JP7074436B2 - 装飾シート、装飾シートを含む構造体及び装飾シートの製造方法 - Google Patents
装飾シート、装飾シートを含む構造体及び装飾シートの製造方法 Download PDFInfo
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- B41M7/0027—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock using protective coatings or layers by lamination or by fusion of the coatings or layers
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- B29C45/00—Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
- B29C45/14—Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor incorporating preformed parts or layers, e.g. injection moulding around inserts or for coating articles
- B29C45/14688—Coating articles provided with a decoration
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Description
(1)G2PETフィルム上にD-6260ポリウレタン溶液を塗布して80℃で5分間、さらに100℃で5分間の条件で乾燥して、25μm厚ポリウレタン層を形成した。
装置:真空蒸着装置EX-400(アルバック株式会社、日本国神奈川県茅ヶ崎市)
ターゲット金属蒸発のエネルギー源:電子線
スズ蒸着層の厚さ:430オングストローム
スズ蒸着層の成膜速度:5オングストローム/秒
50質量部のSK1506BHE、17質量部のYM-5及び33質量部のメチルイソブチルケトン(MIBK)を混合して得られたアクリル接着剤溶液を、剥離処理が施されたG2PETフィルム上に塗布し、80℃で5分間、さらに120℃で5分間の条件で乾燥して、40μm厚アクリル接着層を形成した。
(1)G2PETフィルム上にD-6260ポリウレタン溶液を塗布して80℃で5分間、さらに100℃で5分間の条件で乾燥して、25μm厚ポリウレタン層を形成した。
装置:真空蒸着装置EX-400(アルバック株式会社)
ターゲット金属を蒸発させるエネルギー源:電子線
スズ蒸着層の厚さ:430オングストローム
スズ蒸着層の成膜速度:5オングストローム/秒
50質量部のSK1506BHE、17質量部のYM-5及び33質量部のメチルイソブチルケトン(MIBK)を混合して得られたアクリル接着剤溶液を、剥離処理が施されたG2PETフィルム上に塗布し、80℃で5分間、さらに120℃で5分間の条件で乾燥して、40μm厚アクリル接着層を形成した。
表面粗さ測定機Mitutoyo SURFTEST SV-3100(株式会社ミツトヨ、日本国神奈川県川崎市)を使用して、例1の(7)で形成した加飾層について、D-6260ポリウレタン溶液を平滑面上での乾燥厚みが10μmになる塗布量で塗布し、塗布する前と塗布後の表面粗さRz(μm)を測定した。塗布前の表面粗さは加飾層の印刷面の表面粗さRz1に相当し、塗布後の表面粗さは平滑化樹脂層の表面粗さRz2に相当する。結果を表2に示す。なお、シートに対して塗布方向をMachine Direction(MD)、この方向に直交する方向をCross Direction(CD)とし、それぞれの方向で表面粗さの測定を行った。表2における改善率は(Rz1-Rz2)/Rz1(%)である。
平滑化樹脂層の粘弾性特性を以下の手順で測定した。G2PETフィルム上にD-6260ポリウレタン溶液を塗布して80℃で5分間、さらに100℃で5分間の条件で乾燥して、平滑化樹脂層として25μm厚ポリウレタン層を形成した。動的粘弾性測定装置ARES(ティー・エイ・インスツルメント・ジャパン株式会社製、日本国東京都品川区)を用い、-40℃~200℃の温度範囲において、昇温速度5.0℃/分、周波数10Hzのストレッチモードで測定を行ったところ、100℃で8.55×107Pa、150℃で6.79×106Paであり、ストレッチモードで100℃~150℃の温度範囲における貯蔵弾性率は、1×106Pa~1.5×108Paの範囲に入っていた。
