JP7449249B2 - 再構成植物材料を製造する方法 - Google Patents
再構成植物材料を製造する方法 Download PDFInfo
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- JP7449249B2 JP7449249B2 JP2020573105A JP2020573105A JP7449249B2 JP 7449249 B2 JP7449249 B2 JP 7449249B2 JP 2020573105 A JP2020573105 A JP 2020573105A JP 2020573105 A JP2020573105 A JP 2020573105A JP 7449249 B2 JP7449249 B2 JP 7449249B2
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- nicotine
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- solvent
- plant material
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 title claims description 54
- 239000000463 material Substances 0.000 title claims description 26
- 241000208125 Nicotiana Species 0.000 claims description 78
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 78
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical class CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims description 61
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Chemical compound CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims description 31
- 239000000284 extract Substances 0.000 claims description 30
- 241000196324 Embryophyta Species 0.000 claims description 16
- 239000003125 aqueous solvent Substances 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 12
- 239000002699 waste material Substances 0.000 claims description 11
- LDMPZNTVIGIREC-ZGPNLCEMSA-N nicotine bitartrate Chemical compound O.O.OC(=O)[C@H](O)[C@@H](O)C(O)=O.OC(=O)[C@H](O)[C@@H](O)C(O)=O.CN1CCC[C@H]1C1=CC=CN=C1 LDMPZNTVIGIREC-ZGPNLCEMSA-N 0.000 claims description 10
- 239000006184 cosolvent Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- AIBWPBUAKCMKNS-PPHPATTJSA-N 2-hydroxybenzoic acid;3-[(2s)-1-methylpyrrolidin-2-yl]pyridine Chemical compound OC(=O)C1=CC=CC=C1O.CN1CCC[C@H]1C1=CC=CN=C1 AIBWPBUAKCMKNS-PPHPATTJSA-N 0.000 claims description 5
- MQWJVKLIBZWVEL-XRIOVQLTSA-N 3-[(2s)-1-methylpyrrolidin-2-yl]pyridine;dihydrochloride Chemical compound Cl.Cl.CN1CCC[C@H]1C1=CC=CN=C1 MQWJVKLIBZWVEL-XRIOVQLTSA-N 0.000 claims description 5
- HDJBTCAJIMNXEW-PPHPATTJSA-N 3-[(2s)-1-methylpyrrolidin-2-yl]pyridine;hydrochloride Chemical group Cl.CN1CCC[C@H]1C1=CC=CN=C1 HDJBTCAJIMNXEW-PPHPATTJSA-N 0.000 claims description 5
- YHBIGBYIUMCLJS-UHFFFAOYSA-N 5-fluoro-1,3-benzothiazol-2-amine Chemical compound FC1=CC=C2SC(N)=NC2=C1 YHBIGBYIUMCLJS-UHFFFAOYSA-N 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 229940069688 nicotine bitartrate Drugs 0.000 claims description 5
- BRTHFWPGJMGHIV-UHFFFAOYSA-L zinc;3-(1-methylpyrrolidin-2-yl)pyridine;dichloride;hydrate Chemical compound O.[Cl-].[Cl-].[Zn+2].CN1CCCC1C1=CC=CN=C1 BRTHFWPGJMGHIV-UHFFFAOYSA-L 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 4
- 229960002715 nicotine Drugs 0.000 description 26
- 235000019505 tobacco product Nutrition 0.000 description 25
- 150000001875 compounds Chemical class 0.000 description 15
- 239000000796 flavoring agent Substances 0.000 description 13
- 235000019634 flavors Nutrition 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- 238000000605 extraction Methods 0.000 description 11
- 239000000203 mixture Substances 0.000 description 10
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 9
- 239000000047 product Substances 0.000 description 9
- 239000006286 aqueous extract Substances 0.000 description 8
- 235000019504 cigarettes Nutrition 0.000 description 8
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000003906 humectant Substances 0.000 description 5
- 238000007582 slurry-cast process Methods 0.000 description 5
