JP6087162B2 - ビスラクトン誘導体及びこれを含有する化粧料 - Google Patents
ビスラクトン誘導体及びこれを含有する化粧料 Download PDFInfo
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- JP6087162B2 JP6087162B2 JP2013019115A JP2013019115A JP6087162B2 JP 6087162 B2 JP6087162 B2 JP 6087162B2 JP 2013019115 A JP2013019115 A JP 2013019115A JP 2013019115 A JP2013019115 A JP 2013019115A JP 6087162 B2 JP6087162 B2 JP 6087162B2
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- Prior art keywords
- acid
- hair
- extract
- oil
- glycol
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- 239000002537 cosmetic Substances 0.000 title claims description 46
- PEHLCCGXTLWMRW-UHFFFAOYSA-N bis-lactone Chemical class C1CC2OC(=O)C3C1OC(=O)C32 PEHLCCGXTLWMRW-UHFFFAOYSA-N 0.000 title description 26
- 150000001875 compounds Chemical class 0.000 claims description 90
- 239000000203 mixture Substances 0.000 claims description 61
- 125000004432 carbon atom Chemical group C* 0.000 claims description 23
- 150000002009 diols Chemical group 0.000 claims description 19
- 125000004122 cyclic group Chemical group 0.000 claims description 18
- 125000001142 dicarboxylic acid group Chemical group 0.000 claims description 6
- 229920001515 polyalkylene glycol Chemical group 0.000 claims description 4
- 125000003827 glycol group Chemical group 0.000 claims description 2
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 4
- -1 silane compound Chemical class 0.000 description 185
- 239000000284 extract Substances 0.000 description 156
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 70
- 230000015572 biosynthetic process Effects 0.000 description 59
- 238000003786 synthesis reaction Methods 0.000 description 59
- 235000014113 dietary fatty acids Nutrition 0.000 description 56
- 229930195729 fatty acid Natural products 0.000 description 56
- 239000000194 fatty acid Substances 0.000 description 56
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 49
- 238000002156 mixing Methods 0.000 description 46
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 41
- 229920001296 polysiloxane Polymers 0.000 description 40
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 37
- 239000002253 acid Substances 0.000 description 37
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 36
- 238000002360 preparation method Methods 0.000 description 36
- 239000011734 sodium Substances 0.000 description 36
- 238000009472 formulation Methods 0.000 description 35
- 239000008213 purified water Substances 0.000 description 35
- 235000002639 sodium chloride Nutrition 0.000 description 33
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 30
- 150000004665 fatty acids Chemical class 0.000 description 28
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 27
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 26
- 239000003921 oil Substances 0.000 description 26
- 239000000843 powder Substances 0.000 description 26
- 150000003839 salts Chemical class 0.000 description 26
- 235000019388 lanolin Nutrition 0.000 description 25
- 235000019198 oils Nutrition 0.000 description 25
- 239000004166 Lanolin Substances 0.000 description 24
- 150000002596 lactones Chemical group 0.000 description 24
- 229940039717 lanolin Drugs 0.000 description 24
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 24
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 23
- 229920001577 copolymer Polymers 0.000 description 23
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 22
- 239000003795 chemical substances by application Substances 0.000 description 22
- 239000000539 dimer Substances 0.000 description 22
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 20
- 230000000694 effects Effects 0.000 description 20
- 238000000425 proton nuclear magnetic resonance spectrum Methods 0.000 description 20
- 238000000034 method Methods 0.000 description 19
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 19
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 18
- 238000010438 heat treatment Methods 0.000 description 18
- 239000002453 shampoo Substances 0.000 description 18
- 229910052708 sodium Inorganic materials 0.000 description 18
- 239000004359 castor oil Substances 0.000 description 17
- 235000019438 castor oil Nutrition 0.000 description 17
- 239000004205 dimethyl polysiloxane Substances 0.000 description 17
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 17
