JPH02111011A - Drainage of water and apparatus therefor - Google Patents

Drainage of water and apparatus therefor

Info

Publication number
JPH02111011A
JPH02111011A JP26285088A JP26285088A JPH02111011A JP H02111011 A JPH02111011 A JP H02111011A JP 26285088 A JP26285088 A JP 26285088A JP 26285088 A JP26285088 A JP 26285088A JP H02111011 A JPH02111011 A JP H02111011A
Authority
JP
Japan
Prior art keywords
water
organic solvent
blind hole
boiling point
heated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP26285088A
Other languages
Japanese (ja)
Inventor
Yosuke Yamada
要輔 山田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to JP26285088A priority Critical patent/JPH02111011A/en
Publication of JPH02111011A publication Critical patent/JPH02111011A/en
Pending legal-status Critical Current

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  • Cleaning By Liquid Or Steam (AREA)
  • Manufacturing Of Printed Wiring (AREA)
  • Cleaning Or Drying Semiconductors (AREA)

Abstract

PURPOSE:To simply and surely remove water even in a blind hole and at the inside of a gap by a method wherein a high-boilingpoint organic solvent is heated, an object to be cleaned is immersed in the heated organic solvent and the water on the surface of a workpiece and inside the blind hole of the workpiece is drained. CONSTITUTION:An organic solvent 12 whose boiling point is at 70 to 130 deg.C is heated to its boiling point or near its boiling point; an object 1, to be cleaned, which has a fine gap or a small-diameter blind hole and which has been washed by water is immersed in the heated organic solvent 12; water 3 is also heated and boiled. When the water 3 is boiled up, the water 3 is moved violently; the water is vibrated or flows inside the blind hole 2; one part of the water 3 springs out to the outside of the blind hole 2. When the water 3 is discharged from the inside of the blind hole 2, the organic solvent 12 enters the blind hole 2 and the water 3 is excluded completely from the inside of the blind hole 2. Thereby, also the water at the gap and inside the blind hole 2 can be removed completely and can be drained.

Description

【発明の詳細な説明】 〈産業上の利用分野〉 本発明は、有機溶剤を用いて被洗浄物に付着した水を除
去するものであり、特に被洗浄物の微細な隙間や小径の
盲孔の中に入り込んだ水をも完全に除去できるように企
図したものである。
[Detailed Description of the Invention] <Industrial Field of Application> The present invention uses an organic solvent to remove water adhering to an object to be cleaned. It is designed to completely remove water that has gotten into the tank.

〈従来の技術〉 電子部品、半導体部品、メツキ部品など(以下「ワーク
」と称す)は、最終工程において、汚れ等を取り除くた
め洗浄される。この洗浄では、最初に水により水洗され
、その後、ワークの表面に付着した水を有機溶剤を用い
て水切りして除去する。有機溶剤を几iいて水切りをす
るのは、水洗したワークをそのまま自然乾燥すると、水
に溶は込んでいた不純物(微量な塩など)がワークの表
面に残って「シミ」が発生するので、この「シミ」の発
生を防ぐために行なうのである。
<Prior Art> Electronic parts, semiconductor parts, plated parts, etc. (hereinafter referred to as "workpieces") are cleaned in the final process to remove dirt and the like. In this cleaning, the workpiece is first washed with water, and then water adhering to the surface of the workpiece is drained and removed using an organic solvent. The reason for rinsing off the organic solvent and draining the water is because if you air-dry the washed workpiece as it is, impurities dissolved in the water (such as trace amounts of salt) will remain on the surface of the workpiece and cause "stains". This is done to prevent this "stain" from occurring.

水切りするために用いる有機溶剤としては次のような性
質が必要である。
The organic solvent used for draining water must have the following properties.

(il  水よりもワークを濡らしやすい。即ち、表面
張力及び粘度が水よりも小さい。
(il) Easily wets the workpiece than water. In other words, the surface tension and viscosity are lower than that of water.

fiil  自然乾燥しやすい。即ち、沸点及び蒸発潜
熱が小さく蒸発しやすい。
fiil Easy to air dry. That is, it has a small boiling point and latent heat of vaporization, and is easily evaporated.

