JP5528349B2 - アミンの製造方法 - Google Patents
アミンの製造方法 Download PDFInfo
- Publication number
- JP5528349B2 JP5528349B2 JP2010538578A JP2010538578A JP5528349B2 JP 5528349 B2 JP5528349 B2 JP 5528349B2 JP 2010538578 A JP2010538578 A JP 2010538578A JP 2010538578 A JP2010538578 A JP 2010538578A JP 5528349 B2 JP5528349 B2 JP 5528349B2
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- weight
- range
- process according
- calculated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/835—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with germanium, tin or lead
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/002—Mixed oxides other than spinels, e.g. perovskite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/03—Precipitation; Co-precipitation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/16—Reducing
- B01J37/18—Reducing with gases containing free hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
- C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/06—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by halogen atoms or nitro radicals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07150408 | 2007-12-21 | ||
| EP07150408.8 | 2007-12-21 | ||
| PCT/EP2008/067183 WO2009080507A1 (de) | 2007-12-21 | 2008-12-10 | Verfahren zur herstellung eines amins |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011506529A JP2011506529A (ja) | 2011-03-03 |
| JP2011506529A5 JP2011506529A5 (https=) | 2012-02-02 |
| JP5528349B2 true JP5528349B2 (ja) | 2014-06-25 |
Family
ID=40383837
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010538578A Expired - Fee Related JP5528349B2 (ja) | 2007-12-21 | 2008-12-10 | アミンの製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8278489B2 (https=) |
| EP (1) | EP2225029B1 (https=) |
| JP (1) | JP5528349B2 (https=) |
| CN (1) | CN101903095B (https=) |
| TW (1) | TW200936547A (https=) |
| WO (1) | WO2009080507A1 (https=) |
Families Citing this family (32)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2009104740A (ru) * | 2006-07-14 | 2010-08-27 | Басф Се (De) | Способ получения амина |
| ATE553844T1 (de) * | 2007-12-21 | 2012-05-15 | Basf Se | Verfahren zur herstellung eines amins |
| EP2234717A1 (de) * | 2007-12-21 | 2010-10-06 | Basf Se | Verfahren zur herstellung eines amins |
| US8293945B2 (en) * | 2007-12-21 | 2012-10-23 | Basf Se | Method for producing an amine |
| CN102159311B (zh) * | 2008-09-19 | 2013-07-10 | 巴斯夫欧洲公司 | 使用铝-铜催化剂连续制备胺的方法 |
| WO2010052181A2 (de) | 2008-11-05 | 2010-05-14 | Basf Se | Verfahren zur herstellung von n,n-substituierten-3-aminopropan-1-olen |
| WO2010069856A1 (de) | 2008-12-19 | 2010-06-24 | Basf Se | Verfahren zur herstellung von reinem triethanolamin (teoa) |
| DE102008063308B4 (de) | 2008-12-29 | 2013-03-07 | Basf Se | Verfahren zur Herstellung von Toluylendiamin durch Hydrierung von Dinitrotoluol |
| JP2012526741A (ja) | 2009-05-14 | 2012-11-01 | ビーエーエスエフ ソシエタス・ヨーロピア | 芳香族アミンの製造方法 |
| CN102548952B (zh) | 2009-07-10 | 2014-05-14 | 巴斯夫欧洲公司 | 在电化学分离氢气的情况下将烃直接胺化成氨基烃的方法 |
| PT2451770E (pt) | 2009-07-10 | 2015-03-04 | Basf Se | Processo para a aminação direta de hidrocarbonetos em amino-hidrocarbonetos com a separação eletroquímica de hidrogénio e a transformação eletroquímica do hidrogénio em água |
| EP2506966B1 (de) | 2009-12-03 | 2017-08-16 | Basf Se | Katalysator und verfahren zur herstellung eines amins |
| EP2506965B1 (de) | 2009-12-03 | 2016-11-09 | Basf Se | Katalysator und verfahren zur herstellung eines amins |
