JPH04243802A - Noxious insect attracting agent - Google Patents

Noxious insect attracting agent

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Publication number
JPH04243802A
JPH04243802A JP2528691A JP2528691A JPH04243802A JP H04243802 A JPH04243802 A JP H04243802A JP 2528691 A JP2528691 A JP 2528691A JP 2528691 A JP2528691 A JP 2528691A JP H04243802 A JPH04243802 A JP H04243802A
Authority
JP
Japan
Prior art keywords
hexadecenal
attractant
trap
pests
present
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2528691A
Other languages
Japanese (ja)
Other versions
JP2915157B2 (en
Inventor
Kenji Komori
研二 古森
Yasuo Ninomiya
保男 二宮
Giichi Musa
義一 撫佐
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nitto Denko Corp
Original Assignee
Nitto Denko Corp
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Filing date
Publication date
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Abstract

PURPOSE:To obtain a noxious insect capable of exhibiting excellent attractive effect to Parapediasia teterrella and Spodoptera depravata which are noxious insects of Gramineae plant. CONSTITUTION:(11Z)-Hexadecenal and (9Z)-hexadecenal are used as active ingredients to Parapediasia teterrella and (9Z,12E)-tetradecadienyl acetate is used as an active ingredient to Spodoptera depravata and the above-mentioned compounds are used in combination in order to simultaneously attract both noxious insects to provide a excellent attracting agent.

Description

【発明の詳細な説明】[Detailed description of the invention]

【0001】0001

【産業上の利用分野】本発明はイネ科植物の害虫として
のシバツトガおよびスジキリヨトウに対して優れた誘引
効果を発揮する誘引剤に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an attractant that exhibits an excellent attracting effect on grass moths and cutworms as insect pests of grasses.

【0002】0002

【従来の技術】イネ科植物の害虫としてのシバツトガや
スジキリヨトウは、特に芝害虫として近年重要視されて
いる。シバツトガ(学名:Parapediasia 
 teterrella (Zincken), 慣用
名:Bluegrass webworm)は、植物や
土粒をつづって巣を作り、その中の幼虫が芝草を食害す
る害虫である。このシバツトガによる被害は北海道や東
北ではあまり起こっていないが、関東以西の平野部では
毎年シバツトガの発生し、1968年以降、わが国のゴ
ルフ場の芝草地で多大な被害が生じている。
BACKGROUND OF THE INVENTION In recent years, grass moths and cutworms have become particularly important as grass pests. Shibatsutoga (scientific name: Parapediasia)
Zincken (common name: Bluegrass webworm) is a pest that builds nests out of plants and soil grains, and the larvae inside the nests damage turfgrass. Although damage caused by Shibatsutomo does not occur much in Hokkaido and Tohoku, it occurs every year in the plains west of the Kanto region, and since 1968, it has caused extensive damage to the lawns of golf courses in Japan.

【0003】シバツトガは年3回発生して成虫は夜行性
である。幼虫は新芽の柔らかい部分を食害すると共に、
吐糸で枯れ葉や砂粒などをつづって巣を作りその中で生
息する。幼虫は極めて早く成長するので芝草の被害も急
速に進行し、被害が出始めてからでの防除では被害を食
い止めることができず、成虫の発生量に注意して事前に
防除する必要がある。
[0003] Shibatsutoga occurs three times a year, and the adults are nocturnal. The larvae feed on the soft parts of the new shoots, and
They make their nests by spinning dead leaves, sand grains, etc. with spun silk, and live inside them. Since the larvae grow extremely quickly, the damage to turf grass progresses rapidly, and it is not possible to stop the damage by controlling it after the damage has started, so it is necessary to control the number of adult insects in advance.