610  水よりも比重が大きく水と溶けない。610 It has a higher specific gravity than water and does not dissolve in water.

上述した性質を持つ有機溶剤としては、フロン113(
沸点47,5℃)、塩化メチレン(沸点39.8℃)な
どの低沸点の有機溶剤がある。
As an organic solvent having the above-mentioned properties, Freon 113 (
There are organic solvents with low boiling points such as (boiling point: 47.5°C) and methylene chloride (boiling point: 39.8°C).

そこで従来では上述した低沸点有機溶剤に微量の界面活
性剤を添加した液中にワークを浸漬して水切をしていた
。つまり、水が表面に付着したワークを上述したような
を機溶剤中に入れると1、ワーク表面の水は、界面張力
作用によりワーク表面から引きはがされ、引きはがされ
た水は、比重差によって有機溶剤の表面に浮き上がる。
Therefore, in the past, the workpiece was immersed in a liquid containing the above-mentioned low-boiling point organic solvent and a small amount of surfactant added thereto to drain the water. In other words, when a workpiece with water attached to its surface is placed in a solvent as described above, the water on the workpiece surface is peeled off from the workpiece surface due to interfacial tension action, and the water that is peeled off has a specific gravity of The difference causes it to float on the surface of the organic solvent.

かくて水切ができる。This way you can drain the water.

なお、有機溶剤の表面に浮き上がった水はただちに流し
除かれる。そして水切りされたワークは有機溶剤から取
り出され、更に界面活性剤を取り除くため界面活性剤が
混入されていない有機溶剤を用いて洗浄される。
Note that water floating on the surface of the organic solvent is immediately washed away. The drained workpiece is then taken out from the organic solvent and further washed with an organic solvent not mixed with a surfactant to remove the surfactant.

〈発明が解決しようとする課題〉 ところで、第3図に断面図で示すように、ワークlにね
し孔などの小径の盲孔2がある場合には、上述した低沸
点有機 /8剤に入れても、ワーク1表面の水切はでき
るものの、盲孔2内に入り込んだ水を取り除くことばで
きない。これは、盲孔2の径が小さくて水の界面張力の
作用が大きくなり、水が盲孔2から外に出にくくなって
おり、有機溶剤がなかなか盲孔2内に入れないからであ
る。このような事態は、ワークに微細な隙間があるとき
にも同様に発生する。
<Problems to be Solved by the Invention> By the way, as shown in the cross-sectional view in FIG. Although water can be drained from the surface of the workpiece 1 even if water is poured into the blind hole 2, it is not possible to remove the water that has entered the blind hole 2. This is because the diameter of the blind hole 2 is small and the interfacial tension of the water becomes large, making it difficult for water to come out of the blind hole 2 and making it difficult for the organic solvent to enter into the blind hole 2. This situation also occurs when there are minute gaps in the workpiece.

そこで従来では、盲孔2を有するワーク1などでは、有
機溶剤でワーク表面の水切りをした後、ワークlを熱風
乾燥室に入れて盲孔2内の水を蒸発させたり、水を吸収
するアルコールの中に何度も漬けて盲孔2内の水を徐々
に吸収させて無くすようにしていた。
Therefore, in the past, for a workpiece 1 having a blind hole 2, etc., after draining the surface of the workpiece with an organic solvent, the workpiece 1 is placed in a hot air drying chamber to evaporate the water in the blind hole 2, or an alcohol that absorbs water is used. The water in the blind hole 2 was gradually absorbed and eliminated by immersing it in the water many times.

このように従来では盲孔や微細な隙間があると、その中
に入った水を取り出すのが難がしく、煩雑な作業を別途
行なわなくてはならなかった。
In the past, when there were blind holes or minute gaps, it was difficult to remove the water that had entered them, and a complicated work had to be carried out separately.

