JP5198329B2 - Flow rate setting method and coating apparatus - Google Patents

Description

  The present invention relates to a flow rate setting method and a coating apparatus, and more particularly to a flow rate setting method and a coating apparatus for a coating apparatus that applies a coating liquid by discharging a coating liquid from a plurality of nozzles.

  2. Description of the Related Art Conventionally, various coating apparatuses that apply a coating liquid to a target object such as a substrate have been developed. For example, in an apparatus for manufacturing an organic EL (Electro Luminescence) display device, coating is performed by applying a hole transport material or an organic EL material in a predetermined pattern shape to the main surface of a substrate such as a glass substrate placed on a stage. An apparatus is used (for example, refer to Patent Document 1). In this coating apparatus, a coating liquid (organic EL material or hole transport material) is discharged from a nozzle at a predetermined pressure. Specifically, the coating liquid is stored in a supply source such as a tank provided in the coating apparatus, the coating liquid supplied from the supply source is increased by a pump, and is discharged from the nozzle.

  In the coating apparatus, when red, green, and blue organic EL materials are applied, any one of red, green, and blue organic EL materials is simultaneously ejected from a plurality of nozzles in order to increase manufacturing efficiency. It is common to apply. For example, when a monochromatic organic EL material is simultaneously ejected from a plurality of nozzles using the coating apparatus disclosed in Patent Document 1, a coating solution stored in a single supply source (for example, a red organic EL material) There is a method in which a coating liquid is applied to a plurality of positions simultaneously by branching and supplying to a plurality of nozzles, and simultaneously applying the nozzles onto the substrate from each nozzle.

  FIG. 14 is a block diagram illustrating an example of a coating apparatus that branches and supplies a plurality of nozzles 108 a to 108 n from a single supply source 101. In FIG. 14, the coating liquid stored in the supply source 101 is increased in pressure by the pump 102 and supplied to the manifold (branch pipe) 104 through the filter 103. The manifold 104 is connected to piping of a plurality of nozzle systems (a system to n system), and flows the supplied coating liquid to the piping of the a system to n system.

  The flow rate of the coating solution flowing from the manifold 104 to the system a is controlled by the flow rate control valve 105a, and the flow rate is monitored by the flow meter 106a. Then, the coating liquid that branches and flows into the system a is discharged from the tip of the nozzle 108a through the filter 109a built in the nozzle 108a. In addition, the coating liquid that branches from the manifold 104 to the other b-line to n-line flows similarly to the a-line. In other words, the flow rate of the coating liquid that branches and flows from the manifold 104 to the b system to the n system is controlled by the flow rate control valves 105b to 105n, respectively. 106n, respectively. And each coating liquid which branches and flows into b system -n system is discharged from the tip part of the nozzles 108b-108n through filters 109b-109n built in nozzles 108b-108n, respectively.

JP 2006-205024 A

  Here, in order to discharge the coating liquid at an accurate flow rate from the nozzle, it is necessary to measure and manage the actual discharge flow rate of the coating liquid discharged from the nozzle. For example, the actual discharge flow rate of the coating liquid discharged from the nozzle is measured by the weight of the coating liquid in the container (for example, milligram / minute) with respect to the unit discharge time by discharging the coating liquid from the nozzle into a predetermined container. The And the application | coating flow volume in subsequent application | coating operations is managed using the relationship between the value of the flowmeter at the time of an actual flow measurement, and an actual discharge flow measurement result. For example, it is assumed that the values of the flowmeter when the coating liquid is discharged from the nozzle are X1, X2, and X3, and the actual discharge flow rates are Y1, Y2, and Y3, respectively. At this time, a relational expression between the value of the flow meter and the actual discharge flow rate as shown in FIG. 15 is derived. When it is desired to apply the application liquid from the nozzle at the actual discharge flow rate Yp in the application operation, the flow meter value Xp corresponding to the actual discharge flow rate Yp is calculated based on the derived relational expression, and the flow meter indicates the value Xp. To control the flow rate to the nozzle.

