting the flow velocity of the gas in the guide tube 6 to 0.5 to 3 times the terminal velocity of the circulating particles at 0 m / sec.

【0037】本発明の被覆装置において、被覆される粒
体には特に制限がないが、本発明の被覆装置による被覆
は、粒体に含まれる活性成分の溶出速度を調節する必要
性のある粒体の場合に、特に有効である。活性成分はそ
の使用目的、用途等により異なるが、尿素、硫安、塩
安、硝安、塩化加里、硫酸加里、硝酸加里、硝酸ソー
ダ、燐酸アンモニア、燐酸加里、燐酸石灰、キレート
鉄、酸化鉄、塩化鉄、ホウ酸、ホウ砂、硫酸マンガン、
塩化マンガン、硫酸亜鉛、硫酸銅、モリブデン酸ナトリ
ウム、モリブデン酸アンモニウム、OMUP(クロチリ
デンジウレア)、IBDU(イソブチリデンジウレア)
やオキザマイド等の肥料、殺虫剤、殺菌剤、除草剤等の
農薬等が例示できる。粒体は1種以上の活性成分の粒状
物であっても良く、更には活性成分の1種以上とベント
ナイト、ゼオライト、タルク、クレー、ケイソウ土等の
不活性担体とからなる粒状物であっても良い。更には、
前述の活性成分粒体を樹脂や無機物で被覆したものであ
ってもよい。
In the coating apparatus of the present invention, the granules to be coated are not particularly limited. However, the coating by the coating apparatus of the present invention requires the control of the elution rate of the active ingredient contained in the granules. Particularly effective for the body. The active ingredient varies depending on the purpose and use of the active ingredient. Iron, boric acid, borax, manganese sulfate,
Manganese chloride, zinc sulfate, copper sulfate, sodium molybdate, ammonium molybdate, OMUP (clotilidene diurea), IBDU (isobutylidene diurea)
And pesticides such as insecticides, fungicides, herbicides, and the like. The granules may be granules of one or more active ingredients, and further granules comprising one or more active ingredients and an inert carrier such as bentonite, zeolite, talc, clay, diatomaceous earth and the like. Is also good. Furthermore,
The above-mentioned active ingredient particles may be coated with a resin or an inorganic substance.

【0038】これらの粒体の粒径は特に制限はないが、
0.1〜10mm、特に1〜5mmのものが好ましい。
The particle size of these particles is not particularly limited,
It is preferably from 0.1 to 10 mm, particularly preferably from 1 to 5 mm.

【0039】本発明の被覆装置において、粒体の被覆に
用いる被覆材は特に限定されるものではないが、時限溶
出型の被覆粒体を製造する場合は、粒体に含まれる活性
成分の溶出を厳密に制御できる材料、組成のものを選択
すればよい。このような被覆材としては、硫黄に代表さ
れる無機被覆材や、アルキッド樹脂、フェノール樹脂、
エポキシ樹脂等の熱硬化性樹脂、ポリエチレン、ポリプ
ロピレン等のポリオレフィンやポリ塩化ビニリデン等の
熱可塑性樹脂が挙げられる。
In the coating apparatus of the present invention, the coating material used for coating the granules is not particularly limited. However, in the case of producing time-eluting coated granules, the elution of the active ingredient contained in the granules is required. What is necessary is just to select the material and composition of which can control strictly. As such a coating material, an inorganic coating material represented by sulfur, an alkyd resin, a phenol resin,
Examples include thermosetting resins such as epoxy resins, polyolefins such as polyethylene and polypropylene, and thermoplastic resins such as polyvinylidene chloride.

【0040】これらのうち、肥料や農薬のように、厳
密、且つ長期に亘る溶出制御が求められる活性成分を含
む粒体を被覆する場合は、被覆材として熱硬化性樹脂や
熱可塑性樹脂を用いることが好ましく、より高度な溶出
制御が必要であれば、熱可塑性樹脂を用いることが特に
好ましい。
Of these, thermosetting resins and thermoplastic resins are used as coating materials when coating granules containing active ingredients that require strict and long-term dissolution control, such as fertilizers and agricultural chemicals. It is preferable to use a thermoplastic resin if more sophisticated elution control is required.