- 238000001035 drying Methods 0.000 description 4
- 239000012467 final product Substances 0.000 description 4
- 230000001953 sensory effect Effects 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000000443 aerosol Substances 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 239000000945 filler Substances 0.000 description 3
- 235000013355 food flavoring agent Nutrition 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 230000000391 smoking effect Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- -1 leaves Substances 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000012978 lignocellulosic material Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000003278 mimic effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 239000013055 pulp slurry Substances 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 238000007738 vacuum evaporation Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
- A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
- A24C5/01—Making cigarettes for simulated smoking devices
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/20—Cigarettes specially adapted for simulated smoking devices
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Epidemiology (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Biotechnology (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Botany (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Alternative & Traditional Medicine (AREA)
- Engineering & Computer Science (AREA)
- Manufacture Of Tobacco Products (AREA)
Description
繊維状植物材料を溶媒で抽出して、抽出物及び繊維状部分を得る工程と、
上記繊維状部分から上記抽出物を分離する工程と、
上記繊維状部分から基材シートを形成する工程と、
ニコチン塩を上記抽出物と混合する工程と、
上記抽出物を上記基材シートに塗布する工程と
を有する方法が提供される。
ニコチン塩酸塩、ニコチン二塩酸塩、酒石酸ニコチン、重酒石酸ニコチン、重酒石酸ニコチン二水和物、硫酸ニコチン、ニコチン塩化亜鉛一水和物、及びサリチル酸ニコチン、並びにこれらの組み合わせから選択されるニコチン塩を含み、
ニコチン含量が上記再構成タバコ製品の2~25重量%である、
再構成タバコ製品が提供される。
ニコチン塩酸塩、ニコチン二塩酸塩、酒石酸ニコチン、重酒石酸ニコチン、重酒石酸ニコチン二水和物、硫酸ニコチン、ニコチン塩化亜鉛一水和物、及びサリチル酸ニコチン、並びにこれらの組み合わせから選択されるニコチン塩を含み、
ニコチン含量が上記再構成タバコ製品の2~25重量%である、
再構成タバコ製品が提供される。
繊維状植物材料を溶媒で抽出して、抽出物及び繊維状部分を得る工程と、
上記繊維状部分から上記抽出物を分離する工程と、
上記繊維状部分から基材シートを形成する工程と、
ニコチン塩を上記抽出物と混合する工程と、
上記抽出物を上記基材シートに塗布する工程と
を有する方法を提供する。
ニコチン塩酸塩、ニコチン二塩酸塩、酒石酸ニコチン、重酒石酸ニコチン、重酒石酸ニコチン二水和物、硫酸ニコチン、ニコチン塩化亜鉛一水和物、及びサリチル酸ニコチン、並びにこれらの組み合わせから選択されるニコチン塩を含み、ニコチン含量が上記再構成タバコ製品の2~25重量%である、再構成タバコ製品も提供する。
Claims (9)
- 再構成植物材料を製造する方法であって、
繊維状植物材料を溶媒で抽出して、抽出物及び繊維状部分を得る工程と、
上記繊維状部分から上記抽出物を分離する工程と、
上記繊維状部分から基材シートを形成する工程と、
ニコチン塩を上記抽出物と混合する工程と、
上記抽出物を上記基材シートに塗布する工程と
を有する方法。 - 上記溶媒は水性溶媒である、請求項1に記載の方法。
- 上記抽出物を上記基材シートに塗布する前に、上記抽出物を濃縮して濃縮抽出物を得る工程を有する、請求項1又は2に記載の方法。
- 上記ニコチン塩を上記濃縮抽出物と混合する、請求項3に記載の方法。
- 上記繊維状植物材料はタバコである、請求項1~4のいずれか1項に記載の方法。
- 上記タバコは、タバコ葉、タバコ茎、タバコ粉末、及び/又はタバコくずの形態である、請求項5に記載の方法。
- 上記ニコチン塩は、ニコチン塩酸塩、ニコチン二塩酸塩、酒石酸ニコチン、重酒石酸ニコチン、重酒石酸ニコチン二水和物、硫酸ニコチン、ニコチン塩化亜鉛一水和物、及びサリチル酸ニコチン、並びにこれらの組み合わせから選択される、請求項1~6のいずれか1項に記載の方法。
- 上記ニコチン塩は水溶液として供給される、請求項1~7のいずれか1項に記載の方法。
- 上記ニコチン塩の水溶液は共溶媒を含む、請求項8に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB1810729.2A GB201810729D0 (en) | 2018-06-29 | 2018-06-29 | A method for manufacturing reconstituted plant material |
GB1810729.2 | 2018-06-29 | ||
PCT/EP2019/067304 WO2020002583A1 (en) | 2018-06-29 | 2019-06-28 | A method for manufacturing reconstituted plant material |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2021528986A JP2021528986A (ja) | 2021-10-28 |
JP7449249B2 true JP7449249B2 (ja) | 2024-03-13 |
Family
ID=63143679
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2020573105A Active JP7449249B2 (ja) | 2018-06-29 | 2019-06-28 | 再構成植物材料を製造する方法 |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP3813565A1 (ja) |