本発明は、上記従来技術に鑑み、盲孔や隙間の内部の水
をも、簡単且つ確実に取り除くことのできる水切り方法
及び水切り装置を提供するものである。
In view of the above-mentioned prior art, the present invention provides a draining method and a draining device that can easily and reliably remove water inside blind holes and gaps.

く課題を解決するための手段〉 上記課題を解決する本発明は、高沸点有機溶剤を加熱し
、この加熱した有機溶剤中に被洗浄物(ワーク)を浸漬
してワーク表面ならびにワークの盲孔内などの水切りを
することを、その要旨とする。
Means for Solving the Problems> The present invention solves the above problems by heating a high boiling point organic solvent and immersing an object (work) to be cleaned in the heated organic solvent to clean the surface of the work and the blind holes in the work. The gist of this is to drain the inside of the container.

〈実  施  例〉 以下に本発明の実施例を図面に基づき詳細に説明する。<Example> Embodiments of the present invention will be described in detail below based on the drawings.

第1図は本発明を適用した水切装置を示す。FIG. 1 shows a draining device to which the present invention is applied.

同図に示すように水切槽10内には金網11が配置され
、水切槽lO内が2つの室10a。
As shown in the figure, a wire mesh 11 is arranged inside the draining tank 10, and the inside of the draining tank 10 has two chambers 10a.

10bに仕切られている。この水切槽10内には、界面
活性剤を添加した高沸点の有機溶剤12、具体的にはト
リクロールエチレン(CllCff−CC1t :沸点
86.5℃)を入れている。
It is partitioned into 10b. This draining tank 10 contains a high boiling point organic solvent 12 to which a surfactant has been added, specifically trichlorethylene (CllCff-CC1t: boiling point 86.5°C).

金mllは、水切槽10の底面から高沸点有機溶剤12
の液面よりも上方にまで延在しており、その網目は10
0メツシユ(開度である。
ml of gold is removed from the bottom of the draining tank 10 using a high boiling point organic solvent 12.
It extends above the liquid level, and its mesh size is 10
0 mesh (opening degree).

更に一方の室10bの底面にはヒータ13が設置されて
いる。
Furthermore, a heater 13 is installed at the bottom of one of the chambers 10b.

水切槽10内には有機溶剤、12が次々と注入され、水
切りして有機溶剤、12の表面に浮んだ水と有機溶剤1
2は、仕切壁1・1を越流して分離・回収槽20に流れ
込む。分1雅・回収槽20では、比重差を利用して有a
溶剤12を水から分離し、分離した有a溶剤12を回収
してフィルタリング等の処理をして再び水切槽10に送
る。
Organic solvents 12 are injected one after another into the draining tank 10, and the water and organic solvent 1 float on the surface of the organic solvents 12 after draining.
2 overflows the partition walls 1 and 1 and flows into the separation/recovery tank 20. In the collection tank 20, the difference in specific gravity is used to
The solvent 12 is separated from the water, and the separated aqueous solvent 12 is recovered, subjected to filtering, etc., and sent to the draining tank 10 again.

仕上処理槽30は仕切壁31により2つの室30a、3
0bに分けられており、各室30a、30bには、界面
活性剤を添加していない有機溶剤30、具体的にはトリ
クロールエチレンを入れている。また室30bにはヒー
タ32を設置しており、ヒータ32で有a溶剤30が加
熱されて、有機溶剤ガス33が発生している。
The finishing treatment tank 30 is divided into two chambers 30a and 3 by a partition wall 31.
Each chamber 30a and 30b contains an organic solvent 30 to which no surfactant is added, specifically trichlorethylene. Further, a heater 32 is installed in the chamber 30b, and the aqueous solvent 30 is heated by the heater 32, and an organic solvent gas 33 is generated.

この装置では、水切槽10のヒータ13により有機溶剤
12がその沸点ないし沸点近くまで加熱される。そこで
水が付着した第3回に示すようなワークlを、室10a
内の有機溶剤12中に浸漬すると、水はワークlから取
り除かれて水切される。
In this device, the organic solvent 12 is heated by the heater 13 of the draining tank 10 to its boiling point or close to its boiling point. Then, the work l shown in the third example with water attached was placed in the chamber 10a.
When immersed in the organic solvent 12 in the workpiece 1, water is removed from the workpiece 1 and drained.