【0041】好ましい熱可塑性樹脂としては、ポリオレ
フィン及びその共重合体と、ポリ塩化ビニリデン及びそ
の共重合体とを挙げることができる。好ましいポリオレ
フィン及びその共重合体としてはポリエチレン、ポリプ
ロピレン、エチレン・プロピレン共重合体、エチレン・
酢酸ビニル共重合体、エチレン・一酸化炭素共重合体、
エチレン・酢酸ビニル・一酸化炭素共重合体、エチレン
・アクリレート共重合体、エチレン・メタクリル酸共重
合体、ゴム系樹脂、ポリスチレン、ポリメチルメタアク
リレート等を挙げることができ、好ましいポリ塩化ビニ
リデン及びその共重合体としては、ポリ塩化ビニリデ
ン、塩化ビニリデン・塩化ビニル共重合体等を挙げるこ
とができる。更に、ポリ−2−ハイドロキシ−2−アル
キル酢酸、ポリ−3−ハイドロキシ−3−アルキルプロ
ピオン酸等に代表される生分解性ポリエステルも挙げる
ことができる。
Preferred thermoplastic resins include polyolefins and copolymers thereof, and polyvinylidene chloride and copolymers thereof. Preferred polyolefins and copolymers thereof are polyethylene, polypropylene, ethylene / propylene copolymer, ethylene / propylene.
Vinyl acetate copolymer, ethylene / carbon monoxide copolymer,
Ethylene / vinyl acetate / carbon monoxide copolymer, ethylene / acrylate copolymer, ethylene / methacrylic acid copolymer, rubber resin, polystyrene, polymethyl methacrylate, etc. Examples of the copolymer include polyvinylidene chloride, vinylidene chloride / vinyl chloride copolymer, and the like. Further, biodegradable polyesters represented by poly-2-hydroxy-2-alkylacetic acid, poly-3-hydroxy-3-alkylpropionic acid and the like can also be mentioned.

【0042】これらの被覆材は有機溶剤に溶解させ、噴
流塔内において噴流状態にある粒体に噴霧して被覆を行
っても良く、また溶融状態で噴霧しても良いが、本発明
においては、上記樹脂の貧溶媒溶液を用い、これを粒体
に噴霧すると共に瞬間乾燥することによって被膜を形成
する製膜法において特に有効である。上記樹脂の貧溶媒
を用いて瞬間乾燥する場合には、樹脂と有機溶剤との組
み合わせにおいて、熱時には高濃度で溶解し、冷時には
樹脂が析出してゼリー状となる性質を有する組み合わせ
が好ましい。この組み合わせによる被膜は非常に緻密な
被膜を形成するので、特に時限溶出型の被膜形成に適し
ている。
These coating materials may be dissolved in an organic solvent and sprayed on the granules in a jet state in a jet tower to perform coating, or may be sprayed in a molten state. It is particularly effective in a film forming method in which a film is formed by using a poor solvent solution of the above resin, spraying the solution onto granules and instantaneously drying the granules. In the case of instantaneous drying using a poor solvent for the above resin, a combination of a resin and an organic solvent having a property of dissolving at a high concentration when heated, and precipitating and forming a jelly-like resin when cooled is preferable. Since the film formed by this combination forms a very dense film, it is particularly suitable for forming a time-eluting film.

【0043】上記以外の被覆材としては、タルクに代表
される無機フィラーや、界面活性剤等を用いることもで
きる。これらの被覆材は溶剤に溶解・分散、若しくは溶
融・分散され、噴霧用ノズルに送られ被覆に共される。
As a coating material other than the above, an inorganic filler represented by talc, a surfactant or the like can be used. These coating materials are dissolved / dispersed or melted / dispersed in a solvent, sent to a spray nozzle, and shared with the coating.

【0044】なお、上記説明においては、槽主体4内に
ガイド管6を設けた噴流塔を有する粒体の被覆装置につ
いて説明したが、これに限られない。本発明は、ガイド
管を有していない噴流塔を有する粒体の被覆装置を含む
ものである。この場合も、上記説明は同様に適用され
る。
In the above description, the apparatus for coating a granular material having a jet tower provided with a guide tube 6 in the tank main body 4 has been described, but the present invention is not limited to this. The present invention includes an apparatus for coating a granular material having a jet tower without a guide tube. In this case, the above description is similarly applied.

【0045】更に、本発明粒体の被覆装置は、これをそ
のまま造粒装置として用いることもできるものである。
Further, the granule coating apparatus of the present invention can be used as it is as a granulation apparatus.

【0046】[0046]

【実施例】以下、実施例及び比較例により本発明を具体
的に説明する。
The present invention will be specifically described below with reference to examples and comparative examples.