両面真空成型機(布施真空株式会社、日本国大阪府羽曳野市)を用いて、例1及び比較例1の装飾シートを145℃でプラスチック基材(平板及びカマボコ形状)上に真空圧空成形により貼り付けた。
装飾シート表面への室内蛍光灯の映り込み状態を比較した。結果を図3(例1)及び図4(比較例1)に写真で示す。これらの図面において楕円で囲まれた部分には蛍光灯の映り込みが視認できる。例1の装飾シートでは蛍光灯の映り込みは鮮明であり、装飾シート表面は平滑である。比較例1の装飾シートでは蛍光灯の映り込みが不鮮明であり、その近傍において光が粒状に反射していることから、装飾シート表面に凹凸が生じていることが推察される。
装飾シート表面の鮮映性を客観的に評価する指標として、例1と比較例1の装飾シートについて、MD及びCDそれぞれの方向で、真空圧空成形前後のうねり表面粗さWza及びWzbを測定した。目視での鮮映性と合わせて結果を表3に示す。また、うねり表面粗さWzと併せて測定した真空圧空成形前後の表面粗さRaの値を表4に示す。表3におけるうねり改善率は(Wza-Wzb)/Wza(%)であり、表4における平面改善率は(Raa-Rab)/Raa(%)である。
[態様1]
凹凸を有する印刷面を含む加飾層と、
前記加飾層の前記印刷面の上又は前記加飾層の上方に配置される平滑化樹脂層と
を有し、前記平滑化樹脂層の表面が前記印刷面より平滑である、真空圧空成形法又は射出成形法により基材に接着される、装飾シート。
[態様2]
前記加飾層の前記印刷面の表面粗さRz1が0.2μm以上であり、前記平滑化樹脂層の表面粗さRz2がRz1の0.95倍以下である、態様1に記載の装飾シート。
[態様3]
前記印刷面がグラビア印刷面である、態様1又は2のいずれかに記載の装飾シート。
[態様4]
前記平滑化樹脂層は、周波数10Hz、ストレッチモードの条件で測定したときに100℃~150℃の温度範囲で貯蔵弾性率が1×10 6 Pa~1.5×10 8 Paである、態様1~3のいずれかに記載の装飾シート。
[態様5]
前記平滑化樹脂層は、ポリウレタン又はアクリル樹脂を含む、態様1~4のいずれかに記載の装飾シート。
[態様6]
基材と、前記基材の表面に適用された態様1~5のいずれかに記載の装飾シートとを含む構造体。
[態様7]
凹凸を有する印刷面を含む加飾層を形成する工程と、
前記加飾層の前記印刷面の上又は前記加飾層の上方に平滑化樹脂層を形成し、前記印刷面より平滑な平滑化樹脂層の表面を形成する工程と
を含む、
真空圧空成形法又は射出成形法により基材に接着される、装飾シートの製造方法。
12 加飾層
122 印刷面
14 平滑化樹脂層
142 平滑化樹脂層の表面
16 支持層
162 第1支持層
164 第2支持層
18 接着層
22 表面層
24 接合層
26 光輝層
Claims (7)
- 凹凸を有する印刷面を含む加飾層と、
前記加飾層の前記印刷面の上又は前記加飾層の上方に配置される平滑化樹脂層と
を有し、前記平滑化樹脂層の表面が前記印刷面より平滑であり、前記加飾層の前記印刷面の表面粗さRz1が4μm以下である、真空圧空成形法又は射出成形法により基材に接着される、装飾シート。 - 前記加飾層の前記印刷面の表面粗さRz1が0.2μm以上であり、前記平滑化樹脂層の表面粗さRz2がRz1の0.95倍以下である、請求項1に記載の装飾シート。
- 前記印刷面がグラビア印刷面である、請求項1又は2のいずれかに記載の装飾シート。
- 前記平滑化樹脂層を形成する樹脂の貯蔵弾性率が、周波数10Hz、ストレッチモードの条件で測定したときに100℃~150℃の温度範囲で1×106Pa~1.5×108Paである、請求項1~3のいずれか一項に記載の装飾シート。
- 前記平滑化樹脂層は、ポリウレタン又はアクリル樹脂を含む、請求項1~4のいずれか一項に記載の装飾シート。
- 基材と、前記基材の表面に適用された請求項1~5のいずれか一項に記載の装飾シートとを含む構造体。
- 凹凸を有する印刷面を含む加飾層を形成する工程と、
前記加飾層の前記印刷面の上又は前記加飾層の上方に平滑化樹脂層を形成し、前記印刷面より平滑な平滑化樹脂層の表面を形成する工程と
を含み、前記加飾層の前記印刷面の表面粗さRz1が4μm以下である、
真空圧空成形法又は射出成形法により基材に接着される、装飾シートの製造方法。
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