JPH0473419B2 - - Google Patents
Info
- Publication number
- JPH0473419B2 JPH0473419B2 JP7627785A JP7627785A JPH0473419B2 JP H0473419 B2 JPH0473419 B2 JP H0473419B2 JP 7627785 A JP7627785 A JP 7627785A JP 7627785 A JP7627785 A JP 7627785A JP H0473419 B2 JPH0473419 B2 JP H0473419B2
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- reactor
- ethane
- liquid
- dichloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000006243 chemical reaction Methods 0.000 claims description 55
- 239000007788 liquid Substances 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 24
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 claims description 22
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 22
- 239000005977 Ethylene Substances 0.000 claims description 21
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 20
- 239000012429 reaction media Substances 0.000 claims description 19
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 17
- 239000000460 chlorine Substances 0.000 claims description 16
- 229910052801 chlorine Inorganic materials 0.000 claims description 16
- 239000000047 product Substances 0.000 claims description 9
- 125000001931 aliphatic group Chemical group 0.000 claims description 8
- 229930195735 unsaturated hydrocarbon Natural products 0.000 claims description 8
- MXWRJMIKMODSCY-UHFFFAOYSA-N ethane;dihydrochloride Chemical compound Cl.Cl.CC MXWRJMIKMODSCY-UHFFFAOYSA-N 0.000 claims description 7
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 claims description 6
- 229950011008 tetrachloroethylene Drugs 0.000 claims description 6
- 239000006227 byproduct Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- RWNKSTSCBHKHTB-UHFFFAOYSA-N Hexachloro-1,3-butadiene Chemical compound ClC(Cl)=C(Cl)C(Cl)=C(Cl)Cl RWNKSTSCBHKHTB-UHFFFAOYSA-N 0.000 description 26
- UBOXGVDOUJQMTN-UHFFFAOYSA-N 1,1,2-trichloroethane Chemical compound ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 24
- 238000007086 side reaction Methods 0.000 description 19
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 18
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 10
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 10
- 239000007795 chemical reaction product Substances 0.000 description 9
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 8
- 238000004821 distillation Methods 0.000 description 8
- 229960003750 ethyl chloride Drugs 0.000 description 8
- 239000000126 substance Substances 0.000 description 7
- 238000009835 boiling Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000012535 impurity Substances 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 238000004817 gas chromatography Methods 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 230000002401 inhibitory effect Effects 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 238000000746 purification Methods 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000012295 chemical reaction liquid Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 230000008016 vaporization Effects 0.000 description 2
- JLYXXMFPNIAWKQ-UHFFFAOYSA-N γ Benzene hexachloride Chemical compound ClC1C(Cl)C(Cl)C(Cl)C(Cl)C1Cl JLYXXMFPNIAWKQ-UHFFFAOYSA-N 0.000 description 2
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001555 benzenes Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002683 reaction inhibitor Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000007039 two-step reaction Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7627785A JPS61233638A (ja) | 1985-04-09 | 1985-04-09 | 二塩化エタンの製造方法 |
| DE19863604968 DE3604968A1 (de) | 1985-02-19 | 1986-02-17 | Verfahren zur herstellung von dichlorethan |
| US07/338,538 US4873384A (en) | 1985-02-19 | 1989-04-14 | Method for producing dichloroethane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7627785A JPS61233638A (ja) | 1985-04-09 | 1985-04-09 | 二塩化エタンの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61233638A JPS61233638A (ja) | 1986-10-17 |
| JPH0473419B2 true JPH0473419B2 (de) | 1992-11-20 |
Family
ID=13600774
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7627785A Granted JPS61233638A (ja) | 1985-02-19 | 1985-04-09 | 二塩化エタンの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61233638A (de) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1057992C (zh) * | 1995-03-30 | 2000-11-01 | 株式会社德山 | 多氯甲烷的制造方法 |
-
1985
- 1985-04-09 JP JP7627785A patent/JPS61233638A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS61233638A (ja) | 1986-10-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2102379C1 (ru) | Способ получения уксусной кислоты | |
| RU2397157C2 (ru) | Утилизация тепла реакции уксусной кислоты в других технологических установках | |
| WO2014163500A1 (en) | Process for the preparation of 2,5-furan-dicarboxylic acid | |
| JPS5914255B2 (ja) | オレフインのカルボニル化法 | |
| US5292917A (en) | Process for purifying dimethyl carbonate | |
| EP1024125B1 (de) | Verfahren zur herstellung von 1,1,1,2,2-pentafluoroethan | |
| US4873384A (en) | Method for producing dichloroethane | |
| CS198231B2 (en) | Method of the partial separation of water from gas mixture arising in vinyl acetate preparation | |
| US4759826A (en) | Process for purifying thionyl chloride | |
| JP6693959B2 (ja) | 酢酸の製造方法 | |
| US4496760A (en) | Process of decomposition of a complex of ortho-benzoyl benzoic acid, hydrogen fluoride and boron trifluoride | |
| JPH0819014B2 (ja) | 二塩化エタンの製造方法 | |
| US4794204A (en) | Process for the removal of dimethyl ether in methyl chloride | |
| US2461988A (en) | Hydrogen peroxide distillation after removal of organic peroxides | |
| JPH0473419B2 (de) | ||
| EP0501374A1 (de) | Verfahren zur Reinigung von Dimethylcarbonat | |
| JPH0147454B2 (de) | ||
| US4018880A (en) | Method of purifying hydrogen chloride gas | |
| Peters et al. | Methacrylonitrile and acrylonitrile | |
| US4774372A (en) | Method for producing dichloroethane | |
| NO744466L (de) | ||
| JPS5941924B2 (ja) | 塩化チオニルの精製法 | |
| JP3682805B2 (ja) | 飽和脂肪族カルボン酸アミドの製造方法 | |
| JPH04227853A (ja) | 触媒系及びこの触媒系の使用下におけるエチレンの塩化による１，２−ジクロロエタンの製法 | |
| US3354054A (en) | Process for isolating and purifying 1-cyanobutadiene-(1, 3) by plural stage distillation in the presence of nitrogen oxide |