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 17
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 16
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 16
- 229940008099 dimethicone Drugs 0.000 description 15
- 150000002430 hydrocarbons Chemical group 0.000 description 15
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 14
- 239000003676 hair preparation Substances 0.000 description 14
- 239000001993 wax Substances 0.000 description 14
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 13
- 239000003595 mist Substances 0.000 description 13
- 229960005323 phenoxyethanol Drugs 0.000 description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 12
- 229910019142 PO4 Inorganic materials 0.000 description 12
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
- 238000000862 absorption spectrum Methods 0.000 description 12
- 229960000541 cetyl alcohol Drugs 0.000 description 12
- 235000015165 citric acid Nutrition 0.000 description 12
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 12
- 239000007789 gas Substances 0.000 description 12
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 12
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 12
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 12
- 229960002216 methylparaben Drugs 0.000 description 12
- 235000021317 phosphate Nutrition 0.000 description 12
- 229920000642 polymer Polymers 0.000 description 12
- 229920001451 polypropylene glycol Polymers 0.000 description 12
- 108090000765 processed proteins & peptides Proteins 0.000 description 12
- 239000004094 surface-active agent Substances 0.000 description 12
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 11
- 150000002148 esters Chemical group 0.000 description 11
- 239000000049 pigment Substances 0.000 description 11
- 239000007787 solid Substances 0.000 description 11
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 11
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 10
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 10
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 10
- 239000000118 hair dye Substances 0.000 description 10
- 239000007788 liquid Substances 0.000 description 10
- HQHCYKULIHKCEB-UHFFFAOYSA-N tetradecanedioic acid Natural products OC(=O)CCCCCCCCCCCCC(O)=O HQHCYKULIHKCEB-UHFFFAOYSA-N 0.000 description 10
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 9
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 9
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 9
- 229940022663 acetate Drugs 0.000 description 9
- 235000010323 ascorbic acid Nutrition 0.000 description 9
- 239000011668 ascorbic acid Substances 0.000 description 9
- 229960005070 ascorbic acid Drugs 0.000 description 9
- 229910052799 carbon Inorganic materials 0.000 description 9
- 229960002788 cetrimonium chloride Drugs 0.000 description 9
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 description 9
- 229940075529 glyceryl stearate Drugs 0.000 description 9
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 9
- 239000010452 phosphate Substances 0.000 description 9
- 235000010356 sorbitol Nutrition 0.000 description 9
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- 238000003756 stirring Methods 0.000 description 9
- WNZVVHVYAKZZBU-UHFFFAOYSA-N 1,17-Heptadecanediol Chemical compound OCCCCCCCCCCCCCCCCCO WNZVVHVYAKZZBU-UHFFFAOYSA-N 0.000 description 8
- PGMMMHFNKZSYEP-UHFFFAOYSA-N 1,20-Eicosanediol Chemical compound OCCCCCCCCCCCCCCCCCCCCO PGMMMHFNKZSYEP-UHFFFAOYSA-N 0.000 description 8
- SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-methylpentane-2,4-diol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 8
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 8
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 8
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 8
- BEPAFCGSDWSTEL-UHFFFAOYSA-N dimethyl malonate Chemical compound COC(=O)CC(=O)OC BEPAFCGSDWSTEL-UHFFFAOYSA-N 0.000 description 8
- GHLKSLMMWAKNBM-UHFFFAOYSA-N dodecane-1,12-diol Chemical compound OCCCCCCCCCCCCO GHLKSLMMWAKNBM-UHFFFAOYSA-N 0.000 description 8
- 238000011156 evaluation Methods 0.000 description 8
- 235000011187 glycerol Nutrition 0.000 description 8
- GJBXIPOYHVMPQJ-UHFFFAOYSA-N hexadecane-1,16-diol Chemical compound OCCCCCCCCCCCCCCCCO GJBXIPOYHVMPQJ-UHFFFAOYSA-N 0.000 description 8