  However, in the case of a coating apparatus that simultaneously discharges coating liquid from a plurality of nozzles 108a to 108n as shown in FIG. 14, it is necessary to measure the actual discharge flow rate for each nozzle system and derive the above relational expressions, respectively. It becomes. Moreover, when deriving a highly accurate relational expression, it is necessary to measure actual discharge flow rates at a plurality of points with different flow rates for one nozzle system. In addition, when changing the coating liquid to be applied in the coating apparatus (for example, changing from a red organic EL material to a green organic EL material), it is necessary to measure the actual discharge flow rate even after the coating liquid is changed. The number of man-hours for managing the flow rate of the device increases. In addition, if the actual discharge flow rate measurement time of the coating apparatus becomes longer, the actual discharge flow rate may fluctuate due to evaporation of the solvent in the coating liquid discharged into the container, making it difficult to accurately measure the actual discharge flow rate. Sometimes.

  SUMMARY OF THE INVENTION Therefore, an object of the present invention is to provide a flow rate setting method for a coating apparatus and a coating apparatus that make it easy to manage the flow rate of the coating liquid discharged from each nozzle.

In order to achieve the above object, the present invention has the following features.
In the first aspect of the present invention, the coating liquid supplied from a single supply source via the main pipe is divided into a plurality of branch pipes, and the flow rate of the coating liquid flows through the branch pipes by the branch pipe flow rate measuring means provided in the branch pipes. Is a flow rate setting method of a coating liquid in a coating apparatus that discharges the coating liquid from a nozzle connected to the branch pipe. The flow rate setting method includes a series supply step and a flow rate measurement adjustment step. In the serial supply step, the branch flow rate measuring means are connected in series, the coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series, and the supplied coating liquid is discharged from one of the nozzles. Let The flow rate measurement adjusting step adjusts the measurement result of each coating liquid flow rate in the branch flow rate measuring unit in a state where the coating liquid is supplied to the branch flow rate measuring unit connected in series in the serial supply step.

  A second invention further includes a selective supply step and an actual flow rate measurement step in the first invention. In the selective supply step, the coating liquid supplied from the supply source to the main pipe is supplied only to one selected branch pipe selected from the plurality of branch pipes, and the supply of the coating liquid to the other branch pipes is closed. In the actual flow rate measurement process, in the state where the coating liquid is supplied only to the selected branch pipe in the selective supply process, the measurement result by the branch flow rate measuring means provided in the selected branch pipe and the coating liquid discharged from the nozzle of the selected branch pipe Measure the relationship between the actual discharge amount. In the flow measurement adjustment process, in the state where the supply liquid is supplied to the branch flow rate measuring means connected in series in the serial supply process, the flow rate of the application liquid measured by the branch flow rate measurement means provided in the selected branch pipe is used as a reference. The measurement result of the coating liquid flow rate in the other branch flow rate measuring means is adjusted.

  In a third aspect based on the first aspect, at least one of the branch pipe flow rate measuring means measures the mass flow rate of the coating liquid flowing through the branch pipe. In the flow measurement adjustment process, in the state where the coating liquid is supplied to the branch flow rate measuring means connected in series in the series supply process, the flow rate of the coating liquid measured by the branch flow rate measuring means for measuring the mass flow is used as a reference. The measurement result of the coating liquid flow rate in the branch pipe flow rate measuring means is adjusted.

  The fourth invention further includes a selective supply step and an actual flow rate measurement step in the first invention. In the selective supply step, the coating liquid supplied from the supply source to the main pipe is supplied only to one selected branch pipe selected from the plurality of branch pipes, and the supply of the coating liquid to the other branch pipes is closed. The actual flow rate measurement process is based on the measurement result by the main flow rate measuring means for measuring the flow rate of the coating liquid flowing through the main pipe and the nozzle of the selected branch pipe in the state where the coating liquid is supplied only to the selected branch pipe in the selective supply process The relationship between the actual discharge amount of the discharged coating liquid is measured. In the flow rate measurement adjustment process, in the state where the supply liquid is supplied to the branch flow rate measuring means connected in series in the serial supply process, the flow rate in the branch flow measurement means is based on the coating liquid flow rate measured by the main flow rate measurement means. The measurement result of each coating liquid flow rate is adjusted.