【0004】一方、スジキリヨトウ(学名:Spodo
ptera  depravata  (Butler
),慣用名:Lawn grass cutworm)
 は、春期に樹木の根部や芝草地をスポット状に荒らす
ので、初期には病斑と間違われる。この時期に気が付か
ないと夏期から秋期にかけて芝草地全域に被害が及び、
青々とした芝草の中に大面積の枯れ部が目立つようにな
る。スジキリヨトウの被害部分が地中であること、成虫
は夜行性であること、発生が年3回と多いことから、ゴ
ルフ場ような広い面積の芝草地を管理するところでは、
その被害はわからない間に進行して大きな被害に及ぶ結
果となる。特に、ゴルフ場ではラフでのスジキリヨトウ
の発生に気付かず、ラフの荒廃の大きな原因となる場合
が多く、また、これが芝草地における発生源となるとい
う悪循環を生じている。
On the other hand, Spodo (scientific name: Spodo)
ptera depravata (Butler
), common name: Lawn grass cutworm)
In the spring, it damages the roots of trees and grasslands in spots, so it can be mistaken for lesions in the early stages. If you are not careful during this period, damage will occur to the entire lawn from summer to autumn.
Large areas of dead grass become noticeable among the lush grass. Because the damage caused by striped armyworm is underground, the adults are nocturnal, and the insects often appear three times a year, it is difficult to manage large areas of grassland such as golf courses.
The damage progresses unnoticed and results in major damage. In particular, on golf courses, the occurrence of striped armyworm on the rough is often not noticed, which is a major cause of the deterioration of the rough, and this also becomes a source of infestation on grassy areas, creating a vicious cycle.

【0005】前記シバツトガやスジキリヨトウは成虫や
卵に対する薬剤散布はあまり効果がないので、幼虫に対
してオルトラン水和剤やガードサイド水和剤、サリチオ
ンやEPN、トクチオン、ダイアジノン、スミチオンな
どの各乳剤を散布する方法が採用されている。
[0005] Spraying chemicals on the adults and eggs of the above-mentioned Shibatsutomo and Sujikiri armyworm is not very effective, so various emulsions such as Ortolan hydrating agent, Guardside hydrating agent, Salithion, EPN, Toction, Diazinon, Sumithion, etc. are applied to the larvae. A scattering method is used.

【0006】[0006]

【発明が解決しようとする課題】しかしながら、これら
の害虫は年に3回発生すること、発生の時期が常に一定
ではないこと、殺虫剤の散布では有効成分が分解しやす
いので長期間にわたって殺虫効果を維持することが困難
であること、防除対象の幼虫が地中に生息しているので
殺虫剤が効率的に効かないことなどの問題がある。従っ
て、防除効果を高めるには殺虫剤の散布回数を多くする
必要があるが、発生予察が困難であるので正確な防除時
期を把握できず、多額の費用を伴うにもかかわらず効率
のよい防除効果が期待できないという問題がある。また
、殺虫剤を連続して散布すると耐性を生じたり、環境汚
染の問題もある。従って、本発明は上記シバツトガやス
ジキリヨトウの発生消長の調査、あるいは大量の雄成虫
の誘殺のような防除を効果的に行いうる誘引剤を提供す
ることを目的とする。
[Problems to be solved by the invention] However, these pests occur three times a year, the timing of their occurrence is not always constant, and when spraying insecticides, the active ingredient easily decomposes, so the insecticidal effect does not last for a long time. Problems include that it is difficult to maintain insecticides, and that insecticides are not effective because the larvae to be controlled live underground. Therefore, in order to increase the pest control effect, it is necessary to increase the number of times insecticides are sprayed, but since it is difficult to predict the occurrence of insecticides, it is not possible to determine the exact time of pest control, and efficient pest control is not possible despite the high cost. The problem is that the effects cannot be expected. Continuous spraying of insecticides also causes resistance and environmental pollution problems. Therefore, an object of the present invention is to provide an attractant that can effectively investigate the development and development of the above-mentioned Shibatsuto moth and Sujikiri armyworm, or control them by attracting and killing a large number of male adults.