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- LPNYRYFBWFDTMA-UHFFFAOYSA-N potassium tert-butoxide Chemical compound [K+].CC(C)(C)[O-] LPNYRYFBWFDTMA-UHFFFAOYSA-N 0.000 description 8
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- VBIIFPGSPJYLRR-UHFFFAOYSA-M Stearyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)C VBIIFPGSPJYLRR-UHFFFAOYSA-M 0.000 description 7
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- PMBRBOODEWULOI-UHFFFAOYSA-N trichloromethanide Chemical compound Cl[C-](Cl)Cl PMBRBOODEWULOI-UHFFFAOYSA-N 0.000 description 1
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- QJXPRGZXRIIGOP-UHFFFAOYSA-N tricosanedioic acid Chemical compound OC(=O)CCCCCCCCCCCCCCCCCCCCCC(O)=O QJXPRGZXRIIGOP-UHFFFAOYSA-N 0.000 description 1
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- 239000001069 triethyl citrate Substances 0.000 description 1
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 description 1
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- LINXHFKHZLOLEI-UHFFFAOYSA-N trimethyl-[phenyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound C[Si](C)(C)O[Si](O[Si](C)(C)C)(O[Si](C)(C)C)C1=CC=CC=C1 LINXHFKHZLOLEI-UHFFFAOYSA-N 0.000 description 1
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- 229940118594 trimethylolpropane triisostearate Drugs 0.000 description 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- 229940117972 triolein Drugs 0.000 description 1
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 1
- PBYZMCDFOULPGH-UHFFFAOYSA-N tungstate Chemical compound [O-][W]([O-])(=O)=O PBYZMCDFOULPGH-UHFFFAOYSA-N 0.000 description 1
- 239000008513 turmeric extract Substances 0.000 description 1
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- 229940075466 undecylenate Drugs 0.000 description 1
- 229960002703 undecylenic acid Drugs 0.000 description 1
- 239000004474 valine Substances 0.000 description 1
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- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 1
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 1
- 229960001722 verapamil Drugs 0.000 description 1
- 239000010679 vetiver oil Substances 0.000 description 1
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- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 239000011720 vitamin B Chemical group 0.000 description 1
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- 239000011718 vitamin C Substances 0.000 description 1
- 150000003700 vitamin C derivatives Chemical class 0.000 description 1
- 235000019166 vitamin D Nutrition 0.000 description 1
- 239000011710 vitamin D Substances 0.000 description 1
- 150000003710 vitamin D derivatives Chemical class 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 229940011671 vitamin b6 Drugs 0.000 description 1
- 229940046008 vitamin d Drugs 0.000 description 1
- 239000001717 vitis vinifera seed extract Substances 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
- ZFNVDHOSLNRHNN-UHFFFAOYSA-N xi-3-(4-Isopropylphenyl)-2-methylpropanal Chemical compound O=CC(C)CC1=CC=C(C(C)C)C=C1 ZFNVDHOSLNRHNN-UHFFFAOYSA-N 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- 239000001052 yellow pigment Substances 0.000 description 1
- 239000009538 yokuinin Substances 0.000 description 1
- 150000003751 zinc Chemical class 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
- 229940105125 zinc myristate Drugs 0.000 description 1
- 229940043810 zinc pyrithione Drugs 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 229910000368 zinc sulfate Inorganic materials 0.000 description 1
- 229960001763 zinc sulfate Drugs 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 description 1
- GBFLQPIIIRJQLU-UHFFFAOYSA-L zinc;tetradecanoate Chemical compound [Zn+2].CCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCC([O-])=O GBFLQPIIIRJQLU-UHFFFAOYSA-L 0.000 description 1
- 239000001243 zingiber officinale rosc. root absolute Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 description 1
- 229930007845 β-thujaplicin Natural products 0.000 description 1
- 239000002446 δ-tocopherol Substances 0.000 description 1
Description
また、使用されるジオールとしては、ポリアルキレングリコールであってもよく、具体的には、ジエチレングリコール、トリエチレングリコール、テトラエチレングリコール、ジプロピレングリコール、トリプロピレングリコール、テトラプロピレングリコール、ジブチレングリコール、トリブチレングリコール、テトラブチレングリコール、ジ(テトラメチレングリコール)、トリ(テトラメチレングリコール)、テトラ(テトラメチレングリコール)、ポリエチレングリコール、ポリプロピレングリコール、ポリブチレングリコール、ポリテトラメチレングリコール、およびこれらのランダムまたはブロック共重合体等が挙げられる。これらのうち、本発明の効果をより発揮される観点から、ジエチレングリコール、トリエチレングリコール、テトラエチレングリコール、ジプロピレングリコール、トリプロピレングリコール、ポリエチレングリコール、ポリプロピレングリコール、ポリブチレングリコール、ポリテトラメチレングリコールが好ましいものとして挙げられる。