  In a fifth aspect based on the first aspect, the main pipe is provided with main pipe flow rate measuring means for measuring the mass flow rate of the coating liquid flowing through the main pipe. In the flow rate measurement adjustment process, in the state where the supply liquid is supplied to the branch flow rate measuring means connected in series in the serial supply process, the flow rate in the branch flow measurement means is based on the coating liquid flow rate measured by the main flow rate measurement means. The measurement result of each coating liquid flow rate is adjusted.

  According to a sixth invention, in any one of the first to fifth inventions, the flow rate of the coating liquid flowing through the branch pipe is adjusted to a predetermined flow rate according to the measurement result of the flow rate of the coating liquid by the branch pipe flow rate measuring means. A branch pipe flow rate adjusting means is provided in each of the plurality of branch pipes. In the serial supply step, the branch flow rate measuring means and the branch flow rate adjusting means are respectively connected in series, and the supply liquid is supplied from the supply source to the branch flow rate measuring means and the branch flow rate adjusting means connected in series. The applied coating liquid is discharged from one of the nozzles. In the flow rate measurement adjustment step, in the state where the series supply step supplies the coating liquid to the branch flow rate measurement means and the branch flow rate adjustment means connected in series, based on the measurement result of each coating liquid flow rate in the branch flow rate measurement means. Thus, a target flow rate value that is an adjustment target of the branch flow rate adjusting means corresponding to the predetermined flow rate is set.

  In a seventh aspect of the present invention based on the sixth aspect, in the flow measurement adjustment step, the serial supply step supplies the coating liquid to the branch flow rate measurement means and the branch flow rate adjustment means connected in series. A relational expression between the reference flow rate value and the flow rate value indicated by the branch pipe flow rate measurement means is derived, and the flow rate value of the branch flow rate measurement means corresponding to the reference flow rate value indicating a predetermined flow rate based on the relational expression. Is set to the target flow rate value.

  In an eighth aspect based on the seventh aspect, in the flow rate measurement adjustment step, a relational expression is derived for each type of coating liquid used in the coating apparatus, and a target flow rate value is set.

  In a ninth aspect based on the sixth aspect, in the serial supply step, the reference flow rate value is set to a predetermined flow rate by any one of the branch flow rate adjusting means connected in series. The flow rate adjustment by the other branch flow rate adjustment means is fully opened. In the flow rate measurement adjustment step, the flow rate value indicated by each branch flow rate measurement unit is set to the respective target flow rate value while any one of the branch flow rate adjustment units adjusts the reference flow rate value to a predetermined flow rate. Is done.

  In a tenth aspect based on the ninth aspect, a target flow rate value is set for each type of coating liquid used in the coating apparatus in the flow rate measurement adjustment step.

  In an eleventh aspect based on the first aspect, the plurality of branch pipes are provided with connecting pipes for connecting the branch pipes. In the serial supply step, the coating liquid is supplied from one supply source to one of the plurality of branch pipes, and the supply liquid is sequentially flowed to the other branch pipes via the connecting pipe, and then the most downstream in the flow of the coating liquid. The coating liquid is discharged from a nozzle provided in the branch pipe.

  A twelfth aspect of the invention is a coating apparatus that discharges coating liquid from a plurality of nozzles. The coating apparatus includes a single supply source, a plurality of nozzles, a main pipe, a plurality of branch pipes, a plurality of branch pipe flow rate measuring means, a connecting pipe, and a control unit. A single source stores the coating liquid. The plurality of nozzles discharge the coating liquid. The main pipe supplies the coating liquid from a supply source. The plurality of branch pipes divide the coating liquid supplied from the main pipe and supply the divided liquids to the plurality of nozzles. A plurality of branch pipe flow rate measuring means are provided in each branch pipe and measure the flow rate of the coating liquid flowing through the branch pipe. The connecting pipe connects the downstream side of the branch flow rate measuring means in the branch pipe and the upstream side of the branch pipe flow rate measuring means in another branch pipe. A control part adjusts the measurement result of the coating liquid flow volume which each branch pipe flow measurement means measured. The control unit includes a plurality of branch flow rate measuring means connected in series via the branch pipe and the connecting pipe, and a coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series, and the supplied coating is applied. In a state where the liquid is discharged from one of the nozzles, the measurement result of each coating liquid flow rate in the branch flow rate measuring unit is adjusted.