つまりワーク1の表面に付着した水は、有機溶剤12の
界面張力作用によりワーク1表面から引きは、がされ、
引きはがされた水は有機溶剤12の表面に浮き上がるの
である。この場合、室fob内ではヒータ13により加
熱された有機溶剤12が激しく沸き立ち有機溶剤12が
上下に乱流となって対流し渦や波などが発生し、この渦
や波により、浮き上がった水が有機溶剤12中に細かな
水滴となって混入することがある。しかし室lOb内で
生した渦や彼は、網目の細かい金網11で減衰・消去さ
れるため、室10a内では波などは生ぜず浮き上がった
水が有機溶剤12中に混入することはない。この結果、
室10a内に浸漬したワークに水が再付着することはな
い。もちろん、金網11があっても、室10a10b間
で有機溶剤12が流通できるので、室10a内の有機溶
剤12の温度は沸点ないし沸点に近くなる。
In other words, water adhering to the surface of the workpiece 1 is pulled off from the surface of the workpiece 1 by the interfacial tension effect of the organic solvent 12.
The stripped water floats to the surface of the organic solvent 12. In this case, in the chamber fob, the organic solvent 12 heated by the heater 13 boils violently, and the organic solvent 12 becomes a turbulent flow up and down, generating convective eddies and waves, and these eddies and waves cause the floating water to It may be mixed into the organic solvent 12 in the form of fine water droplets. However, since the vortices and waves generated in the chamber lOb are attenuated and eliminated by the fine wire mesh 11, no waves are generated in the chamber 10a, and the floating water does not mix into the organic solvent 12. As a result,
Water will not re-adhere to the workpiece immersed in the chamber 10a. Of course, even with the wire mesh 11, the organic solvent 12 can flow between the chambers 10a and 10b, so the temperature of the organic solvent 12 in the chamber 10a is at or near the boiling point.

一方、ワーク1内の盲孔2内に入った水も容易に取り除
かれる。このことを第2図を参照して説明する。第2図
(a)に示すように、盲孔2内に水3が入ったワークl
を、高温(例えば86℃)となった有機溶剤12中に入
れると、水3も加熱されて沸き立ってくる。水3が沸き
立つと水3の動きが激しくなり水3が盲孔2内で振動し
たり流動する。そうすると第2図℃)に示すように水3
の一部が盲孔2外に飛び出すことがあり、水3が盲孔2
外に出た分だけ有機溶剤12が盲孔2内に入り込む。−
旦を機溶剤12が盲孔12内に入ると、界面張力の均衡
状態が破れ、第2図(C)に示すように有機溶剤12が
盲孔12内に入りやすくなる。こうすると、水3の振動
と有機溶剤12の流入とが相俟って、水3が盲孔2内か
ら出ていくと同時に有機溶剤12が盲孔2内に入り、つ
いには水3は完全に盲孔2内から排除されてしまう。か
くて、盲孔2内の水切も行なわれる。
On the other hand, water that has entered the blind hole 2 in the workpiece 1 is also easily removed. This will be explained with reference to FIG. As shown in Fig. 2(a), a work l containing water 3 in a blind hole 2
When the water 3 is placed in the organic solvent 12 at a high temperature (for example, 86° C.), the water 3 is also heated and comes to a boil. When the water 3 boils, the movement of the water 3 becomes intense and the water 3 vibrates and flows within the blind hole 2. Then, as shown in Figure 2 (°C), water 3
A part of the water may jump out of the blind hole 2, and the water 3
The organic solvent 12 enters into the blind hole 2 by the amount that comes out. −
Once the organic solvent 12 enters the blind hole 12, the equilibrium state of interfacial tension is broken, and the organic solvent 12 easily enters the blind hole 12, as shown in FIG. 2(C). In this way, the vibration of the water 3 and the inflow of the organic solvent 12 combine to cause the water 3 to exit from the blind hole 2 and at the same time the organic solvent 12 enters the blind hole 2, and finally the water 3 is completely removed. It will be expelled from the blind hole 2. In this way, the blind hole 2 is also drained.