両性界面活性剤では、ラウリルベタイン(ラウリルジメチルアミノ酢酸ベタイン)等のN−アルキル−N,N−ジメチルアミノ酸ベタイン;コカミドプロピルベタイン、ラウラミドプロピルベタイン等の脂肪酸アミドアルキル−N,N−ジメチルアミノ酸ベタイン;ココアンホ酢酸ナトリウム、ラウロアンホ酢酸ナトリウム等のイミダゾリン型ベタイン;アルキルジメチルタウリン等のアルキルスルホベタイン;アルキルジメチルアミノエタノール硫酸エステル等の硫酸型ベタイン;アルキルジメチルアミノエタノールリン酸エステル等のリン酸型ベタイン;ホスファチジルコリン、ホスファチジルエタノールアミン、ホスファチジルセリン、スフィンゴミエリン等のスフィンゴリン脂質、リゾレシチン、水素添加大豆リン脂質、部分水素添加大豆リン脂質、水素添加卵黄リン脂質、部分水素添加卵黄リン脂質、水酸化レシチン等のリン脂質類;シリコーン系両性界面活性剤等;高分子界面活性剤では、ポリビニルアルコール、アルギン酸ナトリウム、デンプン誘導体、トラガントガム、アクリル酸・メタアクリル酸アルキル共重合体;シリコーン系各種界面活性剤が好ましいものとして挙げられる。
赤色223号、赤色225号、赤色226号、赤色227号、赤色228号、赤色230−1号、赤色230−2号、赤色231号、赤色232号、赤色3号、赤色401号、赤色404号、赤色405号、赤色501号、赤色502号、赤色503号、赤色504号、赤色505号、赤色506号、橙色201号、橙色203号、橙色204号、橙色205号、橙色206号、橙色207号、橙色401号、橙色402号、橙色403号、黄色201号、黄色202−1号、黄色202−2号、黄色203号、黄色204号、黄色205号、黄色4号、黄色401号、黄色402号、黄色403−1号、黄色404号、黄色405号、黄色406号、黄色407号、黄色5号等の法定色素;Acid Red 14等のその他酸性染料;Arianor Sienna Brown、Arianor Madder Red、Arianor Steel Blue、Arianor Straw Yellow等の塩基染料;HC Yellow 2、HC Yellow 5、HC Red 3、4-hydoxypropylamino-3-nitrophenol、N,N’-bis(2-hydroxyethyl)-2-nitro-p-
phenylenediamine、HC Blue 2、Basic
Blue 26等のニトロ染料;分散染料;二酸化チタン、酸化亜鉛等の無機白色顔料;酸化鉄(ベンガラ)、チタン酸鉄等の無機赤色系顔料;γ−酸化鉄等の無機褐色系顔料;黄酸化鉄、黄土等の無機黄色系顔料;黒酸化鉄、低次酸化チタン等の無機黒色系顔料;マンゴバイオレット、コバルトバイオレット等の無機紫色系顔料;酸化クロム、水酸化クロム、チタン酸コバルト等の無機緑色系顔料;群青、紺青等の無機青色系顔料;酸化チタンコーテッドマイカ、酸化チタンコーテッドオキシ塩化ビスマス、酸化チタンコーテッドタルク、着色酸化チタンコーテッドマイカ、オキシ塩化ビスマス、魚鱗箔等のパール顔料;アルミニウムパウダー、カッパーパウダー、金等の金属粉末顔料;表面処理無機及び金属粉末顔料;赤色201号、赤色202号、赤色204号、赤色205号、赤色220号、赤色226号、赤色228号、赤色405号、橙色203号、橙色204号、黄色205号、黄色401号、青色404号、赤色3号、赤色104号、赤色106号、赤色227号、赤色230号、赤色401号、赤色505号、橙色205号、黄色4号、黄色5号、黄色202号、黄色203号、緑色3号、青色1号等のジルコニウム、バリウム又はアルミニウムレーキ等の有機顔料;表面処理有機顔料;アスタキサンチン、アリザリン等のアントラキノン類、アントシアニジン、β−カロチン、カテナール、カプサンチン、カルコン、カルサミン、クエルセチン、クロシン、クロロフィル、クルクミン、コチニール、シコニン等のナフトキノン類、ビキシン、フラボン類、ベタシアニジン、ヘナ、ヘモグロビン、リコピン、リボフラビン、ルチン等の天然色素・染料;p−フェニレンジアミン、トルエン−2,5−ジアミン、o−,m−,若しくはp−アミノフェノール、m−フェニレンジアミン、5−アミノ−2−メチルフェノール、レゾルシン、1−ナフトール、2,6−ジアミノピリジン等及びその塩等の酸化染料中間体及びカップラー;インドリン等の自動酸化型染料;ジヒドロキシアセトンが好ましいものとして挙げられる。
攪拌機、温度計、ガス導入管を備えた50mLの反応器に、γ-ヒドロキシメチル−γ−ブチロラクトン1.84g(0.0158モル)、ピリジン1.31g(0.0166モル)、トルエン 4.19gを仕込み、窒素雰囲気下にセバコイルクロリド1.80g(0.0075モル)を滴下して、25℃で2時間反応させた。得られた反応液を水洗、酸洗浄、脱酸、水洗を行い、トルエン層を濃縮し目的物の化合物2.08gを固形物として得た。得られた固形物は白色固体であった(赤外吸収スペクトル(KBr錠剤法):2930、2857、1775、1732、1152cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表1にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた200mLの反応器に、DL−ホモセリン10.0g(0.0839モル)、水18.0g、アセトン12.0gを仕込み、水酸化ナトリウムでpHを11〜13に調整しながら、セバコイルクロリド8.0g(0.0336モル)を滴下して、15℃で1時間反応させた。得られた反応液中に水21.3gを加えて、pHが1.5になるまで硫酸を加えた。分液した上層を濃縮後、85℃で減圧乾燥して固体として8gを得た。得られた固形物は白色固体であった(赤外吸収スペクトル(KBr錠剤法)2930、2857、1775、1643、1545、1170cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表2にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた500mLの反応器に、1,6−ヘキサンジオールジグリシジルエーテル70.0g(0.304モル)、マロン酸ジメチル80.3g(0.608モル)、カリウムt−ブトキシド6.8g、t−ブチルアルコ−ル35.0gを仕込み、16時間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム106.4gを加えた後、70℃で5時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水70gを加えて50%硫酸でpHを2に調整した。生じた上層を減圧しながら加熱して内温140℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物64gを高粘性の褐色油として得た(赤外吸収スペクトル(KBr錠剤法)2930、2859、1761、1170、1115cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表3にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた500mLの反応器に、1,10−デカンジオールジグリシジルエーテル45.0g(0.157モル)、マロン酸ジメチル49.8g(0.377モル)、カリウムt−ブトキシド3.5g、t−ブチルアルコ−ル50.0gを仕込み、12時間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム69.1gを加えた後、70℃で3時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水90gを加えて50%硫酸でpHを2に調整した。生じた上層を脱水し、減圧しながら加熱して内温130℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物43gを高粘性の黄色油として得た(赤外吸収スペクトル(ATR法)2924、2855、1761、1115cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表4にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた500mLの反応器に、ポリプロピレングリコール400ジグリシジルエーテル120.0g(0.224モル)、マロン酸ジメチル70.9g(0.537モル)、カリウムt−ブトキシド5.0g、t−ブチルアルコ−ル60.0gを仕込み、10時間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム98.5gを加えた後、70℃で3時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水120gを加えて50%硫酸でpHを3に調整した。生じた上層を脱水し、減圧しながら加熱して内温130℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物75gを高粘性の褐色油として得た(赤外吸収スペクトル(ATR法)2970、2870、1763、1092cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表5にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた500mLの反応器に、ポリエチレングリコール400ジグリシジルエーテル120.0g(0.228モル)、マロン酸ジメチル72.2g(0.547モル)、カリウムt−ブトキシド5.1g、t−ブチルアルコ−ル60.0gを仕込み、12時間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム100.3gを加えた後、70℃で3時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水120gを加えて50%硫酸でpHを3に調整した。