【0007】[0007]

【課題を解決するための手段】そこで、本発明者らは上
記目的を達成するために鋭意検討を重ねた結果、誘引剤
として見い出した特定の化合物を用いて上記害虫を誘引
すると、困難であったこれらの害虫の発生予察が的確に
行えるので防除時期が把握でき、その結果、従来から使
用している殺虫剤を用いても効率よく防除できることが
判明した。さらに、一般的には異なる誘引剤を併用する
と、互いに誘引作用に影響を及ぼし、単独で使用した場
合のような誘引効果を充分に発揮できないと云われてい
るが、本発明では驚くべきことにシバツトガ用の誘引剤
とスジキリヨトウ用の誘引剤を併用してもこのような効
果の減少は生じず、これら二種類の害虫を同時に誘引す
ることができることを見い出した。
[Means for Solving the Problems] The present inventors have conducted intensive studies to achieve the above object, and have found that it is difficult to attract the above pests using a specific compound as an attractant. Since the occurrence of these pests can be accurately predicted, it is possible to know when to control them, and as a result, it has been found that they can be efficiently controlled even with conventionally used insecticides. Furthermore, it is generally said that when different attractants are used in combination, they affect the attracting effects of each other and cannot exhibit the attracting effect as much as when used alone; however, the present invention surprisingly provides It has been found that such a decrease in effectiveness does not occur even when an attractant for Shibatsuto moth and an attractant for striped armyworm are used in combination, and these two types of pests can be attracted at the same time.

【0008】即ち、本発明は(11Z)−ヘキサデセナ
ールおよび(9Z)−ヘキサデセナールを有効成分とす
るシバツトガ用の害虫誘引剤を第1の発明とし、(9Z
,12E)−テトラデカジエニルアセテートを有効成分
とするスジキリヨトウ用の害虫誘引剤を第2の発明、(
11Z)−ヘキサデセナールおよび(9Z)−ヘキサデ
セナール並びに(9Z,12E)−テトラデカジエニル
アセテートを有効成分とするシバツトガおよびスジキリ
ヨトウを同時誘引可能な害虫誘引剤を第3の発明として
提供するものである。
[0008] That is, the present invention provides a first invention of an insect pest attractant for snail moth containing (11Z)-hexadecenal and (9Z)-hexadecenal as active ingredients;
, 12E)-Tetradecadienyl acetate is the second invention, (
A third aspect of the present invention provides a pest attractant capable of simultaneously attracting grasshopper moths and cutworms, which contains 11Z)-hexadecenal, (9Z)-hexadecenal, and (9Z,12E)-tetradecadienyl acetate as active ingredients.

【0009】本発明の害虫誘引剤に用いる化合物は、誘
引効果のある化合物を探索した結果、見い出したもので
あって、シバツトガに対しては(11Z)−ヘキサデセ
ナールおよび(9Z)−ヘキサデセナールとの混合物が
有効であり、スジキリヨトウに対しては(9Z,12E
)−テトラデカジエニルアセテートが有効であり、また
両害虫にはこれらの化合物を混合することによって誘引
効果を発揮する。
[0009] The compound used in the pest attractant of the present invention was discovered as a result of searching for a compound that has an attracting effect, and for Shibatsuto moth, a mixture of (11Z)-hexadecenal and (9Z)-hexadecenal is used. is effective, and against striped armyworm (9Z, 12E)
)-tetradecadienyl acetate is effective, and a mixture of these compounds exhibits an attractive effect on both pests.

【0010】シバツトガに対して誘引効果を発揮する上
記混合物は、その混合比率((11Z)−ヘキサデセナ
ール/(9Z)−ヘキサデセナール)を100/1〜1
/1、好ましくは50/1〜5/1とすることによって
優れた誘引効果を示す。
[0010] The above-mentioned mixture exhibiting an attracting effect on Shibatsutomo has a mixing ratio ((11Z)-hexadecenal/(9Z)-hexadecenal) of 100/1 to 1.
/1, preferably 50/1 to 5/1, exhibits an excellent attracting effect.