上述した如くしてワーク表面及び盲孔2内の水が取り除
かれたワークlは、水切槽10から引き上げられ、仕上
処理槽30にて界面活性剤が洗い流される。つまり、ワ
ークlは一旦、室30a中の有機溶剤30(これには界
面活性剤が含まれていない)に浸漬された後、有機溶剤
ガス33にさらされて洗浄される。盲孔2内に入った有
機溶剤は、水と異なり、ただちに蒸発する。
The work l from which the water on the work surface and in the blind hole 2 has been removed as described above is lifted from the draining tank 10, and the surfactant is washed away in the finishing treatment tank 30. That is, the work l is once immersed in the organic solvent 30 (which does not contain a surfactant) in the chamber 30a, and then exposed to the organic solvent gas 33 to be cleaned. The organic solvent that enters the blind hole 2 evaporates immediately, unlike water.

なお高沸点有a溶剤12としては、トリクロールエチレ
ンの他、沸点が70℃〜130℃のa機ン容斉り、例え
ばパークレン(CC4’ z = CCj! t:沸点
121.2℃)、1・l・1トリクロールエタン(CL
CClz ’沸点74.1″C)、ダイクロンS20 
(R−112+イソオクタン:沸点92.5℃)、ダ・
イフロンS (R−112;沸点92.8℃)などを用
いてもよい。
In addition to trichlorethylene, the high boiling point solvent 12 may include trichlorethylene, a solvent having a boiling point of 70° C. to 130° C., for example, percrene (CC4' z = CCj! t: boiling point 121.2° C.), 1・l・1 trichloroethane (CL
CClz 'boiling point 74.1''C), Dicron S20
(R-112+isooctane: boiling point 92.5°C), da.
Iflon S (R-112; boiling point 92.8°C) or the like may be used.

〈発明の効果〉 以上実施例とともに具体的に説明したように本発明によ
れば、高沸点(70°c−130℃)の有機溶剤をその
沸点ないし沸点近くまで加熱し、その中に被洗浄物を浸
漬するため、被洗浄物の微細な隙間や小径の盲孔の中に
入った水も加熱されて外部に出てしまうので、隙間や盲
孔内の水をも完全に取り除いて水切りすることができる
6しかも本発明を実現するには、有機溶剤として高沸点
のものを用いこれを加熱するというきわめて簡単な手段
を採用するだけでよい。
<Effects of the Invention> As specifically explained above in conjunction with the examples, according to the present invention, an organic solvent with a high boiling point (70°C to 130°C) is heated to its boiling point or close to its boiling point, and the to-be-cleaned solvent is heated to the boiling point or close to the boiling point. Since the items are immersed, any water that gets into the minute gaps or small diameter blind holes of the object to be cleaned is heated and flows out, so the water in the gaps and blind holes is completely removed and drained. Moreover, in order to realize the present invention, it is only necessary to employ an extremely simple method of using a high boiling point organic solvent and heating it.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は本発明を適用した水切装置を示す構成図、第2
図(a) (b) (C)は盲孔内の水を取り除いて水
切する様子を示す説明図、第3図は盲孔を有するワーク
を示す断面図である。 図  面  中 lはワーク(被洗浄物)、 2は盲孔、 3は水、 10は水切槽、 10a、’lobは室、 11は金網(網材)、 12は高沸点の有機溶剤、 13はヒータ、 14は仕切壁、 20は分離・回収槽、 30は仕上処理槽、 30a、30bは室、 31は仕切壁、 32はヒータ、 33は有機溶剤ガスである。
Fig. 1 is a configuration diagram showing a draining device to which the present invention is applied;
Figures (a), (b), and (c) are explanatory diagrams showing how water in the blind hole is removed and drained, and Fig. 3 is a sectional view showing a workpiece having a blind hole. In the drawing, l is the workpiece (object to be cleaned), 2 is the blind hole, 3 is water, 10 is the draining tank, 10a and 'lob are the chambers, 11 is the wire mesh (mesh material), 12 is the high boiling point organic solvent, 13 is a heater, 14 is a partition wall, 20 is a separation/recovery tank, 30 is a finishing treatment tank, 30a and 30b are chambers, 31 is a partition wall, 32 is a heater, and 33 is an organic solvent gas.

