JP7645364B2 - モレキュラーシーブｓｓｚ－１２３、その合成と使用 - Google Patents

モレキュラーシーブｓｓｚ－１２３、その合成と使用 Download PDF

Info

Publication number
JP7645364B2
JP7645364B2 JP2023513464A JP2023513464A JP7645364B2 JP 7645364 B2 JP7645364 B2 JP 7645364B2 JP 2023513464 A JP2023513464 A JP 2023513464A JP 2023513464 A JP2023513464 A JP 2023513464A JP 7645364 B2 JP7645364 B2 JP 7645364B2
Authority
JP
Japan
Prior art keywords
molecular sieve
reaction mixture
source
aluminum
alkali
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2023513464A
Other languages
English (en)
Japanese (ja)
Other versions
JP2023539598A (ja
JP2023539598A5 (https=
JPWO2022043772A5 (https=
Inventor
シエ、ダン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chevron USA Inc
Original Assignee
Chevron USA Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chevron USA Inc filed Critical Chevron USA Inc
Publication of JP2023539598A publication Critical patent/JP2023539598A/ja
Publication of JP2023539598A5 publication Critical patent/JP2023539598A5/ja
Publication of JPWO2022043772A5 publication Critical patent/JPWO2022043772A5/ja
Application granted granted Critical
Publication of JP7645364B2 publication Critical patent/JP7645364B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7026—MFS-type, e.g. ZSM-57
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/633—Pore volume less than 0.5 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
JP2023513464A 2020-08-28 2021-05-10 モレキュラーシーブｓｓｚ－１２３、その合成と使用 Active JP7645364B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US202063071451P 2020-08-28 2020-08-28
US63/071,451 2020-08-28
PCT/IB2021/053941 WO2022043772A1 (en) 2020-08-28 2021-05-10 Molecular sieve ssz-123, its synthesis and use

Publications (4)

Publication Number Publication Date
JP2023539598A JP2023539598A (ja) 2023-09-15
JP2023539598A5 JP2023539598A5 (https=) 2024-03-07
JPWO2022043772A5 JPWO2022043772A5 (https=) 2024-03-07
JP7645364B2 true JP7645364B2 (ja) 2025-03-13

Family

ID=75919359

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2023513464A Active JP7645364B2 (ja) 2020-08-28 2021-05-10 モレキュラーシーブｓｓｚ－１２３、その合成と使用

Country Status (6)

Country Link
US (2) US11628429B2 (https=)
EP (1) EP4204361B1 (https=)
JP (1) JP7645364B2 (https=)
KR (1) KR20230057352A (https=)
CN (1) CN116075364A (https=)
WO (1) WO2022043772A1 (https=)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016519646A (ja) 2013-04-19 2016-07-07 エクソンモービル ケミカル パテンツ インコーポレイテッド モレキュラーシーブ、ｃｏｋ−５、その合成及び使用
JP2016523221A (ja) 2013-06-10 2016-08-08 エクソンモービル ケミカル パテンツ インコーポレイテッド モレキュラーシーブの製造方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR8504010A (pt) * 1984-08-21 1986-06-10 Mobil Oil Corp Processo para preparacao de zeolito cristalino poroso sintetico e processo para efetuar conversao catalitica de carga organica
US4873067A (en) 1984-08-21 1989-10-10 Mobil Oil Corporation Zeolite ZSM-57
US7011810B2 (en) 2001-09-28 2006-03-14 Exxonmobil Chemical Patents Inc. Crystalline molecular sieves
CN101384361A (zh) 2006-02-14 2009-03-11 埃克森美孚化学专利公司 用于制备mfs结构型分子筛的方法及其应用
WO2011023360A2 (en) 2009-08-28 2011-03-03 Exxonmobil Chemical Patents Inc. Method of making and use of molecular sieve of mfs framework type with controllable average size
US10046975B2 (en) * 2016-10-11 2018-08-14 Chevron U.S.A. Inc. Synthesis of molecular sieve SSZ-83
CN112585093A (zh) 2018-08-27 2021-03-30 埃克森美孚研究工程公司 分子筛和制造分子筛的方法
EP3931152B1 (en) * 2019-02-27 2023-09-06 Chevron U.S.A. Inc. Molecular sieve ssz-115, its synthesis and use
US11299443B2 (en) * 2020-04-03 2022-04-12 Exxonmobil Research And Engineering Company Distillate production from olefins in moving bed reactors

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016519646A (ja) 2013-04-19 2016-07-07 エクソンモービル ケミカル パテンツ インコーポレイテッド モレキュラーシーブ、ｃｏｋ−５、その合成及び使用
JP2016523221A (ja) 2013-06-10 2016-08-08 エクソンモービル ケミカル パテンツ インコーポレイテッド モレキュラーシーブの製造方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
LIAO, X. et al.，Synthesis,characterization of COK-5 with different Si/Al ratios and their catalytic properties for the tert-buthylation of phenol，Microporous and Mesoporous Materials，NL，Elsevier，2009年05月18日，Vol.124，PP.210-217，ISSN:1387-1811, DOI:10.1016/j.miromeso.2009.05.013

Also Published As

Publication number Publication date
JP2023539598A (ja) 2023-09-15
US20230191377A1 (en) 2023-06-22
KR20230057352A (ko) 2023-04-28
EP4204361A1 (en) 2023-07-05
CN116075364A (zh) 2023-05-05
US20220062877A1 (en) 2022-03-03
US11628429B2 (en) 2023-04-18
WO2022043772A1 (en) 2022-03-03
US11845066B2 (en) 2023-12-19
EP4204361B1 (en) 2024-08-21

Similar Documents

Publication Publication Date Title
JP6371476B2 (ja) モレキュラーシーブｓｓｚ−９８の製造方法
JP6381797B2 (ja) モレキュラーシーブｓｓｚ−９８
EP3755660A1 (en) Molecular sieve ssz-113, its synthesis and use
JP7622198B2 (ja) モレキュラーシーブｓｓｚ－１２２、その合成及び使用
JP7050794B2 (ja) モレキュラーシーブｓｓｚ－１１１、その合成及び使用
JP7645364B2 (ja) モレキュラーシーブｓｓｚ－１２３、その合成と使用
KR102694636B1 (ko) 분자체 ssz-115, 이의 합성 및 용도
JP7513701B2 (ja) Ｓｅｗ骨格型のアルミニウム含有モレキュラーシーブの合成
US10273161B2 (en) Synthesis of MFI framework type molecular sieves
JP7177935B2 (ja) モレキュラーシーブｓｓｚ－６３を調製する方法
JP7417711B2 (ja) モレキュラーシーブｓｓｚ－１１８及びその合成と使用
JP2026507208A (ja) 小型結晶ｓｓｚ－８１ゼオライトの調製方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20240227

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20240227

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20250219

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20250228

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20250303

R150 Certificate of patent or registration of utility model

Ref document number: 7645364

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150