【0011】本発明の誘引剤における上記有効成分は、
そのままで誘引剤として使用したり、例えばアセトンや
ジクロロメタンなどの任意の希釈溶剤にて希釈して使用
することができる。また、これらの誘引剤はそのまま用
いてもよいが、綿棒やプラスチック製材料、ゴム製材料
などからなる任意形状の担持体に含浸や吸着などの手段
にて担持させて製剤化して用いることができる。本発明
の誘引剤の使用量は使用環境に応じて適宜決定すること
ができるが、通常、製剤当たりシバツトガの誘引におい
ては(11Z)−ヘキサデセナールと(9Z)−ヘキサ
デセナールとの混合物を0.05〜10mg、好ましく
は0.1〜5mg程度、スジキリヨトウの誘引において
は(9Z,12E)−テトラデカジエニルアセテートを
0.05〜10mg、好ましくは0.1〜5mg程度、
両害虫の誘引においては上記単独誘引の際に用いる使用
量の合計量程度とする。
[0011] The above-mentioned active ingredients in the attractant of the present invention are:
It can be used as an attractant as it is, or diluted with any diluting solvent such as acetone or dichloromethane. In addition, these attractants may be used as they are, but they can also be formulated into a formulation by being supported on a carrier of any shape such as a cotton swab, plastic material, rubber material, etc. by means such as impregnation or adsorption. . The amount of the attractant of the present invention to be used can be appropriately determined depending on the usage environment, but usually, in order to attract Shibatsuto moth per preparation, a mixture of (11Z)-hexadecenal and (9Z)-hexadecenal is used at a concentration of 0.05 to 10 mg, preferably about 0.1 to 5 mg, and for attracting striped armyworm, about 0.05 to 10 mg, preferably about 0.1 to 5 mg, of (9Z,12E)-tetradecadienyl acetate.
When attracting both types of pests, the amount used should be approximately the total amount used when attracting the above individual pests.

【0012】本発明の害虫誘引剤は捕獲容器に配設する
ことによって、誘引された害虫を捕獲することもでき、
また容器内に水をいれ捕獲害虫を殺虫することもできる
ものである。また、従来から用いられている殺虫剤と本
発明の誘引剤とを併用することによって、防除効果を向
上させることもできる。
[0012] The pest attractant of the present invention can also be placed in a trap container to capture the attracted pests.
It is also possible to kill captured pests by filling the container with water. Moreover, the pesticidal effect can be improved by using a conventionally used insecticide and the attractant of the present invention together.

【0013】[0013]

【実施例】以下に実施例を示し、本発明の害虫誘引剤の
誘引効果について具体的に説明する。
[Examples] Examples are shown below to specifically explain the attracting effect of the pest attractant of the present invention.

【0014】実施例1 支持板の上面に粘着剤層を積層した粘着式トラップの中
央部に、(11Z)−ヘキサデセナール2.9mgと(
9Z)−ヘキサデセナール0.1mgとの混合物を含浸
させたゴム製材料からなるキャップ状担持体を設置して
誘引トラップを作製した。
Example 1 2.9 mg of (11Z)-hexadecenal and (
An attraction trap was prepared by installing a cap-shaped carrier made of a rubber material impregnated with a mixture of 0.1 mg of 9Z)-hexadecenal.

【0015】実施例2 実施例1において誘引剤を(11Z)−ヘキサデセナー
ル1.1mgと(9Z)−ヘキサデセナール0.09m
gとの混合物とした以外は、実施例1と同様にして誘引
トラップを作製した。
Example 2 In Example 1, the attractants were (11Z)-hexadecenal 1.1 mg and (9Z)-hexadecenal 0.09 m
An attraction trap was produced in the same manner as in Example 1, except that the mixture was mixed with g.

【0016】実施例3 実施例1において誘引剤を(11Z)−ヘキサデセナー
ル0.99mgと(9Z)−ヘキサデセナール0.02
mgとの混合物とした以外は、実施例1と同様にして誘
引トラップを作製した。
Example 3 In Example 1, the attractants were (11Z)-hexadecenal 0.99 mg and (9Z)-hexadecenal 0.02 mg.
An attraction trap was produced in the same manner as in Example 1, except that the mixture was mixed with mg.

【0017】比較例1 実施例1において誘引剤を(11Z)−ヘキサデセナー
ル2mgとした以外は、実施例1と同様にして誘引トラ
ップを作製した。
Comparative Example 1 An attraction trap was prepared in the same manner as in Example 1 except that 2 mg of (11Z)-hexadecenal was used as the attractant.

【0018】比較例2 実施例1において誘引剤を(9Z)−ヘキサデセナール
2mgとした以外は、実施例1と同様にして誘引トラッ
プを作製した。
Comparative Example 2 An attraction trap was prepared in the same manner as in Example 1 except that 2 mg of (9Z)-hexadecenal was used as the attractant.