生じた上層を脱水し、減圧しながら加熱して内温130℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物60gを高粘性の黄色油として得た(赤外吸収スペクトル(ATR法)2866、1763、1094cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表6にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた500mLの反応器に、ポリテトラメチレングリコール650ジグリシジルエーテル120.0g(0.154モル)、マロン酸ジメチル48.8g(0.370モル)、カリウムt−ブトキシド3.5g、t−ブチルアルコ−ル60.0gを仕込み、12時間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム67.8gを加えた後、70℃で3時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水120gを加えて50%硫酸でpHを3に調整した。生じた上層を脱水し、減圧しながら加熱して内温130℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物73gを高粘性の黄色油として得た(赤外吸収スペクトル(ATR法)2938、2855、1767、1103cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表7にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた200mLの反応器に、1,4−シクロヘキサンジメタノールジグリシジルエーテル30.0g(0.117モル)、マロン酸ジメチル37.2g(0.281モル)、カリウムt−ブトキシド2.6g、t−ブチルアルコ−ル5.3gを仕込み、5間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム53.4gを加えた後、70℃で18時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水20gを加えて50%硫酸でpHを2に調整した。生じた上層を減圧しながら加熱して内温140℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物17gを高粘性の黄色油として得た(赤外吸収スペクトル(ATR法)2916、2855、1759、1121cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表8にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた200mLの反応器に、水添ビスフェノールAジグリシジルエーテル30.0g(0.085モル)、マロン酸ジメチル26.9g(0.204モル)、カリウムt−ブトキシド1.9g、t−ブチルアルコ−ル3.8gを仕込み、5間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム35.7gを加えた後、70℃で18時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水41gを加えて50%硫酸でpHを2に調整した。トルエン、IPAを加えて、、得られた上層を濃縮して、内温140℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物15gを白色の固体として得た(赤外吸収スペクトル(KBr錠剤法)2936、2860、1763、1101cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表9にその帰属を示す)。
攪拌機、温度計、ガス導入管を備えた200mLの反応器に、1.7−オクタジエンジエポキサイド20.0g(0.141モル)、マロン酸ジメチル44.6g(0.338モル)、カリウムt−ブトキシド3.2g、t−ブチルアルコ−ル6.4gを仕込み、12時間還流反応させた。得られた反応液を室温に戻して水で希釈し、48%水酸化ナトリウム59.1gを加えた後、70℃で4時間加水分解を行った。その後、t−ブチルアルコールを減圧にて回収し、水40gを加えて50%硫酸でpHを2に調整した。得られた固体相を減圧しながら加熱して内温160℃まで昇温し、脱炭酸/脱水閉環を行い、目的物の化合物17.5gを黄色の固形物として得た(赤外吸収スペクトル(KBr錠剤法)2938、2862、1748、1180、995cm−1)。本化合物について1H−NMRスペクトルにて構造確認を行ったところ、下記構造式で表される化合物であることを確認した(式中に1H−NMRスペクトルの帰属番号を、表10にその帰属を示す)。
表11、表12の組成で、合成例1〜10の化合物を配合した毛髪化粧料を作製した(実施例1〜10)。また比較としてビスラクトン誘導体を含有しない毛髪化粧料を作製した(比較例1)。これらの毛髪化粧料を用いて、毛髪のハリコシ改善効果を評価した。試験方法は以下のように行った。結果は表13に記載した。
(試験方法)
健常黒髪人毛に市販ブリーチ剤にてブリーチ処理を1回行い、損傷毛の毛束を作製した。次に損傷毛の毛束3gに実施例1の毛髪化粧料0.5gを均一に塗布後、風乾し毛束A1とした。毛束A1の一部はドライヤーの温風で3分間熱処理し、毛束B1とした。また、毛束B1の一部は、さらにラウレス硫酸Na3%水溶液にて洗浄、水洗を5回繰り返した後、風乾し毛束C1とした。同様にして、実施例2の毛髪化粧料を用いて毛束A2〜C2を、実施例3の毛髪化粧料を用いて毛束A3〜C3、実施例4の毛髪化粧料を用いて毛束A4〜C4を、実施例5の毛髪化粧料を用いて毛束A5〜C5、実施例6の毛髪化粧料を用いて毛束A6〜C6を、実施例7の毛髪化粧料を用いて毛束A7〜C7、実施例8の毛髪化粧料を用いて毛束A8〜C8を、実施例9の毛髪化粧料を用いて毛束A9〜C9、実施例10の毛髪化粧料を用いて毛束A10〜C10を、比較例1の毛髪化粧料を用いて毛束A11〜C11を作製した。作製したそれぞれの毛束について、官能評価(パネラー7名)にて毛髪のハリコシ改善効果を評価した。
実施例1〜10の毛髪化粧料を用いて毛髪のくせ付け評価を行った。比較としてビスラクトン誘導体を含有しない比較例1の毛髪化粧料を用いた。試験方法は以下のように行った。結果は表14に記載した。
(試験方法)
長さ25cmにカットした健常黒髪人毛に市販ブリーチ剤にてブリーチ処理を2回行い、損傷毛の毛束を作製した。次に作製した毛束3gに実施例1〜10又は比較例1の毛髪化粧料0.5gを均一に塗布し、風乾した。その後、ホットカーラー(PANASONIC社製
EH 9402P、大大カーラー直径30mm)を用いて10分間加熱(約60℃)し、毛束にカールを施した。このようにして得られたカール処理毛について、処理直後、および、恒温恒湿下(40℃、70%)で1時間放置させた後のカールのかかり度合いを目視および触診で評価した(パネラー7名)。なお、毛髪化粧料を未塗布の毛束についても同様の処理を行い、比較対照とした。
合成例1〜10の化合物について、アミノ基との反応性を試験した。試験は以下のように行い、結果を表15に示した。
(試験方法)
ステアリルアミン10mg(0.037ミリモル)、合成例1の化合物8.4mg(0.025ミリモル)、シクロヘキサン100μLを試験管内で均一に溶解し、ブロックヒーターにて60℃、80℃、120℃の各温度で15分間加熱した。その後、減圧にて温度をかけずに乾燥させ、得られた残渣について赤外吸収スペクトル(KBr錠剤法)を測定し、ラクトン由来の1760〜1780cm−1付近のピーク及びアミド由来の1635cm−1付近のピークの変化を確認した。合成例2〜10についても同様にして試験を実施した。
本発明のビスラクトン誘導体と毛髪との反応性について試験した。試験は以下のように行い、結果を表16に示した。
(試験方法)
健常黒髪人毛を市販ブリーチ剤にて1回処理を行い、損傷毛の毛束を作製した。作製した損傷毛の毛束1gに、合成例1〜10の化合物の1%エタノール溶液0.2gを均一に塗布して風乾した。得られた毛束についてヘアアイロン(泉精器製作所社製、商品名Allure)を用いて、アタッチメントをストレートタイプとして、80℃、100℃、120℃の各温度で、30秒の熱処理を2回施した。熱処理前後の毛束について、赤外吸収スペクトル(ATR法)を測定し、ラクトン由来の1760〜1780cm−1付近のピークの有無を確認した。なお、合成例1〜10の化合物を塗布する前の毛束では、ラクトンのピークは確認されなかった。
下記処方のヘアミストを調製した。このヘアミストは、べたつかず、毛髪につるつるとした良好な感触とハリコシ感を付与することができるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例1の化合物 0.60
SUCRAPH AG−8(日本精化) 0.30
ジメチコン 0.10
セトリモニウムクロリド(30%) 6.00
エタノール 8.00
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に撹拌、混合した。
下記処方のヘアエッセンスを調製した。このヘアエッセンスは、さっぱりとした感触で、べたつかず、毛髪にハリコシ感を付与できるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2の化合物 0.70
シクロヘキサン−1,4−ジカルボン酸
ビスエトキシジグリコール 1.00