JP (1) | JP7449249B2 (ja) |
GB (1) | GB201810729D0 (ja) |
TW (1) | TWI832870B (ja) |
WO (1) | WO2020002583A1 (ja) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111528515A (zh) * | 2020-04-30 | 2020-08-14 | 云南中烟工业有限责任公司 | 一种含尼古丁-3,5-二羟基苯甲酸盐的烟草再造烟叶及其应用 |
KR102616656B1 (ko) * | 2021-05-12 | 2023-12-21 | 주식회사 케이티앤지 | 니코틴 시트 및 이를 포함하는 에어로졸 발생 물품 |
CN114698867B (zh) * | 2022-04-08 | 2023-03-03 | 贵州黄果树金叶科技有限公司 | 一种精准成分再造烟叶制备方法及再造烟叶 |
Citations (2)
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JP5292935B2 (ja) | 2008-06-16 | 2013-09-18 | 日本電気株式会社 | メモリモジュール制御方法及びメモリモジュール並びにデータ転送装置 |
CN105455190A (zh) | 2016-02-01 | 2016-04-06 | 湖北中烟工业有限责任公司 | 一种电子烟液 |
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GB1111007A (en) | 1965-03-30 | 1968-04-24 | Imp Tobacco Co Ltd | Improvements in cigarettes and paper therefor |
US3385303A (en) * | 1966-06-16 | 1968-05-28 | Philip Morris Inc | Reconstituted tobacco product |
BE788844A (fr) | 1971-09-23 | 1973-01-02 | Imp Tobacco Group Ltd | Renforcement de la nicotine des produits a fumer |
GB1466912A (en) | 1974-06-19 | 1977-03-09 | British American Tobacco Co | Smoking materials |
US5143097A (en) * | 1991-01-28 | 1992-09-01 | R. J. Reynolds Tobacco Company | Tobacco reconstitution process |
US5501237A (en) * | 1991-09-30 | 1996-03-26 | R. J. Reynolds Tobacco Company | Tobacco reconstitution process |
US5377698A (en) * | 1993-04-30 | 1995-01-03 | Brown & Williamson Tobacco Corporation | Reconstituted tobacco product |
JP2928388B2 (ja) * | 1993-05-28 | 1999-08-03 | ブラウン アンド ウイリアムソン タバコ コーポレーション | 喫煙品 |
US5325877A (en) | 1993-07-23 | 1994-07-05 | R. J. Reynolds Tobacco Company | Tobacco reconstitution process |
US5533530A (en) | 1994-09-01 | 1996-07-09 | R. J. Reynolds Tobacco Company | Tobacco reconstitution process |
US7428905B2 (en) | 2004-07-30 | 2008-09-30 | R.J. Reynolds Tobacco Company | Method of making smokeable tobacco substitute filler having an increased fill value |
US20110173721A1 (en) * | 2005-05-11 | 2011-07-14 | Albino Anthony P | Reduced risk tobacco products and methods of making same |
GB201108860D0 (en) * | 2011-05-26 | 2011-07-06 | British American Tobacco Co | Tobacco treatment |
JP5981123B2 (ja) * | 2011-10-11 | 2016-08-31 | サンサ コーポレーション (バルバドス) インク | ニコチン薬の製造法およびその方法により製造される医薬 |
CN103462204B (zh) | 2013-09-18 | 2015-06-03 | 浙江中烟工业有限责任公司 | 一种水提法和超临界co2萃取法制得的复合烟草致香物质的再造烟叶及由其制备的卷烟 |
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CN106793835A (zh) * | 2014-08-13 | 2017-05-31 | 菲利普莫里斯生产公司 | 包括多用途计算装置的气溶胶生成系统 |
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GB201521626D0 (en) * | 2015-12-08 | 2016-01-20 | British American Tobacco Co | Tobacco composition |
-
2018
- 2018-06-29 GB GBGB1810729.2A patent/GB201810729D0/en not_active Ceased
-
2019
- 2019-06-28 EP EP19734771.9A patent/EP3813565A1/en active Pending
- 2019-06-28 WO PCT/EP2019/067304 patent/WO2020002583A1/en active Application Filing
- 2019-06-28 JP JP2020573105A patent/JP7449249B2/ja active Active
- 2019-06-28 TW TW108122778A patent/TWI832870B/zh active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5292935B2 (ja) | 2008-06-16 | 2013-09-18 | 日本電気株式会社 | メモリモジュール制御方法及びメモリモジュール並びにデータ転送装置 |
CN105455190A (zh) | 2016-02-01 | 2016-04-06 | 湖北中烟工业有限责任公司 | 一种电子烟液 |
Also Published As
Publication number | Publication date |
---|---|
TW202000049A (zh) | 2020-01-01 |
WO2020002583A1 (en) | 2020-01-02 |
TWI832870B (zh) | 2024-02-21 |
GB201810729D0 (en) | 2018-08-15 |
EP3813565A1 (en) | 2021-05-05 |
JP2021528986A (ja) | 2021-10-28 |
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