Claims (2)

【特許請求の範囲】[Claims] (1)沸点が70℃〜130℃の有機溶剤をその沸点な
いし沸点近くまで加熱しておき、微細な隙間や小径の盲
孔を有する水洗された被洗浄物を、加熱された前記有機
溶剤中に浸漬して水切りすることを特徴とする水切り方
法。
(1) An organic solvent with a boiling point of 70°C to 130°C is heated to the boiling point or close to the boiling point, and the washed object having fine gaps and small diameter blind holes is placed in the heated organic solvent. A draining method characterized by soaking in water and draining.
(2)沸点が70℃〜130℃の有機溶剤が貯留される
水切槽と、水切槽の底面から有機溶剤の液面上方にまで
配置されて水切槽内を二つの室に仕切るとともに有機溶
剤の流通を許容する一方で有機溶剤の急激な流勢を減衰
させる程度の網目となっている網材と、網材で仕切られ
た一方の室に設置されて前記有機溶剤をその沸点ないし
沸点近くまで加熱するヒータと、を有することを特徴と
する水切り装置。
(2) A draining tank that stores organic solvents with a boiling point of 70°C to 130°C, and a draining tank that is arranged from the bottom of the tank to above the liquid level of the organic solvent to partition the inside of the tank into two chambers and to remove the organic solvent. A mesh material having a mesh that allows the flow of the organic solvent while attenuating the rapid flow of the organic solvent, and a mesh material installed in one chamber partitioned by the mesh material to bring the organic solvent to its boiling point or close to its boiling point. A draining device characterized by having a heater for heating.
JP26285088A 1988-10-20 1988-10-20 Drainage of water and apparatus therefor Pending JPH02111011A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP26285088A JPH02111011A (en) 1988-10-20 1988-10-20 Drainage of water and apparatus therefor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP26285088A JPH02111011A (en) 1988-10-20 1988-10-20 Drainage of water and apparatus therefor

Publications (1)

Publication Number Publication Date
JPH02111011A true JPH02111011A (en) 1990-04-24

Family

ID=17381490

Family Applications (1)

Application Number Title Priority Date Filing Date
JP26285088A Pending JPH02111011A (en) 1988-10-20 1988-10-20 Drainage of water and apparatus therefor

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008235813A (en) * 2007-03-23 2008-10-02 Dainippon Screen Mfg Co Ltd Substrate treatment apparatus
JP2015015450A (en) * 2013-06-04 2015-01-22 三ツ星ベルト株式会社 Hole filling substrate having conductive film, manufacturing method thereof, and discoloration or ooze restraining method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5628684A (en) * 1979-08-03 1981-03-20 Daikin Ind Ltd Method of washing and drying article
JPS57209676A (en) * 1981-06-20 1982-12-23 Daikin Ind Ltd Washing and drying device
JPS6362234A (en) * 1986-09-02 1988-03-18 Daikin Ind Ltd Method and apparatus for removing adhering water on surface of article

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5628684A (en) * 1979-08-03 1981-03-20 Daikin Ind Ltd Method of washing and drying article
JPS57209676A (en) * 1981-06-20 1982-12-23 Daikin Ind Ltd Washing and drying device
JPS6362234A (en) * 1986-09-02 1988-03-18 Daikin Ind Ltd Method and apparatus for removing adhering water on surface of article

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008235813A (en) * 2007-03-23 2008-10-02 Dainippon Screen Mfg Co Ltd Substrate treatment apparatus
JP2015015450A (en) * 2013-06-04 2015-01-22 三ツ星ベルト株式会社 Hole filling substrate having conductive film, manufacturing method thereof, and discoloration or ooze restraining method

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