| US8637668B2 (en) | 2010-06-15 | 2014-01-28 | Basf Se | Process for preparing a cyclic tertiary methylamine |
| US8933223B2 (en) | 2010-10-14 | 2015-01-13 | Basf Se | Process for preparing a cyclic tertiary amine |
| JP5879123B2 (ja) * | 2011-12-27 | 2016-03-08 | 花王株式会社 | 3級アミンの製造方法 |
| WO2013178534A1 (de) | 2012-06-01 | 2013-12-05 | Basf Se | Verfahren zur herstellung eines mono-n-alkyl-piperazins |
| US8884015B2 (en) | 2012-06-01 | 2014-11-11 | Basf Se | Process for the preparation of a mono-N-alkypiperazine |
| WO2013178693A1 (de) | 2012-06-01 | 2013-12-05 | Basf Se | Verfahren zur herstellung eines mono-n-alkyl-piperazins |
| WO2013182465A1 (de) | 2012-06-06 | 2013-12-12 | Basf Se | Verfahren zur herstellung von piperazin |
| IN2014DN09263A (https=) | 2012-06-06 | 2015-07-10 | Basf Se | |
| US8981093B2 (en) | 2012-06-06 | 2015-03-17 | Basf Se | Process for preparing piperazine |
| IN2014DN10837A (https=) | 2012-07-13 | 2015-09-04 | Basf Se | |
| US9315479B2 (en) | 2012-07-13 | 2016-04-19 | Basf Se | Process for preparing pyrrolidine |
| WO2014184039A1 (de) | 2013-05-16 | 2014-11-20 | Basf Se | Verfahren zur herstellung von n-alkyl-piperazinen |
| CN111433183B (zh) | 2017-11-30 | 2023-12-22 | 巴斯夫欧洲公司 | 连续制备1,2-丙二胺和二甲基二亚乙基三胺的方法 |
| CN111801319A (zh) * | 2018-03-15 | 2020-10-20 | 巴斯夫欧洲公司 | 从包含甲氧基乙醇和吗啉的混合物中移除甲氧基乙醇的方法 |
| US20230025575A1 (en) * | 2019-12-03 | 2023-01-26 | Basf Se | Process for preparing amines over a copper catalyst |
| CN111118899A (zh) * | 2019-12-26 | 2020-05-08 | 安徽元琛环保科技股份有限公司 | 一种滤料用抗硫酸氢铵整理剂的制备方法与应用 |
| EP4463435A1 (en) | 2022-01-14 | 2024-11-20 | Basf Se | Method for the manufacture or conversion of alkanolamines |
| CN117358239B (zh) * | 2022-06-30 | 2026-02-03 | 中国石油化工股份有限公司 | 烷基二胺的制备方法 |
| WO2025157662A1 (en) * | 2024-01-26 | 2025-07-31 | Basf Se | Process for the manufacture of chemical products and passivation of heterogeneous metal catalysts |
Family Cites Families (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL296139A (https=) | 1963-08-02 | |||
| NL169595C (nl) | 1970-05-21 | 1982-08-02 | Shell Int Research | Werkwijze voor de bereiding van aminen en van smeerolien en vloeibare motorbrandstoffen die deze bevatten. |
| US3922303A (en) | 1971-02-17 | 1975-11-25 | Dai Ichi Kogyo Seiyaku Co Ltd | Process for the production of tertiary amines having higher alkyl group |
| US4152353A (en) | 1977-08-29 | 1979-05-01 | The Dow Chemical Company | Method of producing amines from alcohols, aldehydes, ketones and mixtures thereof |
| US4153581A (en) | 1977-09-01 | 1979-05-08 | The Dow Chemical Company | Method of producing amines from alcohols, aldehydes, ketones and mixtures thereof |
| US4625030A (en) | 1984-05-23 | 1986-11-25 | Union Carbide Corporation | Potentiated nickel catalysts for amination |
| DE3611230A1 (de) | 1986-04-04 | 1987-10-08 | Basf Ag | Polybutyl- und polyisobutylamine, verfahren zu deren herstellung und diese enthaltende kraft- und schmierstoffzusammensetzungen |
| DE3903367A1 (de) * | 1989-02-04 | 1990-08-16 | Basf Ag | Katalysator und verfahren zur hydrierenden aminierung von alkoholen |
| DE4116367A1 (de) * | 1991-05-18 | 1992-11-19 | Basf Ag | Verfahren zur herstellung von aminen |
