JP6162250B2 - 間隙充填用スウェリングテープ - Google Patents
間隙充填用スウェリングテープ Download PDFInfo
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- JP6162250B2 JP6162250B2 JP2015538036A JP2015538036A JP6162250B2 JP 6162250 B2 JP6162250 B2 JP 6162250B2 JP 2015538036 A JP2015538036 A JP 2015538036A JP 2015538036 A JP2015538036 A JP 2015538036A JP 6162250 B2 JP6162250 B2 JP 6162250B2
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Images
Classifications
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Description
基材層を、横の長さが10mmであり、縦の長さが50mmになるように裁断して試片を製造する。製造された試片をカーボネート系電解質に含浸させて、密封した状態で常温で1日間放置した後、電解質から取り出して前記試片の縦方向の長さを測定した後、下記数式Aにより基材層の長手方向の変形率を測定する。
前記数式Aで、L1は、電解質に含浸させる前の基材層の縦方向の初期長さ、すなわち、50mmであり、L2は、電解質に含浸させた後に測定した前記基材層の縦方向の長さである。
スウェリングテープを、横の長さが25mmであり、縦の長さが200mmになるように裁断して試片を製造する。試片を粘着層を媒介してガラス板に2kgのゴムローラーを使用して付着し、常温で引張試験機を使用して5mm/secの剥離速度及び180°の剥離角度でスウェリングテープを剥離しながら剥離力を測定する。
実施例及び比較例で製造された電池を常温で1日間保管した後、電池を分解して電極組立体を取り出して、電極組立体に付着されていたスウェリングテープの状態を評価し、下記基準によって立体形状具現能を評価する。
○:スウェリングテープの立体形状が観察される。
△:スウェリングテープの立体形状が観察されない。
×:スウェリングテープの立体形状が観察されないで、テープが電極組立体から剥離される。
スウェリングテープの間隙充填能は、電極組立体の流動防止特性を評価する方法で評価することができる。前記方式には、例えば微小振動評価方式と微小衝撃評価方式が存在する。微小振動評価方式は、UN38.3規格の振動実験方法によって実行され、評価後に電池が電源無感になれば、流動による端子の切断と判断する。微小衝撃評価方式は、8角円柱内に電池を入れて、回転させて所定時間が経た後、電池が電源無感になれば、流動による端子の切断と判断する。前記方式によって評価したスウェリングテープの間隙充填能は、下記の基準によって評価する。
○:微小振動評価及び微小衝撃評価後、電池の電源が測定される。
△:微小振動評価または微小衝撃評価後、電池の電源が測定されるが、抵抗が10% 以上増加する。
×:微小振動評価または微小衝撃評価後、電池の電源が測定されない。
アルミニウムプレートに製造されたスウェリングテープの粘着層を付着した。この過程でテープは、横の長さが70mmであり、縦の長さが150mmになるように裁断して使用した。その後、前記付着されたテープの上部に再度同一なスウェリングテープを付着した。この過程でテープは、横の長さが25mmであり、縦の長さが130mmになるように裁断して使用した。前記二番目のテープの付着後に、常温でアルミニウムプレートを固定し、二番目のテープは、180゜に折って別途のPETフィルムに固定した後、5mm/secの剥離速度で剥離しながら背面剥離力を評価した。
[スウェリングテープの製造]
熱可塑性ポリウレタン(TPU)で製造された厚さが約40μmの無延伸フィルムを基材層で使用した。前記基材層の一面に約0.2重量部のイソシアネート架橋剤で架橋された100重量部のアクリル粘着樹脂を含むアクリル系粘着層として、SUS板に対する剥離力が600gf/25mm程度であり、厚さが15μm程度である粘着層を形成した。その後、粘着層の形成面と反対側の基材層の面に目的とする背面剥離力(20gf/25mm)を考慮して、フッ素系離型剤で背面コーティング層を形成してスウェリングテープを製造した。
陰極、陽極及びセパレーターを含むゼリーロール形状の電極組立体(断面直径:17.2mm)の外周の約50%の面積を覆うようにスウェリングテープを付着し、前記組立体を円筒状の缶(断面直径:17.5mm)に挿入した。その後、前記缶の内部にカーボネート系電解質を注入し、密封して電池を完成した。
[スウェリングテープの製造]