【0047】1.被覆装置 実施例及び比較例で用いた被覆装置を図1に、また用い
た絞り円盤を図2(実施例)、図4(比較例)に示す。
1. Coating Apparatus The coating apparatus used in Examples and Comparative Examples is shown in FIG. 1, and the drawing disks used are shown in FIGS. 2 (Example) and 4 (Comparative Example).

【0048】被覆装置の噴流塔2の内径は600mm、
高さは5000mmであった。また、ガイド管6は、直
径150mm、長さ880mmのものであった。実施例
に用いた絞り円盤は、直径154mm、噴出孔56の内
径45mm、噴出孔数4個(開口率34%)、各噴出口
56の中央にそれぞれ噴出ノズルを設けたものであっ
た。なお、噴出ノズル26は、絞り円盤の中心を中心と
する直径95mmの円上に配置した。
The inner diameter of the jet tower 2 of the coating apparatus is 600 mm,
The height was 5000 mm. The guide tube 6 had a diameter of 150 mm and a length of 880 mm. The throttle disk used in the example had a diameter of 154 mm, an inner diameter of the ejection hole 56 of 45 mm, the number of ejection holes 4 (opening ratio 34%), and an ejection nozzle provided at the center of each ejection port 56. The ejection nozzle 26 was arranged on a circle having a diameter of 95 mm centered on the center of the drawing disk.

【0049】また、比較例に用いた絞り円盤は、直径1
54mm、噴出口82の内径95mm(開口率38%)
のものであった。
The drawing disk used in the comparative example had a diameter of 1 mm.
54 mm, inner diameter 95 mm of spout 82 (opening ratio 38%)
It was.

【0050】2.被覆方法 ブロアー22を用いて、所定の風量と温度に保持した空
気を噴流塔2に送りながら、所定量の粒体を粒体投入口
36から投入した。次いで塔内の粒体が70℃に達した
ら、被覆液供給ポンプ28を作動させて被覆液調製槽3
2内の被覆液を所定の速度で噴霧ノズル26に所定時間
送って被覆液を噴霧し、所定の被覆率とした後、ブロア
ー22を止めて被覆粒体抜き出し口16より被覆粒体を
抜き出した。
2. Coating Method Using a blower 22, a predetermined amount of particles was injected from the particle input port 36 while sending air maintained at a predetermined air volume and temperature to the jet tower 2. Next, when the temperature of the particles in the tower reaches 70 ° C., the coating liquid supply pump 28 is operated to activate the coating liquid preparation tank 3.
The coating liquid in 2 was sent to the spray nozzle 26 at a predetermined speed for a predetermined time to spray the coating liquid, and the coating rate was adjusted to a predetermined rate. After that, the blower 22 was stopped and the coated particles were extracted from the coated particle extraction port 16. .

【0051】表1は尿素粒体を被覆した際の、被覆装置
の操作条件、及び結果を示すものである。なお、被覆率
は12重量%である。
Table 1 shows the operating conditions and results of the coating apparatus when the urea granules were coated. The coverage is 12% by weight.

【0052】比較例1〜3においては、「溶出率24時
間後」(初期溶出率(%))の値はガス温度、空気流量
の増加と共に著しく増加した。また、「噴流状態」につ
いては脈動が生じ、更に、「塔内の融解・固結の有無」
については、融解・固結があった。
In Comparative Examples 1 to 3, the value of "after 24 hours of dissolution rate" (initial dissolution rate (%)) increased remarkably as the gas temperature and the air flow rate increased. In addition, pulsation occurs in the “jet state”, and furthermore, “the presence or absence of melting and solidification in the tower”
About, there was melting and consolidation.

【0053】これに対し、実施例1〜4においては、ガ
ス温度、空気流量に関係なく「溶出率24時間後」の値
は低いものであった。しかも、「噴流状態」については
脈動が認められず、更に「塔内の融解・固結の有無」に
ついても、融解・固結は皆無であった。
On the other hand, in Examples 1 to 4, the value of "after 24 hours of elution rate" was low regardless of the gas temperature and the air flow rate. In addition, no pulsation was observed in the “jet state”, and no melting / consolidation was observed in “presence of melting / consolidation in the tower”.

【0054】被覆液は下記表2に示す組成よりなる10
0℃の溶液、被覆粒体は表3に示す尿素である。
The coating solution had the composition shown in Table 2 below.
The solution at 0 ° C. and the coated granules are urea shown in Table 3.

