JPH0364534B2 - - Google Patents
Info
- Publication number
- JPH0364534B2 JPH0364534B2 JP20346585A JP20346585A JPH0364534B2 JP H0364534 B2 JPH0364534 B2 JP H0364534B2 JP 20346585 A JP20346585 A JP 20346585A JP 20346585 A JP20346585 A JP 20346585A JP H0364534 B2 JPH0364534 B2 JP H0364534B2
- Authority
- JP
- Japan
- Prior art keywords
- tank
- polyester
- stirring roller
- stirring
- wall
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000003756 stirring Methods 0.000 claims description 49
- 229920000642 polymer Polymers 0.000 claims description 30
- 238000006116 polymerization reaction Methods 0.000 claims description 29
- 238000006243 chemical reaction Methods 0.000 claims description 23
- 229920000728 polyester Polymers 0.000 claims description 23
- 239000010409 thin film Substances 0.000 claims description 17
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 239000000178 monomer Substances 0.000 claims description 6
- 238000010008 shearing Methods 0.000 claims description 4
- 230000002093 peripheral effect Effects 0.000 claims 1
- 238000000034 method Methods 0.000 description 20
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 17
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 12
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 8
- 239000012295 chemical reaction liquid Substances 0.000 description 8
- -1 polyethylene terephthalate Polymers 0.000 description 8
- 230000007246 mechanism Effects 0.000 description 7
- 239000000047 product Substances 0.000 description 5
- 230000036632 reaction speed Effects 0.000 description 5
- 238000007789 sealing Methods 0.000 description 5
- 238000005809 transesterification reaction Methods 0.000 description 5
- 229920000139 polyethylene terephthalate Polymers 0.000 description 4
- 239000005020 polyethylene terephthalate Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000010408 film Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 238000007790 scraping Methods 0.000 description 2
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
- ISPYQTSUDJAMAB-UHFFFAOYSA-N 2-chlorophenol Chemical compound OC1=CC=CC=C1Cl ISPYQTSUDJAMAB-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000001361 adipic acid Substances 0.000 description 1
- 235000011037 adipic acid Nutrition 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 150000002009 diols Chemical class 0.000 description 1
- 239000004815 dispersion polymer Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 238000009775 high-speed stirring Methods 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 150000002681 magnesium compounds Chemical class 0.000 description 1
- 229940071125 manganese acetate Drugs 0.000 description 1
- 150000002697 manganese compounds Chemical class 0.000 description 1
- UOGMEBQRZBEZQT-UHFFFAOYSA-L manganese(2+);diacetate Chemical compound [Mn+2].CC([O-])=O.CC([O-])=O UOGMEBQRZBEZQT-UHFFFAOYSA-L 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- KYTZHLUVELPASH-UHFFFAOYSA-N naphthalene-1,2-dicarboxylic acid Chemical compound C1=CC=CC2=C(C(O)=O)C(C(=O)O)=CC=C21 KYTZHLUVELPASH-UHFFFAOYSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000002685 polymerization catalyst Substances 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- YGSDEFSMJLZEOE-UHFFFAOYSA-M salicylate Chemical compound OC1=CC=CC=C1C([O-])=O YGSDEFSMJLZEOE-UHFFFAOYSA-M 0.000 description 1
- 229960001860 salicylate Drugs 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004246 zinc acetate Substances 0.000 description 1
- 150000003752 zinc compounds Chemical class 0.000 description 1
Landscapes
- Polyesters Or Polycarbonates (AREA)
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP20346585A JPS6264822A (ja) | 1985-09-17 | 1985-09-17 | ポリエステルの製造方法および装置 |
US06/904,180 US5053201A (en) | 1985-09-17 | 1986-09-05 | Process and apparatus for preparation of polyesters |
EP86112684A EP0215460B1 (en) | 1985-09-17 | 1986-09-13 | Process and apparatus for preparation of polyesters |
DE8686112684T DE3676399D1 (de) | 1985-09-17 | 1986-09-13 | Verfahren und apparat zur herstellung von polyestern. |
KR1019860007848A KR870003146A (ko) | 1985-09-17 | 1986-09-17 | 폴리에스테르의 제조방법 및 장치 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP20346585A JPS6264822A (ja) | 1985-09-17 | 1985-09-17 | ポリエステルの製造方法および装置 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS6264822A JPS6264822A (ja) | 1987-03-23 |
JPH0364534B2 true JPH0364534B2 (enrdf_load_stackoverflow) | 1991-10-07 |
Family
ID=16474577
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP20346585A Granted JPS6264822A (ja) | 1985-09-17 | 1985-09-17 | ポリエステルの製造方法および装置 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6264822A (enrdf_load_stackoverflow) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10322830A1 (de) * | 2003-05-19 | 2004-12-09 | Tesa Ag | Verfahren zur kontinuierlichen Herstellung von Polymeren aus vinylischen Verbindungen durch Substanz-beziehungsweise Lösungsmittelpolymerisation |
-
1985
- 1985-09-17 JP JP20346585A patent/JPS6264822A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS6264822A (ja) | 1987-03-23 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US3161710A (en) | Polymerization process for polyester films | |
US4056514A (en) | Continuous manufacture of polybutylene terephthalates | |
US5635589A (en) | Process for production of condensation polymers | |
US3591344A (en) | Device for continuous polycondensation | |
JP4063844B2 (ja) | ポリトリメチレンテレフタレート樹脂およびその製造方法 | |
US5856423A (en) | Apparatus and process for a polycondensation reaction | |
US5331066A (en) | Process for producing polyester ether copolymer | |
KR100684683B1 (ko) | 폴리트리메틸렌 테레프탈레이트 수지 | |
RU2271369C2 (ru) | Способ увеличения скорости твердофазной полимеризации сложных полиэфиров | |
EP0889922B1 (en) | Apparatus and process for a polycondensation reaction | |
WO1997035902A9 (en) | Apparatus and process for a polycondensation reaction | |
JPH0364534B2 (enrdf_load_stackoverflow) | ||
EP0215460B1 (en) | Process and apparatus for preparation of polyesters | |
JP4144967B2 (ja) | 横型反応装置 | |
JP3602958B2 (ja) | 横型反応槽 | |
US3679368A (en) | Continuous polyester polymerization apparatus | |
US3836574A (en) | Process for the manufacture of film-and fiber-forming polyesters | |
JP3573576B2 (ja) | ポリエステルの連続反応方法及びその装置 | |
KR100467403B1 (ko) | 중축합반응방법및장치 | |
JPS62131017A (ja) | ポリエステルの重合装置 | |
CA2247239C (en) | Apparatus and process for a polycondensation reaction | |
JP2002105184A (ja) | 高分子量ポリブチレンサクシネートの連続製造方法 | |
JPS6368630A (ja) | ポリエステルの重合装置 | |
JP2004225008A (ja) | 高重合度ポリトリメチレンテレフタレートの製造方法 | |
JPH0454198Y2 (enrdf_load_stackoverflow) |