熱可塑性ポリウレタン(TPU)で製造された厚さが約40μmの無延伸フィルムを基材層で使用した。前記基材層の一面に約0.2重量部のイソシアネート架橋剤で架橋された100重量部のアクリル粘着樹脂を含むアクリル系粘着層として、SUS板に対する剥離力が595gf/25mm程度であり、厚さが15μm程度である粘着層を形成した。その後、粘着層の形成面と反対側の基材層の面に目的とする背面剥離力(20gf/25mm)を考慮して、シリコーン系離型剤で背面コーティング層を形成してスウェリングテープを製造した。
陰極、陽極及びセパレーターを含むゼリーロール形状の電極組立体(断面直径:17.2mm)の外周の約50%の面積を覆うようにスウェリングテープを付着し、前記組立体を円筒状の缶(断面直径:17.5mm)に挿入した。その後、前記缶の内部にカーボネート系電解質を注入し、密封して電池を完成した。
[スウェリングテープの製造]
熱可塑性ポリウレタン(TPU)で製造された厚さが約40μmの無延伸フィルムを基材層で使用した。前記基材層の一面に約0.2重量部のイソシアネート架橋剤で架橋された100重量部のアクリル粘着樹脂を含むアクリル系粘着層として、SUS板に対する剥離力が600gf/25mm程度であり、厚さが15μm程度である粘着層を形成した。その後、粘着層の形成面と反対側の基材層の面に目的とする背面剥離力(10gf/25mm)を考慮して、脂肪族系離型剤で背面コーティング層を形成してスウェリングテープを製造した。
陰極、陽極及びセパレーターを含むゼリーロール形状の電極組立体(断面直径:17.2mm)の外周の約50%の面積を覆うようにスウェリングテープを付着し、前記組立体を円筒状の缶(断面直径:17.5mm)に挿入した。その後、前記缶の内部にカーボネート系電解質を注入し、密封して電池を完成した。
[スウェリングテープの製造]
熱可塑性ポリウレタン(TPU)で製造された厚さが約40μmの無延伸フィルムを基材層で使用した。前記基材層の一面に約0.2重量部のイソシアネート架橋剤で架橋された100重量部のアクリル粘着樹脂を含むアクリル系粘着層として、SUS板に対する剥離力が605gf/25mm程度であり、厚さが15μm程度である粘着層を形成してスウェリングテープを製造した。基材層に別途の離型処理をしないで測定された背面剥離力は、500gf/25mmであった。
陰極、陽極及びセパレーターを含むゼリーロール形状の電極組立体(断面直径:17.2mm)の外周の約50%の面積を覆うようにスウェリングテープを付着し、前記組立体を円筒状の缶(断面直径:17.5mm)に挿入した。その後、前記缶の内部にカーボネート系電解質を注入し、密封して電池を完成した。
[スウェリングテープの製造]
熱可塑性ポリウレタン(TPU)で製造された厚さが約40μmの無延伸フィルムを基材層で使用した。前記基材層の一面に約0.2重量部のイソシアネート架橋剤で架橋された100重量部のアクリル粘着樹脂を含むアクリル系粘着層として、SUS板に対する剥離力が100gf/25mm程度であり、厚さが15μm程度である粘着層を形成してスウェリングテープを製造した。基材層に別途の離型処理をしないで測定された背面剥離力は、70gf/25mmであった。
陰極、陽極及びセパレーターを含むゼリーロール形状の電極組立体(断面直径:17.2mm)の外周の約50%の面積を覆うようにスウェリングテープを付着し、前記組立体を円筒状の缶(断面直径:17.5mm)に挿入した。その後、前記缶の内部にカーボネート系電解質を注入し、密封して電池を完成した。
20 基材層
103、104 間隙を形成している対象
101 立体形状を具現する前のスウェリングテープ
102 立体形状を具現したスウェリングテープ
2 スウェリングテープ
201 基材層
202 粘着層
51a、51b スウェリングテープ
52 缶
53 電極組立体
Claims (15)
- 電解液と接触すれば長手方向に変形する基材層と、
前記基材層の一面に前記基材層の長手方向と水平の方向に形成されており、下記数式1を満足する粘着層と、
前記基材層の前記粘着層が形成された面とは反対側面に存在する背面コーティング層と、
を含み、
前記基材層の前記粘着層が形成された面とは反対側面に対して、常温で5mm/secの剥離速度及び180゜の剥離角度で測定した前記粘着層の剥離力が、100gf/25mm以下であり、
ガラス板に対して、常温で5mm/secの剥離速度及び180゜の剥離角度で測定した前記粘着層の剥離力が、300gf/25mm以上であり、
前記背面コーティング層は、フッ素系離型剤、シリコーン型離型剤、ビニル基またはアクリル基を有すると共にシリコンを含有する離型剤及び脂肪族またはアミド系列の離型剤からなる群より選択された1種以上を含み、
前記基材層は、熱可塑性ポリウレタンを含み、
前記基材層は、下記数式2による長手方向への変形率が10%以上である間隙充填用スウェリングテープ。
数式1: 5 ≦ X2/X1 ≦ 130
数式2: 基材層の長手方向への変形率 = (L2−L1)/L1 × 100
数式1で、X1は、前記基材層の前記粘着層が形成されている面とは反対側面に対して、常温で5mm/secの剥離速度及び180゜の剥離角度で測定した前記粘着層の剥離力であり、X2は、ガラスに対して、常温で5mm/secの剥離速度及び180゜の剥離角度で測定した前記粘着層の剥離力であり、