セタノール 1.00
ステアルトリモニウムクロリド(63%) 0.80
ジココジモニウムクロリド(75%) 2.80
テトラオレイン酸ソルベス−60 1.00
PEG−40水添ヒマシ油 0.20
B部
メチルパラベン 0.10
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温して溶解させた。別の容器にB部をとり、約80℃に加温して溶解させた。A部にB部を徐々に加えて均一に混合した。
下記処方のヘアローションを調製した。このヘアローションは、散布することで、メントールの爽快感が持続し、頭皮を健やかに保つものであり、毛髪にハリコシを与えるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1の化合物 0.50
PEG−4 3.00
メントール 0.05
エタノール 50.0
B部
ピリドキシンHCl 0.10
グリチルリチン酸2K 0.10
BG 3.00
パンテノール 2.00
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部各成分を混合する(A部)。B部各成分を混合する(B部)。A部にB部を加え、均一に混合させる。
下記処方の寝癖直しを調製した。この寝癖直しは、毛髪に散布することで、すべり、まとまりが向上し、しっとり感、ハリコシ感を付与することができた。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例1の化合物 0.60
N−メチルピロリドン 2.00
グリセリン 2.00
ペンチレングリコール 2.00
ベヘントリモニウムクロリド(80%) 0.60
エタノール 20.0
ジメチコンプロピルPGベタイン 1.00
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
全成分を均一に溶解させる。
下記処方のヘアクリームを調製した。このヘアクリームは、艶があり、べたつかず、毛髪の水分を保ち、つるつるとした良好な感触を付与し、毛髪にハリコシ感を与えるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例3の化合物 13.00
セタノール 4.00
ジメチコン(500cs) 5.00
ステアリン酸グリセリル 4.80
オレス−10リン酸 1.80
ステアリン酸グリセリル(SE) 1.90
B部
フェノキシエタノール 0.40
メチルパラベン 0.20
10%NaOH 0.60
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、溶解させた。別容器にB部を加え、約80℃に加温し、溶解させた。A部にB部を加え撹拌混合した。
下記処方のヘアワックスを調製した。このヘアワックスは、べたつかず、髪への密着性がよくセット性に優れ、セットの持続性が高いものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
マイクロクリスタリンワックス 12.00
トリエチルヘキサノイン 5.00
キャンデリラロウ 6.00
ヒドロキシステアリン酸 4.00
ステアリン酸グリセリル(レオドール MS−60) 1.00
ステアリン酸グリセリル(ニッコールMGS−BSE) 1.00
べへネス−2 4.00
べへネス−20 10.00
合成例2の化合物 4.00
フェノキシエタノール 0.60
メチルパラベン 0.20
BG 3.00
B部
アルコックス Z−240(明成化学) 0.20
精製水 合計で100となる量
C部
クエン酸(1%) 適量
クエン酸Na(1%) 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合する。A部にB部を攪拌しながら徐々に加え、均一に混合した後、冷却する(D部)。D部にC部を加えpHを6に調整する。
下記処方のヘアワックスを調製した。このヘアミストワックスは、べたつかず、髪への密着性がよくセット性およびセットの持続性に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
PEG−8 1.00
PEG−6、PEG−32 2.00
ソルビトール 0.50
エタノール 35.00
合成例1の化合物 7.00
フェノキシエタノール 0.60
(アクリル酸アルキル/ジアセトンアクリルアミド)
コポリマーAMP 1.20
クエン酸Na(1%) 適量
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に撹拌、混合し、pHを6に調整する。
下記処方のムースを調製した。このムースはつるつるとした良好な使用感と軽い仕上がりでセット性及びセットの持続性があるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(原液処方)
合成例3の化合物 1.50
エタノール 5.00
オレス−20 1.00
アクリル樹脂アルカノールアミン液 2.00
ユカフォーマーAM75W(三菱化学社製) 1.00
ステアリン酸ジエチルアミノエチルアミド 0.50
ピロリドンカルボン酸 0.20
POE、POP変性シリコーン 1.00
防腐剤、香料 適量
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に攪拌混合する。
上記原液:石油液化ガス=92:8の割合で混合し、噴射型ムースとした。
下記処方のヘアスプレーを調製した。このヘアスプレーは、良好な使用感とセット性があり、髪につやとうるおい、セットの持続性を付与する等の感触向上が得られる。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(原液処方)
A部
合成例1の化合物 3.00
Plandool−G(日本精化) 1.00
LUSPLAN DA−R(日本精化) 2.00
B部
PEG水添ヒマシ油 0.02
C部
香料 0.05
エタノール(無水) 合計で全量100となる量
(充填処方)
原液 55.00
LPG 45.00
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部にB部を添加する(D部)。D部にC部を添加・混合し、この原液を缶に充填後、ガスを充填した。
下記処方のスタイリングジェルを調製した。このスタイリングジェルは、毛髪に塗布すると、べたつかず、動いてもばらけず、毛束感があり、セットの持続性に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 STRUCTURE 2001(アクゾノーベル社製) 5.00
2 TEA(50%) 3.50
3 AMPHOMER SH30(アクゾノーベル社製) 3.00
4 エタノール(95%) 3.00
5 メチルイソチアゾリンオン 0.01
6 合成例1の化合物 4.00
7 グリコール酸 適量
8 TEA 適量
9 精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
No.9にNo.6を加温溶解させ、次いでNo.2、No.5を溶解させる(A部)。A部にNo.1を徐々に加え、均一に混合させる(B部)。No.3をNo.4に溶解させ、40℃に冷却したB部に混合しながら徐々に加え、均一に溶解させる。No.7又はNo.8でpHを7.0〜7.5に調整する。
下記処方のシャンプーを調製した。このシャンプーは、軋みを抑え、毛髪にしっとり感を付与し、なめらかな指通りとハリコシ感を付与することができるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1の化合物 1.00
ココイルグルタミン酸TEA(30%) 50.00
テトラデセンスルホン酸Na(36%) 15.00
ジステアリン酸PEG−150 5.00
メチルパラベン 0.20
フェノキシエタノール 0.50
プロピレングリコール 1.00
(エイコサン二酸/テトラデカン二酸)
ポリグリセリル−10(日本精化) 1.00
B部
カチオン化グアーガム 0.20
精製水 合計で100となる量
C部
リン酸(10%) 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。B部にA部を加え、均一に混合した後、冷却した(D部)。D部にC部を加えpHを6〜6.5に調整した。
下記処方のリンスインシャンプーを調製した。このリンスインシャンプーは、毛髪にしっとり感を付与し、なめらかな指通りとハリコシ感を付与することができるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例3の化合物 0.90
コカミドプロピルベタイン(30%) 20.00
ラウリル硫酸TEA(40%) 15.00
コカミドDEA 2.00
ココイルグルタミン酸TEA(30%) 30.00
ジステアリン酸エチレングリコール 1.20
ポリクオタニウム−10 1.60
ステアリルトリモニウムブロミド(70%) 0.60
フェノキシエタノール 0.20
B部
メチルパラベン 0.20
安息香酸Na 0.40
精製水 全量100でとなる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。B部にA部を加え、均一に混合した後、冷却した。
下記処方のヘアカラー用シャンプーを調製した。このヘアカラー用シャンプーは、ヘアカラーの色落ちを抑制し、髪につや、しっとり感を付与する等の感触向上及び持続効果が得られる。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
ポリ(HEMAグルコシド)(20%) 4.00
合成例1の化合物 1.50
ココイルメチルタウリンNa(30%) 15.00
オレフィン(C14−16)スルホン酸Na(36%) 13.00