| DE4428004A1 (de) | 1994-08-08 | 1996-02-15 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE4429547A1 (de) | 1994-08-19 | 1996-02-22 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE19645047A1 (de) * | 1996-10-31 | 1998-05-07 | Basf Ag | Katalysatoren für die Aminierung von Alkylenoxiden, Alkoholen, Aldehyden und Ketonen |
| DE19644107A1 (de) * | 1996-10-31 | 1998-05-07 | Basf Ag | Katalysatoren für die Aminierung von Alkylenoxiden, Alkoholen, Aldehyden und Ketonen |
| SG70081A1 (en) | 1997-05-14 | 2000-01-25 | Kuraray Co | Process for producing diamines |
| DE19742911A1 (de) | 1997-09-29 | 1999-04-01 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE19826396A1 (de) | 1998-06-12 | 1999-12-16 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE19910960A1 (de) | 1999-03-12 | 2000-09-14 | Basf Ag | Verfahren zur Herstellung von Aminen |
| WO2000069804A1 (en) | 1999-05-13 | 2000-11-23 | Symyx Technologies Inc. | Amination of aromatic hydrocarbons and heterocyclic analogs thereof |
| ATE272605T1 (de) | 1999-12-06 | 2004-08-15 | Basf Ag | Verfahren zur herstellung von aminen |
| DE10153411A1 (de) | 2001-10-30 | 2003-05-15 | Basf Ag | Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese |
| DE10153410A1 (de) | 2001-10-30 | 2003-05-15 | Basf Ag | Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese |
| US7196033B2 (en) * | 2001-12-14 | 2007-03-27 | Huntsman Petrochemical Corporation | Advances in amination catalysis |
| DE10211101A1 (de) | 2002-03-14 | 2003-09-25 | Basf Ag | Katalysatoren und Verfahren zur Herstellung von Aminen |
| DE10261193A1 (de) * | 2002-12-20 | 2004-07-01 | Basf Ag | Verfahren zur Herstellung eines Armins |
| DE102004062253A1 (de) | 2004-12-23 | 2006-07-06 | Basf Ag | Direktaminierung von Kohlenwasserstoffen |
| DE102005047458A1 (de) * | 2005-09-30 | 2007-04-12 | Basf Ag | Verfahren zur Herstellung von Aminodiglykol (ADG) und Morpholin |
| CN101460445B (zh) | 2006-05-31 | 2013-06-05 | 巴斯夫欧洲公司 | 制备胺的方法 |
| RU2009104738A (ru) | 2006-07-14 | 2010-08-27 | Басф Се (De) | Способ получения амина |
| CN101489673A (zh) | 2006-07-14 | 2009-07-22 | 巴斯夫欧洲公司 | 生产胺的方法 |
| WO2008006752A1 (de) | 2006-07-14 | 2008-01-17 | Basf Se | Verfahren zur herstellung eines amins |
| RU2009104740A (ru) | 2006-07-14 | 2010-08-27 | Басф Се (De) | Способ получения амина |
| US7919655B2 (en) | 2006-07-14 | 2011-04-05 | Basf Se | Method for producing an amine |
| US8293945B2 (en) | 2007-12-21 | 2012-10-23 | Basf Se | Method for producing an amine |
| ATE553844T1 (de) | 2007-12-21 | 2012-05-15 | Basf Se | Verfahren zur herstellung eines amins |
| EP2234717A1 (de) | 2007-12-21 | 2010-10-06 | Basf Se | Verfahren zur herstellung eines amins |
-
2008
- 2008-12-10 WO PCT/EP2008/067183 patent/WO2009080507A1/de not_active Ceased
- 2008-12-10 JP JP2010538578A patent/JP5528349B2/ja not_active Expired - Fee Related
- 2008-12-10 US US12/809,653 patent/US8278489B2/en not_active Expired - Fee Related
- 2008-12-10 EP EP08863552.9A patent/EP2225029B1/de not_active Not-in-force
- 2008-12-10 CN CN200880122274.0A patent/CN101903095B/zh not_active Expired - Fee Related
- 2008-12-19 TW TW097149918A patent/TW200936547A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US20110054167A1 (en) | 2011-03-03 |
| EP2225029B1 (de) | 2016-08-03 |
| JP2011506529A (ja) | 2011-03-03 |
| US8278489B2 (en) | 2012-10-02 |
| CN101903095A (zh) | 2010-12-01 |
| WO2009080507A1 (de) | 2009-07-02 |
| EP2225029A1 (de) | 2010-09-08 |
| CN101903095B (zh) | 2013-07-10 |
| TW200936547A (en) | 2009-09-01 |
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