【0055】[0055]

【表1】 W:噴流塔への尿素粒子の投入量 Q:噴流用空気の流量 T:絞り部入口のガス温度 u0:絞り円盤の噴出口における空気流速 溶出率24時間後:25℃、24時間経過後の水中(被覆粒体10g、水200 ml)溶出率[Table 1] W: Input amount of urea particles into the jet tower Q: Flow rate of jet air T: Gas temperature at the inlet of the throttle unit u 0 : Air flow rate at the outlet of the throttle disk Elution rate After 24 hours: 25 ° C, After 24 hours Dissolution rate of water in water (coated granules 10g, water 200ml)

【0056】[0056]

【表2】 [Table 2]

【0057】[0057]

【表3】 [Table 3]

【0058】[0058]

【発明の効果】本発明の被覆装置用絞り円盤は、上記の
様に所定数の噴出孔を円盤主体に均一に穿設してあるの
で、絞り円盤上に粒体が堆積して融解固結する事を防止
すると共に、噴流塔内に均一かつ滑らかに噴流気体を噴
出する。このため、装置の運転が安定し、被覆粒体を大
量かつ安定に製造することができる。従って、この装置
を用いて時限溶出型の被覆粒体を製造する場合は、得ら
れる被覆粒体は溶出が安定しており、特に被膜組成によ
って決定される初期溶出抑制期間が安定した被覆粒体を
一度に、大量に製造できる。また、本発明の被覆装置は
槽主体内にガイド管を設けることもでき、この場合には
更に安定した時限溶出型の被覆粒体を簡単に製造でき
る。
As described above, in the drawing disk for a coating apparatus of the present invention, a predetermined number of ejection holes are uniformly formed mainly in the disk as described above, so that particles are deposited on the drawing disk and melted and consolidated. And jetting the jet gas uniformly and smoothly into the jet tower. For this reason, the operation of the apparatus is stable, and a large amount of coated granules can be stably manufactured. Therefore, when time-eluting type coated granules are produced using this apparatus, the obtained coated granules have stable elution, and in particular, have a stable initial elution suppression period determined by the coating composition. Can be manufactured in large quantities at one time. Further, the coating apparatus of the present invention can be provided with a guide tube in the tank main body. In this case, a more stable time-eluting type coated granule can be easily produced.

【0059】更に、本発明装置は、粒体表面にポリオレ
フィン被膜を均質に被覆する必要がある場合であって、
被覆材の溶媒としてポリオレフィン等の貧溶媒を用いる
場合に、特に有効である。
Further, the apparatus of the present invention is applicable to a case where it is necessary to uniformly coat a polyolefin film on the surface of a granular material,
This is particularly effective when a poor solvent such as polyolefin is used as a solvent for the coating material.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の粒体の被覆装置の構成の一例を示す概
略説明図である。
FIG. 1 is a schematic explanatory view showing an example of the configuration of a granule coating device of the present invention.

【図2】本発明の粒体の被覆装置用絞り円盤の一例を示
す拡大平面図である。
FIG. 2 is an enlarged plan view showing an example of a drawing disk for a granule coating device of the present invention.

【図3】本発明の粒体の被覆装置用絞り円盤の他の例を
示す拡大平面図である。
FIG. 3 is an enlarged plan view showing another example of a drawing disk for a particle coating apparatus according to the present invention.

【図4】従来の粒体の被覆装置用絞り円盤の一例を示す
平面図である。
FIG. 4 is a plan view showing an example of a conventional drawing disk for a particle coating apparatus.

【符号の説明】[Explanation of symbols]

2 噴流塔 4 槽主体 6 ガイド管 8 底部 10 絞り部 20 気体加熱器 22 ブロアー 26 噴霧ノズル 32 被覆液調製槽 52 絞り円盤 54 円盤主体 56 噴出孔 60 間隙 2 Jet Tower 4 Tank Main Body 6 Guide Tube 8 Bottom 10 Throttle Section 20 Gas Heater 22 Blower 26 Spray Nozzle 32 Coating Liquid Preparation Tank 52 Throttle Disk 54 Disk Main Body 56 Spouting Hole 60 Gap

Claims (4)