【0019】対照例1 実施例1において本発明の誘引剤を用いずに粘着式トラ
ップのみを用意した。
Comparative Example 1 In Example 1, only an adhesive trap was prepared without using the attractant of the present invention.

【0020】上記各実施例、比較例、対照例にて作製し
たトラップを、9月期にそれぞれ一個ずつゴルフ場の芝
草地帯(約25アール)に、各トラップ間を50m以上
あけて日没前に配置した。翌日、各トラップを回収して
1日で誘引捕獲されたシバツトガの全数を調べるという
操作を実施日を異なえて3回行い、その結果を表1に示
した。
[0020] The traps prepared in each of the above Examples, Comparative Examples, and Control Examples were placed in the grass area (approximately 25 ares) of a golf course in September, with a gap of 50 m or more between each trap, before sunset. It was placed in The next day, each trap was collected and the total number of Shibatsuto moths attracted and captured in one day was determined three times on different days, and the results are shown in Table 1.

【0021】[0021]

【表1】[Table 1]

【0022】実施例4 実施例1にて用いた粘着式トラップの中央部に、(9Z
,12E)−テトラデカジエニルアセテート1mgとの
混合物を含浸させたゴム製材料からなるキャップ状担持
体を設置し誘引トラップを作製した。
Example 4 In the center of the adhesive trap used in Example 1, (9Z
, 12E) - A cap-shaped carrier made of a rubber material impregnated with a mixture of 1 mg of tetradecadienyl acetate was installed to prepare an attraction trap.

【0023】対照例2 実施例4において本発明の誘引剤を用いずに粘着式トラ
ップのみを用意した。
Comparative Example 2 In Example 4, only an adhesive trap was prepared without using the attractant of the present invention.

【0024】上記実施例4および対照例2にて作製した
トラップを、9月期にそれぞれ一個ずつゴルフ場の芝草
地帯(約25アール)に、各トラップ間を50m以上あ
けて日没前に配置した。翌日、各トラップを回収して1
日で誘引捕獲されたスジキリヨトウの全数を調べるとい
う操作を実施日を異なえて3回行い、その結果を表2に
示した。
[0024] The traps prepared in Example 4 and Comparative Example 2 were placed one each in the grass area (approximately 25 ares) of a golf course in September with a gap of 50 m or more between each trap before sunset. did. The next day, collect each trap and
The operation of examining the total number of striped armyworms attracted and captured on a given day was carried out three times on different days, and the results are shown in Table 2.

【0025】[0025]

【表2】[Table 2]

【0026】実施例5 実施例1にて用いた粘着式トラップの中央部に、(11
Z)−ヘキサデセナール2.9mg、(9Z)−ヘキサ
デセナール0.1mgの混合物を含浸させたゴム製材料
からなるキャップ状担持体と、(9Z,12E)−テト
ラデカジエニルアセテート1mgを含浸させたゴム製材
料からなるキャップ状担持体をそれぞれ1個ずつ併置し
、誘引トラップを作製した。
Example 5 In the center of the adhesive trap used in Example 1, (11
A cap-shaped carrier made of a rubber material impregnated with a mixture of 2.9 mg of Z)-hexadecenal and 0.1 mg of (9Z)-hexadecenal, and a rubber impregnated with 1 mg of (9Z,12E)-tetradecadienyl acetate. Attraction traps were fabricated by placing cap-shaped carriers made of raw materials in parallel.

【0027】対照例3 実施例5において本発明の誘引剤を用いずに粘着式トラ
ップのみを用意した。
Comparative Example 3 In Example 5, only an adhesive trap was prepared without using the attractant of the present invention.

【0028】上記実施例5および対照例3にて作製した
トラップを、9月期にそれぞれ一個ずつゴルフ場の芝草
地帯(約25アール)に、各トラップ間を50m以上あ
けて日没前に配置した。翌日、各トラップを回収して1
日で誘引捕獲されたスジキリヨトウの全数を調べるとい
う操作を実施日を異なえて3回行い、その結果を表3に
示した。
[0028] The traps prepared in Example 5 and Comparative Example 3 were placed one each in the grass area (approximately 25 ares) of a golf course in September, with a gap of 50 m or more between each trap, before sunset. did. The next day, collect each trap and
The operation of checking the total number of striped armyworms attracted and captured on a given day was carried out three times on different days, and the results are shown in Table 3.