ココアンホ酢酸Na(30%) 8.00
PPG−12−PEG−50ラノリン 2.50
ココイルグルタミン酸(30%) 7.00
ポリクオタニウム−10 1.00
ラウラミドプロピルヒドロキシスルタイン/水 4.00
PEG−20水添ヒマシ油 2.00
エチドロン酸 0.20
PG 0.20
ベンジルアルコール 2.00
メチルパラベン 0.20
フェノキシエタノール 0.20
精製水 全量100でとなる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
全成分を均とり、80℃に加温し均一に撹拌、混合後冷却した。
下記処方のリンスを調製した。このリンスは、毛髪にしっとり感、艶を付与し、なめらかな指通り、ハリコシ感を付与することができるリンスであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1の化合物 15.00
Plandool−H(日本精化) 0.50
セトリモニウムクロリド(30%) 5.20
オクチルドデカノール 4.70
セタノール 2.80
ステアルトリモニウムクロリド(63%) 0.60
セバシン酸ジエチルヘキシル(日本精化) 0.70
スクワラン 0.30
ミリスチル硫酸Na 0.20
セテス−40 0.10
オレス−5 0.10
セチル硫酸Na 0.10
B部
クエン酸 0.10
メチルパラベン 0.10
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、溶解させた。B部を約80℃に加温し溶解させた。A部にB部を攪拌しながら、徐々に加え均一に混合し、攪拌した後、急冷した。
下記処方のトリートメントを調製した。このトリートメントは、毛髪にしっとり感、ハリコシ感を付与することができるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2の化合物 1.80
ベヘントリモニウムクロリド(80%) 2.40
セタノール 5.20
ステアリン酸グリセリル 1.20
LUSPLAN DA−R(日本精化) 0.40
ジメチコン 2.00
(アミノエチルアミノプロピルメチコン/ジメチコン)
コポリマー 0.50
B部
メチルパラベン 0.10
プロピルパラベン 0.10
精製水 合計で100となる量
C部
アデノシン一リン酸(10%) 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。A部にB部を攪拌しながら徐々に加え、均一に混合した後、冷却した(D部)。D部にC部を加えpHを5.2〜5.7に調整した。
下記処方のトリートメントを調製した。このトリートメントは、毛髪にハリコシ感、つるっとした感触を付与できるトリートメントであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例1の化合物 7.00
ステアルトリモニウムクロリド(63%) 3.80
ステアルトリモニウムブロミド(70%) 1.00
セテス−18 0.80
オレイルアルコール 3.00
セタノール 4.00
LUSPLAN DD−DA5(日本精化) 0.60
ステアリン酸ジメチルアミノプロピルアミド 2.00
B部
加水分解コラーゲン(日本精化) 1.00
クエン酸 適量
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温した。別容器にB部を加え、加温し、溶解させた。攪拌しながらB部にA部を徐々に加え、均一に混合し、1分間攪拌後急冷した。
下記処方の洗い流さないヘアトリートメントを調製した。このヘアトリートメントは、毛髪のすべり、まとまり、指通り、しっとり感、ハリコシ感が向上するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例3の化合物 2.50
シクロヘキサン−1,4−ジカルボン酸
ビスエトキシジグリコール 2.00
セトリモニウムクロリド(25%) 3.80
カプリリルグルコシド(50%) 0.80
グリセリン 4.00
フェノキシエタノール 0.20
B部
エタノール 20.00
C部
ポリクオタニウム−6 0.60
ポリクオタニウム−7 0.40
シロキクラゲ多糖体 0.05
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
C部を約80℃に加温し、溶解させた。次にA部を約80℃に加温し溶解させた。C部を攪拌しながらA部加え、均一に混合後、約40℃まで冷却させた。次いで、B部を加え、均一に混合させた。
下記処方のリーブオントリートメント(毛髪用)を調製した。このリーブオントリートメント(毛髪用)は、毛髪にしっとり感とすべり感、ハリコシ感を付与できるものであった。また、安定性も良好であった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2の化合物 3.00
セバシン酸ジエチル 1.00
ミリスチルアルコール 5.00
ベヘニルアルコール 1.00
オレイルアルコール 1.00
ステアリン酸ジメチルプロピルアミド 2.00
ココアンホ酢酸Na(30%) 2.00
ステアリン酸グリセリル 0.40
ミリスチン酸 0.60
フェノキシエタノール 0.40
B部
乳酸 0.60
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、均一に溶解させた。B部を約80℃に加温し、溶解させた。A部にB部を徐々に加え、均一に混合した。
下記処方のリーブオントリートメント(毛髪用)を調製した。このリーブオントリートメント(毛髪用)は、毛髪にしなやかさとしっとり感を付与できるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例2の化合物 5.50
パルミチン酸イソプロピル 4.00
セタノール 5.00
ステアルトリモニウムクロリド(63%) 3.20
ベヘントリモニウムクロリド(80%) 1.00
スクワラン 1.00
グリセリン 1.00
B部
メチルパラベン 0.10
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、溶解させた。B部を約80℃に加温し、溶解させた。A部にB部を徐々に加えて均一に混合した。
下記処方の育毛剤を調製した。この育毛剤は、髪に弾力を与え、脱毛、ふけ、かゆみを防止できるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例3の化合物 0.80
メントール 0.10
トウガラシチンキ 0.50
センブリエキス 2.00
エタノール 30.00
防腐剤 適量
香料 適量
PPG−6デシルテトラデセス−30 0.30
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
各成分を均一に撹拌混合した。
下記処方の酸性染毛料を調製した。この酸性染毛料は、毛髪に施術することにより、染色性が良く、毛髪にハリコシ感、すべり感等の良好な感触を付与できる酸性染毛剤であった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例1の化合物 2.00
N−メチルピロリドン 5.00
ベンジルアルコール 5.00
クエン酸 1.00
褐色201号 0.13
黒色401号 0.05
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を加温、溶解し均一に混合した。
下記処方の酸性染毛料を調製した。この毛髪脱色剤(2剤式)は、毛髪に施術することにより、脱色後の毛髪の損傷感を低減し、ハリコシ感、すべり感等の良好な感触を付与できる脱色剤であった。
(1剤)
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例2の化合物 3.00
ポリオキシエチレンオレイルエーテル 52.00
アンモニア水(25%) 25.50
セトリモニウムクロリド(30%) 10.00
エタノール 10.00
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に攪拌、混合した。
(2剤)
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
過酸化水素水 17.00
セトリモニウムクロリド(30%) 10.00
セタノール 3.00
セテス−2 1.00
セテス−20 1.00
ピロリン酸Na 0.10
ジエチレントリアミン五酢酸 0.10
クエン酸(50%) 適量
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に混合し、クエン酸でpHを3.5〜4.0に調整した。
(配合比)
1剤:2剤=1:7
下記処方の酸化染毛剤を調製した。この酸化染毛剤は、毛髪に施術することにより、毛髪にしっとり感、ハリコシ感等の良好な感触を付与できる酸化染毛剤であった。
(1剤)
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例3の化合物 5.00
セトリモニウムクロリド(25%) 24.00
セタノール 9.00
オクチルドデカノール 9.00
モノエタノールアミン 3.80
アンモニア水 2.00
ミリスチル硫酸Na 1.50
オレス−20 1.40
塩酸トルエン−2,5−ジアミン 1.00
レゾルシン 1.00
メタアミノフェノール 0.50
パラアミノフェノール 0.20
オルトアミノフェノール 0.10
アスコルビン酸 0.20
香料 0.10
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に混合した。
(2剤)
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
過酸化水素水 17.00
