JPH01225793A - チタン及びチタン合金の陽極酸化皮膜組成物の製造方法 - Google Patents
チタン及びチタン合金の陽極酸化皮膜組成物の製造方法Info
- Publication number
- JPH01225793A JPH01225793A JP5064688A JP5064688A JPH01225793A JP H01225793 A JPH01225793 A JP H01225793A JP 5064688 A JP5064688 A JP 5064688A JP 5064688 A JP5064688 A JP 5064688A JP H01225793 A JPH01225793 A JP H01225793A
- Authority
- JP
- Japan
- Prior art keywords
- oxide film
- titanium
- anodic oxide
- film composition
- metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000010407 anodic oxide Substances 0.000 title claims abstract description 182
- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 56
- 239000000203 mixture Substances 0.000 title claims description 113
- 239000010936 titanium Substances 0.000 title claims description 62
- 229910052719 titanium Inorganic materials 0.000 title claims description 61
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims description 59
- 238000004519 manufacturing process Methods 0.000 title claims description 13
- 229910000000 metal hydroxide Inorganic materials 0.000 claims abstract description 36
- 150000004692 metal hydroxides Chemical class 0.000 claims abstract description 35
- 229910052751 metal Inorganic materials 0.000 claims abstract description 18
- 239000002184 metal Substances 0.000 claims abstract description 18
- 150000003839 salts Chemical class 0.000 claims abstract description 15
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 6
- 239000000725 suspension Substances 0.000 claims abstract description 5
- 150000004820 halides Chemical class 0.000 claims abstract description 4
- 229910052737 gold Inorganic materials 0.000 claims abstract 4
- 229910052791 calcium Inorganic materials 0.000 claims abstract 3
- 239000000243 solution Substances 0.000 claims description 41
- 239000007864 aqueous solution Substances 0.000 claims description 38
- 238000011282 treatment Methods 0.000 claims description 19
- 229910044991 metal oxide Inorganic materials 0.000 claims description 14
- 150000004706 metal oxides Chemical class 0.000 claims description 14
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 238000007743 anodising Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 229910052742 iron Inorganic materials 0.000 claims description 4
- 229910052748 manganese Inorganic materials 0.000 claims description 4
- 239000012266 salt solution Substances 0.000 claims description 4
- 229940037003 alum Drugs 0.000 claims description 3
- 150000003863 ammonium salts Chemical class 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 150000001860 citric acid derivatives Chemical class 0.000 claims description 3
- 150000003891 oxalate salts Chemical class 0.000 claims description 3
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 3
- 150000003892 tartrate salts Chemical class 0.000 claims description 3
- LCQXXBOSCBRNNT-UHFFFAOYSA-K ammonium aluminium sulfate Chemical compound [NH4+].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O LCQXXBOSCBRNNT-UHFFFAOYSA-K 0.000 claims description 2
- 150000002823 nitrates Chemical class 0.000 claims description 2
- 229910052804 chromium Inorganic materials 0.000 claims 3
- 229910052802 copper Inorganic materials 0.000 claims 3
- 229910052758 niobium Inorganic materials 0.000 claims 3
- 229910052710 silicon Inorganic materials 0.000 claims 3
- 229910052712 strontium Inorganic materials 0.000 claims 3
- 229910052718 tin Inorganic materials 0.000 claims 3
- 229910052720 vanadium Inorganic materials 0.000 claims 3
- 229910052749 magnesium Inorganic materials 0.000 claims 2
- 229910052759 nickel Inorganic materials 0.000 claims 2
- 238000002845 discoloration Methods 0.000 abstract description 3
- 238000011109 contamination Methods 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 239000010408 film Substances 0.000 description 175
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 12
- 238000002441 X-ray diffraction Methods 0.000 description 8
- 238000000862 absorption spectrum Methods 0.000 description 8
- 238000010998 test method Methods 0.000 description 8
- 238000002076 thermal analysis method Methods 0.000 description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 6
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
- -1 Sbs Chemical class 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 238000005299 abrasion Methods 0.000 description 4
- 238000001962 electrophoresis Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 2
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229910021538 borax Inorganic materials 0.000 description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
- 239000004327 boric acid Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- IMBKASBLAKCLEM-UHFFFAOYSA-L ferrous ammonium sulfate (anhydrous) Chemical compound [NH4+].[NH4+].[Fe+2].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O IMBKASBLAKCLEM-UHFFFAOYSA-L 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 235000017550 sodium carbonate Nutrition 0.000 description 2