【0029】[0029]

【表3】 A:シバツトガ,  B:スジキリヨトウ[Table 3] A: Shibatsutoga, B: Sujikiriyotou

【0030】[0030]

【発明の効果】本発明の害虫誘引剤は上記のように、シ
バツトガやスジキリヨトウに対して優れた誘引効果を有
するので、害虫の発生予察が容易に行え、殺虫剤による
防除を有効に行なえると共に、捕獲容器と組み合わせる
ことによってこれらの害虫を誘引・捕獲することもでき
るものである。さらに、本発明によれば害虫としてのシ
バツトガとスジキリヨトウとを同時に防除することがで
きるという効果も発揮するものである。
[Effects of the Invention] As mentioned above, the pest attractant of the present invention has an excellent attracting effect on Shibatsuto moth and Sujikiri armyworm, so it is easy to predict the occurrence of pests, and it is possible to effectively control pests using insecticides. It is also possible to attract and capture these pests by combining it with a trapping container. Further, according to the present invention, it is possible to simultaneously control the insect pests such as the staghorn moth and the cutworm.

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】  (11Z)−ヘキサデセナールおよび
(9Z)−ヘキサデセナールを有効成分とするシバツト
ガ用の害虫誘引剤。
Claim: 1. A pest attractant for Shibatsuto moth containing (11Z)-hexadecenal and (9Z)-hexadecenal as active ingredients.
【請求項2】  (9Z,12E)−テトラデカジエニ
ルアセテートを有効成分とするスジキリヨトウ用の害虫
誘引剤。
2. An insect attractant for cutworms containing (9Z,12E)-tetradecadienyl acetate as an active ingredient.
【請求項3】  (11Z)−ヘキサデセナールおよび
(9Z)−ヘキサデセナール並びに(9Z,12E)−
テトラデカジエニルアセテートを有効成分とするシバツ
トガおよびスジキリヨトウを同時誘引可能な害虫誘引剤
Claim 3: (11Z)-hexadecenal and (9Z)-hexadecenal and (9Z,12E)-
A pest attractant that contains tetradecadienyl acetate as an active ingredient and can simultaneously attract Shibattutomoth and Sparrowworm.
JP2528691A 1991-01-25 1991-01-25 Pest attractant Expired - Lifetime JP2915157B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2528691A JP2915157B2 (en) 1991-01-25 1991-01-25 Pest attractant

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2528691A JP2915157B2 (en) 1991-01-25 1991-01-25 Pest attractant

Publications (2)

Publication Number Publication Date
JPH04243802A true JPH04243802A (en) 1992-08-31
JP2915157B2 JP2915157B2 (en) 1999-07-05

Family

ID=12161779

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2528691A Expired - Lifetime JP2915157B2 (en) 1991-01-25 1991-01-25 Pest attractant

Country Status (1)

Country Link
JP (1) JP2915157B2 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005047889A (en) * 2003-07-14 2005-02-24 Shin Etsu Chem Co Ltd Method for predicting occurrence of trigonotylus caelestialium
KR100982244B1 (en) * 2009-12-24 2010-09-14 다연산업 주식회사 Brushing apparatus for liverstock
US8900611B2 (en) * 2004-09-15 2014-12-02 Shin-Etsu Chemical Co., Ltd. Sustained releaser comprising sex pheromone substances

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005047889A (en) * 2003-07-14 2005-02-24 Shin Etsu Chem Co Ltd Method for predicting occurrence of trigonotylus caelestialium
US8900611B2 (en) * 2004-09-15 2014-12-02 Shin-Etsu Chemical Co., Ltd. Sustained releaser comprising sex pheromone substances
KR100982244B1 (en) * 2009-12-24 2010-09-14 다연산업 주식회사 Brushing apparatus for liverstock

Also Published As

Publication number Publication date
JP2915157B2 (en) 1999-07-05

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