数式2で、L1は、前記基材層が電解液と接触する前の初期長さであり、L2は、常温または60℃で前記基材層を電解液と24時間の間接触させた後に測定した前記基材層の長さである。 - 電解液と接触時に長手方向と垂直の方向に、高さが0.001mm〜2.00mmである立体構造を形成する請求項1に記載の間隙充填用スウェリングテープ。
- 前記基材層は、ASTM D2240によるショアA硬度が70A以上である請求項1に記載の間隙充填用スウェリングテープ。
- 前記基材層は、JIS K−7311によるショアD硬度が40D以上である請求項1に記載の間隙充填用スウェリングテープ。
- 前記基材層は、ポリエステルポリオール化合物、鎖延長剤及びイソシアネート化合物を含む混合物の反応物である請求項1に記載の間隙充填用スウェリングテープ。
- 前記数式1のX2/X1は、5〜130である請求項1に記載の間隙充填用スウェリングテープ。
- 前記粘着層は、アクリル粘着剤、ウレタン粘着剤、エポキシ粘着剤、シリコーン粘着剤またはゴム粘着剤を含む請求項1に記載の間隙充填用スウェリングテープ。
- 前記粘着層は、多官能性架橋剤により架橋されたアクリル重合体を含む請求項1に記載の間隙充填用スウェリングテープ。
- 前記基材層の前記粘着層が形成された面とは反対側面に前記粘着層が付着されている状態で巻き取られている請求項1に記載の間隙充填用スウェリングテープ。
- 第1基板及び前記第1基板と離隔されている第2基板の間に形成された間隙を充填する方法であって、
第1基板または第2基板に、請求項1に記載のスウェリングテープの粘着層を付着させて、前記スウェリングテープの基材層を電解液と接触させる方法を含む間隙充填方法。 - 前記第1及び第2基板のいずれか一つは電極組立体であり、他の一つは前記組立体を収納する缶である請求項10に記載の間隙充填方法。
- 請求項1のテープが外周面に付着されている電極組立体。
- 請求項12に記載の電極組立体と、
前記組立体が収納されている缶と、
前記缶の内部で前記組立体と接触している電解液と、を含む電池。 - 前記電極組立体の粘着テープは、電解液により具現された立体形状によって前記組立体を缶の内部に固定している請求項13に記載の電池。
- 前記電解液は、カーボネート系電解液である請求項14に記載の電池。
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KR101375888B1 (ko) * | 2011-01-27 | 2014-03-19 | 주식회사 엘지화학 | 간극 충전용 스웰링 테이프 |
JP2012164489A (ja) * | 2011-02-04 | 2012-08-30 | Nitto Denko Corp | 非水系電池用粘着テープ |
JP2012184396A (ja) * | 2011-02-15 | 2012-09-27 | Nitto Shinko Kk | 粘着テープ |
KR101292722B1 (ko) * | 2011-02-24 | 2013-08-01 | 주식회사 영우 | 감압성 점착테이프 |
JP5982131B2 (ja) * | 2011-02-28 | 2016-08-31 | 日東電工株式会社 | 電池用粘着テープ、及び該粘着テープを使用した電池 |
WO2012138153A2 (ko) * | 2011-04-05 | 2012-10-11 | 주식회사 엘지화학 | 간극 충진용 스웰링 테이프 |
JP5611883B2 (ja) | 2011-04-13 | 2014-10-22 | 日東電工株式会社 | 再剥離用水分散型アクリル系粘着剤組成物及び粘着シート |
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TWI513082B (zh) | 2015-12-11 |
EP2924765A1 (en) | 2015-09-30 |
KR101587326B1 (ko) | 2016-01-20 |
US10115951B2 (en) | 2018-10-30 |
TW201444150A (zh) | 2014-11-16 |
CN104798223B (zh) | 2017-02-22 |
EP2924765B1 (en) | 2018-06-13 |
WO2014077647A1 (ko) | 2014-05-22 |
US20150270524A1 (en) | 2015-09-24 |
EP2924765A4 (en) | 2016-05-25 |
KR20140063478A (ko) | 2014-05-27 |
JP2016500729A (ja) | 2016-01-14 |
CN104798223A (zh) | 2015-07-22 |
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