- 239000004328 sodium tetraborate Substances 0.000 description 2
- 235000010339 sodium tetraborate Nutrition 0.000 description 2
- 239000006104 solid solution Substances 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000011975 tartaric acid Substances 0.000 description 2
- 235000002906 tartaric acid Nutrition 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910021503 Cobalt(II) hydroxide Inorganic materials 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 1
- RSBNPUNXBGVNNB-UHFFFAOYSA-M S(=O)(=O)([O-])[O-].[NH4+].[Co+] Chemical compound S(=O)(=O)([O-])[O-].[NH4+].[Co+] RSBNPUNXBGVNNB-UHFFFAOYSA-M 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- OIDPCXKPHYRNKH-UHFFFAOYSA-J chrome alum Chemical compound [K]OS(=O)(=O)O[Cr]1OS(=O)(=O)O1 OIDPCXKPHYRNKH-UHFFFAOYSA-J 0.000 description 1
- 229910000423 chromium oxide Inorganic materials 0.000 description 1
- 239000008199 coating composition Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 229940044175 cobalt sulfate Drugs 0.000 description 1
- 229910000361 cobalt sulfate Inorganic materials 0.000 description 1
- KTVIXTQDYHMGHF-UHFFFAOYSA-L cobalt(2+) sulfate Chemical compound [Co+2].[O-]S([O-])(=O)=O KTVIXTQDYHMGHF-UHFFFAOYSA-L 0.000 description 1
- LFSBSHDDAGNCTM-UHFFFAOYSA-N cobalt(2+);oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[O-2].[Ti+4].[Co+2] LFSBSHDDAGNCTM-UHFFFAOYSA-N 0.000 description 1
- ASKVAEGIVYSGNY-UHFFFAOYSA-L cobalt(ii) hydroxide Chemical compound [OH-].[OH-].[Co+2] ASKVAEGIVYSGNY-UHFFFAOYSA-L 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 210000004955 epithelial membrane Anatomy 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
Landscapes
- Chemical Treatment Of Metals (AREA)
- Other Surface Treatments For Metallic Materials (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5064688A JPH01225793A (ja) | 1988-03-04 | 1988-03-04 | チタン及びチタン合金の陽極酸化皮膜組成物の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5064688A JPH01225793A (ja) | 1988-03-04 | 1988-03-04 | チタン及びチタン合金の陽極酸化皮膜組成物の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH01225793A true JPH01225793A (ja) | 1989-09-08 |
| JPH0443993B2 JPH0443993B2 (OSRAM) | 1992-07-20 |
Family
ID=12864710
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5064688A Granted JPH01225793A (ja) | 1988-03-04 | 1988-03-04 | チタン及びチタン合金の陽極酸化皮膜組成物の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH01225793A (OSRAM) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007029602A1 (ja) * | 2005-09-08 | 2007-03-15 | Kinki University | 骨代替材料、該骨代替材料を含む医療用材料、及び該骨代替材料の製造方法 |
| JP2010540779A (ja) * | 2007-10-03 | 2010-12-24 | アクセンタス パブリック リミテッド カンパニー | 殺生物特性を持つ金属の製造方法 |
| CN103173835A (zh) * | 2011-12-22 | 2013-06-26 | 中国科学院大连化学物理研究所 | 一种金属钛材料的处理方法 |
| CN109537021A (zh) * | 2018-11-26 | 2019-03-29 | 天津师范大学 | 一种用于钠离子电池负极的氧化钛/氧化锡复合膜的制备方法 |
| US11312107B2 (en) * | 2018-09-27 | 2022-04-26 | Apple Inc. | Plugging anodic oxides for increased corrosion resistance |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS50121138A (OSRAM) * | 1974-03-11 | 1975-09-22 | ||
| JPS5219535A (en) * | 1975-08-06 | 1977-02-14 | Ricoh Co Ltd | Dry type developing powder |
| JPS5318438A (en) * | 1976-08-04 | 1978-02-20 | Mitsui Keikinzoku Kako | Process for forming electrolytic pigmentation coatings on aluminum and aluminum alloy |
| JPS634095A (ja) * | 1986-06-23 | 1988-01-09 | Seiko Instr & Electronics Ltd | チタン又はチタン合金カラ−発色の外装部品 |
| JPS6350497A (ja) * | 1986-08-18 | 1988-03-03 | Crown Denken:Kk | チタン材の彩色方法 |
-
1988
- 1988-03-04 JP JP5064688A patent/JPH01225793A/ja active Granted
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS50121138A (OSRAM) * | 1974-03-11 | 1975-09-22 | ||
| JPS5219535A (en) * | 1975-08-06 | 1977-02-14 | Ricoh Co Ltd | Dry type developing powder |
| JPS5318438A (en) * | 1976-08-04 | 1978-02-20 | Mitsui Keikinzoku Kako | Process for forming electrolytic pigmentation coatings on aluminum and aluminum alloy |
| JPS634095A (ja) * | 1986-06-23 | 1988-01-09 | Seiko Instr & Electronics Ltd | チタン又はチタン合金カラ−発色の外装部品 |
| JPS6350497A (ja) * | 1986-08-18 | 1988-03-03 | Crown Denken:Kk | チタン材の彩色方法 |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007029602A1 (ja) * | 2005-09-08 | 2007-03-15 | Kinki University | 骨代替材料、該骨代替材料を含む医療用材料、及び該骨代替材料の製造方法 |
| JP2010540779A (ja) * | 2007-10-03 | 2010-12-24 | アクセンタス パブリック リミテッド カンパニー | 殺生物特性を持つ金属の製造方法 |
| CN103173835A (zh) * | 2011-12-22 | 2013-06-26 | 中国科学院大连化学物理研究所 | 一种金属钛材料的处理方法 |
| CN103173835B (zh) * | 2011-12-22 | 2016-01-06 | 中国科学院大连化学物理研究所 | 一种金属钛材料的处理方法 |
| US11312107B2 (en) * | 2018-09-27 | 2022-04-26 | Apple Inc. | Plugging anodic oxides for increased corrosion resistance |
| CN109537021A (zh) * | 2018-11-26 | 2019-03-29 | 天津师范大学 | 一种用于钠离子电池负极的氧化钛/氧化锡复合膜的制备方法 |
| CN109537021B (zh) * | 2018-11-26 | 2020-07-21 | 天津师范大学 | 一种用于钠离子电池负极的氧化钛/氧化锡复合膜的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0443993B2 (OSRAM) | 1992-07-20 |
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