【特許請求の範囲】[Claims] 【請求項1】 所定数の噴出孔を均一に円盤主体に穿設
してなり、その開口率が10〜70%である粒体の被覆
装置用絞り円盤であって、前記絞り円盤の噴出孔の少な
くとも1個に被覆液噴霧ノズルを挿入して噴流塔の下部
に取り付けられ、噴流塔の下部から前記噴出孔を通して
噴流塔内に気体を噴出させて前記噴流塔内に粒体の噴流
層を形成すると共に、前記噴流層を形成する粒体に前記
ノズルから被覆液を噴霧して前記粒体を被膜で被覆する
粒体の被覆装置の噴流塔の下部に取付けて気体を噴流塔
内に噴出させることを特徴とする粒体の被覆装置用絞り
円盤。
1. A drawing disk for a coating apparatus for a granular material, wherein a predetermined number of ejection holes are uniformly formed mainly in a disk, and the opening ratio of the ejection holes is 10 to 70%. The coating liquid spray nozzle is inserted into at least one of the jet towers and attached to the lower part of the spout tower. Gas is jetted from the lower part of the spout tower through the jet hole into the spout tower to form a spouted layer of granular material in the spout tower. At the same time, the coating liquid is sprayed from the nozzle onto the granules forming the spouted bed and the granules are coated with a coating film. A squeezing disk for a coating apparatus for granular material, characterized in that the squeezing disk is used.
【請求項2】 請求項1に記載の絞り円盤が取り付けら
れていることを特徴とする粒体の被覆装置。
2. A granule coating apparatus to which the drawing disk according to claim 1 is attached.
【請求項3】 噴流塔内にその軸方向を垂直に取り付け
られたガイド管を有する請求項2に記載の粒体の被覆装
置。
3. The apparatus for coating granules according to claim 2, further comprising a guide pipe which is vertically mounted in the jet tower.
【請求項4】 所定数の噴出孔を均一に円盤主体に穿設
してなり、その開口率が10〜70%である絞り円盤を
噴流塔の下部に取り付けると共に、前記絞り円盤の噴出
孔の少なくとも1個に噴霧ノズルを挿入し、前記噴霧ノ
ズルの上方であって前記噴流塔内に垂直にガイド管を設
けてなる噴流塔を有する粒体の被覆装置を用い、前記絞
り円盤の噴出孔を通して噴流塔内に気体を噴出させて前
記噴流塔内に粒体の噴流層を形成すると共に、前記噴流
層を形成する粒体に噴霧ノズルから被覆液を噴霧して前
記粒体を被膜で被覆することを特徴とする粒体の被覆方
法。
4. A predetermined number of ejection holes are uniformly drilled mainly in a disk, and a throttle disk having an opening ratio of 10 to 70% is attached to a lower portion of the jet tower, and a discharge hole of the throttle disk is formed. Insert a spray nozzle into at least one of the spray nozzles, and use a granule coating device having a jet tower provided with a guide tube vertically above the spray nozzle and inside the jet tower, and passing through the jet hole of the throttle disk A gas is blown into the spout tower to form a spouted layer of particles in the spout tower, and the particles forming the spouted bed are sprayed with a coating liquid from a spray nozzle to coat the granules with a coating. A method for coating granules, characterized in that:
JP15395598A 1998-05-19 1998-05-19 Squeezing disk for granule coating apparatus, granule coating apparatus having the disc, and granule coating method Expired - Lifetime JP3921813B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP15395598A JP3921813B2 (en) 1998-05-19 1998-05-19 Squeezing disk for granule coating apparatus, granule coating apparatus having the disc, and granule coating method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP15395598A JP3921813B2 (en) 1998-05-19 1998-05-19 Squeezing disk for granule coating apparatus, granule coating apparatus having the disc, and granule coating method

Publications (2)

Publication Number Publication Date
JPH11319535A true JPH11319535A (en) 1999-11-24
JP3921813B2 JP3921813B2 (en) 2007-05-30

Family

ID=15573733

Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Status (1)

Country Link
JP (1) JP3921813B2 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006111521A (en) * 2004-09-14 2006-04-27 Chisso Corp Coated granular fertilizer and method of manufacturing the same
US8197729B2 (en) 2007-10-30 2012-06-12 Toyo Engineering Corporation Method of granulation with a fluidized bed granulator

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006111521A (en) * 2004-09-14 2006-04-27 Chisso Corp Coated granular fertilizer and method of manufacturing the same
US8197729B2 (en) 2007-10-30 2012-06-12 Toyo Engineering Corporation Method of granulation with a fluidized bed granulator
US8834142B2 (en) 2007-10-30 2014-09-16 Toyo Engineering Corporation Fluidized bed granulator

Also Published As

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