セトリモニウムクロリド(25%) 10.00
セタノール 3.00
オレス−2 1.00
オレス−20 1.00
ピロリン酸Na 0.10
ジエチレントリアミン五酢酸 0.10
クエン酸(50%) 適量
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に混合し、クエン酸でpHを3.5〜4.0に調整した。
(配合比)
1剤:2剤=1:1
下記処方のプレパーマ液を調製した。このプレパーマ液は、パーマネント処理前に毛髪に塗布することにより、毛髪ダメージの抑制ができ、パーマのかかり、持ちが向上することができるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例1の化合物 3.00
4−エトキシメチル−1,3−ジオキソラン−2−オン 1.00
カチオンNH(日本精化) 0.80
カプリリルグルコシド(50%) 1.00
クエン酸 適量
クエン酸Na 適量
メチルパラベン 0.20
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に溶解させる。
下記処方のパーマ剤を調製した。このパーマ剤は、毛髪に施術することにより、毛髪にすべり感、ハリコシ感を与えるパーマ剤であった。
(1液)
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 合成例3の化合物 1.00
2 ポリクオタニウム−22 2.00
3 アルギニン 0.30
4 モノエタノールアミン 1.00
5 アンモニア水(28%) 1.00
6 PEG−50水添ヒマシ油 0.20
7 炭酸水素アンモニウム 2.00
8 リン酸2Na 0.50
9 チオグリコール酸アンモニウム水溶液(50%) 11.50
10 システイン 1.50
11 EDTA−4Na 0.15
12 水酸化Na 0.25
13 ポリクオタニウム−10 0.10
14 精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
No.14の大部分にNo.12を溶解させ、次いでNo.13を少量ずつ加えて溶解させ、さらにNo.9〜11を加え溶解させた(A部)。別容器にNo.14の残りをとり、No.7、8を加え、加温、溶解させた(B部)。別容器にNo.1〜6を加え、約50℃に加温し、溶解させた(C部)。A部にB部を加え、均一に混合させた後、C部を徐々に加え、均一に混合した。
(2液)
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 合成例2の化合物 0.10
2 安息香酸Na 0.20
3 エデト酸2Na 0.10
4 リン酸二アンモニウム 0.10
5 エマコールTS−703(山栄化学) 2.00
6 ステアリルトリモニウムクロリド(50%) 2.00
7 臭素酸Na 10.00
8 エマコールNZ(山栄化学) 4.00
9 オレス−20 3.00
10 精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
No.10の大部分をとり、約60℃に加温し、No.1〜3を加え溶解させた後No.4を加え溶解させた。次いでNo.5、6を加え、加温、溶解させ、徐冷しながら40℃付近でNo.7〜9を加え均一にさせた。残りのNo.10を加え、均一に混合し、冷却した。
下記処方のヘアミストを調製した。このヘアミストは、ドライヤーで加熱する前に塗布することにより、毛髪にハリコシ感、すべり感等の良好な感触を付与し、その効果が長く持続するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成例4の化合物 0.30
SUCRAPH AG−8(日本精化) 0.30
ポリクオタニウムー10 0.20
べヘンセトリモニウムクロリド(80%) 3.00
ポリクオタニウムー7 0.20
エタノール 3.00
ジメチコン(50cs) 0.50
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に撹拌、混合した。
下記処方のリーブオントリートメント(毛髪用)を調製した。このリーブオントリートメント(毛髪用)は、ヘアカーラーで加熱する前に塗布することにより、毛髪のくせ付けが改善され、またハリコシ感、すべり感等の良好な感触を付与し、その効果が長く持続するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例5の化合物 3.50
セバシン酸エチルヘキシル 6.00
ステアリルアルコール 4.00
ステアルトリモニウムクロリド(63%) 3.00
ベヘントリモニウムクロリド(80%) 1.00
スクワラン 1.00
グリセリン 1.00
B部
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、溶解させた。B部を約80℃に加温した。A部にB部を徐々に加えて均一に混合した。
下記処方のトリートメントを調製した。このトリートメントは、ドライヤーで加熱する前に塗布することにより、毛髪にハリコシ感、しっとり感等の良好な感触を付与するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例6の化合物 1.00
ステアルトリモニウムクロリド(63%) 2.50
セタノール 4.00
LUSPLAN SR−DM4(日本精化) 0.50
ネオペンタン酸イソデシル 2.00
シクロヘキサン−1,4−ジカルボン酸
ビスエトキシジグリコール(日本精化) 0.50
グリセリン 3.00
B部
プロピルパラベン 0.10
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。A部にB部を攪拌しながら徐々に加え、均一に混合した後、冷却した。
下記処方のシャンプーを調製した。このシャンプーは、軋みを抑え、毛髪にしっとり感を付与し、なめらかな指通りとハリコシ感を付与することができるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例7の化合物 0.50
コカミドプロピルベタイン(30%) 20.00
ラウレス硫酸Na(27%) 38.00
ラウラミドDEA 2.50
メチルパラベン 0.20
フェノキシエタノール 0.50
シクロヘキサン−1,4−ジカルボン酸
ビスエトキシジグリコール(日本精化) 0.50
ジステアリン酸グリコール 1.50
B部
ポリクオタニウム−10 1.50
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部、B部をそれぞれとり、約80℃に加温し、均一に混合した。B部にA部を加え、均一に混合した後、冷却した。
下記処方のヘアミストを調製した。このヘアミストは、ヘアカーラーで加熱する前に塗布することにより、毛髪のくせ付けが改善され、またハリコシ感、すべり感等の良好な感触を付与し、その効果が長く持続するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
合成8の化合物 0.10
SUCRAPH AG−8(日本精化) 0.30
ジステアリルジモニウムクロリド(96%) 1.00
PEG−12ジメチコン 1.00
コレステロール 0.05
エタノール 8.00
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
各成分を均一に撹拌、混合した。
下記処方のリーブオントリートメント(毛髪用)を調製した。このリーブオントリートメント(毛髪用)は、毛髪にしっとり感とすべり感、ハリコシ感を付与できるものであった。また、安定性も良好であった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例9の化合物 1.00
セバシン酸ジエチルヘキシル 1.00
セタノール 2.00
ベヘニルアルコール 1.00
ステアリン酸ジメチルプロピルアミド 2.00
ステアリン酸グリセリル 0.40
Plandool−LG2(日本精化) 0.10
フェノキシエタノール 0.40
B部
乳酸 0.60
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、均一に溶解させた。B部を約80℃に加温し、溶解させた。A部にB部を徐々に加え、均一に混合した。
下記処方のトリートメントを調製した。このトリートメントは、ヘアカーラーで加熱する前に塗布することにより、毛髪のくせ付けが改善され、またハリコシ感、すべり感等の良好な感触を付与し、その効果が長く持続するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
A部
合成例10の化合物 0.50
エチルヘキサン酸セチル 1.00
セトステアリルアルコール 3.80
ジステアリルジモニウムクロリド(96%) 2.00
セトリモニウムクロリド(70%) 0.50
ステアリン酸グリセリル 0.50
Plandool−H(日本精化) 0.10
ジメチコン(100万cs) 0.50
フェノキシエタノール 0.40
B部
精製水 合計で100となる量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
A部を約80℃に加温し、均一に溶解させた。B部を約80℃に加温し、溶解させた。A部にB部を徐々に加え、均一に混合した。
Claims (4)
- 下記の一般式(2)で表される化合物を含有することを特徴とする化粧料。
- 請求項1の一般式(2)で表される化合物、又は、請求項2の一般式(4)で表される化合物を含有することを特徴とする毛髪化粧料。
- 塗布後に毛髪に加熱処理を施すことを特徴とする請求項3に記載の毛髪化粧料。
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