  In a thirteenth aspect based on the twelfth aspect, the control unit supplies the coating liquid supplied from the supply source to the main pipe only to one selected branch pipe selected from the plurality of branch pipes, and supplies it to the other branch pipes. In a state where the supply of the coating liquid is closed, the relationship between the measurement result by the branch flow rate measuring means provided in the selected branch pipe and the actual discharge amount of the coating liquid discharged from the nozzle of the selected branch pipe is measured. . The control unit includes a plurality of branch flow rate measuring means connected in series via the branch pipe and the connecting pipe, and a coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series, and the supplied coating is applied. In the state in which the liquid is discharged from one of the nozzles, the measurement result of the coating liquid flow rate in the other branch flow rate measuring means is adjusted based on the coating liquid flow rate measured by the branch flow rate measuring means provided in the selected branch pipe.

  In a fourteenth aspect based on the twelfth aspect, at least one of the plurality of branch pipe flow rate measuring means is a mass flow meter for measuring a mass flow rate of the coating liquid flowing through the branch pipe. The control unit includes a plurality of branch flow rate measuring means connected in series via the branch pipe and the connecting pipe, and a coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series, and the supplied coating is applied. In a state where the liquid is discharged from one of the nozzles, the measurement result of the coating liquid flow rate in the other branch flow rate measuring means is adjusted with reference to the coating liquid flow rate measured by the mass flow meter.

  In a fifteenth aspect based on the twelfth aspect, the main flow rate measuring means is further provided. The main pipe flow rate measuring means is provided in the main pipe and measures the flow rate of the coating liquid flowing through the main pipe. The control unit supplies the coating liquid supplied from the supply source to the main pipe only to one selected branch pipe selected from a plurality of branch pipes, and in a state where the supply of the coating liquid to the other branch pipes is closed. The relationship between the measurement result by the pipe flow rate measuring means and the actual discharge amount of the coating liquid discharged from the nozzle of the selected branch pipe is measured. The control unit includes a plurality of branch flow rate measuring means connected in series via the branch pipe and the connecting pipe, and a coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series, and the supplied coating is applied. In a state where the liquid is discharged from one of the nozzles, the measurement result of the coating liquid flow rate in the branch flow rate measuring unit is adjusted based on the coating liquid flow rate measured by the main flow rate measuring unit.

  In a sixteenth aspect based on the twelfth aspect, a mass flow meter is further provided. The mass flow meter is provided in the main pipe and measures the mass flow rate of the coating liquid flowing through the main pipe. The control unit includes a plurality of branch flow rate measuring means connected in series via the branch pipe and the connecting pipe, and a coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series, and the supplied coating is applied. In a state where the liquid is discharged from one of the nozzles, the measurement result of the coating liquid flow rate in the branch flow rate measuring unit is adjusted based on the coating liquid flow rate measured by the mass flow meter.

  In a seventeenth aspect according to any one of the twelfth to sixteenth aspects, a plurality of branch pipe flow rate adjusting means is further provided. The plurality of branch pipe flow rate adjusting means are respectively provided in the branch pipes and adjust the flow rate of the coating liquid flowing through the branch pipes to a predetermined flow rate according to the measurement result of the coating liquid flow rate by the branch pipe flow rate measuring means. The control unit includes a plurality of branch flow rate measuring means and branch flow rate adjusting means connected in series via the branch pipe and the connecting pipe, respectively, and the application liquid is supplied from the supply source to the branch flow rate measuring means and the branch flow rate adjusting means connected in series. In the state where the supplied coating liquid is discharged from one of the nozzles, the branch flow rate adjusting means corresponding to the predetermined flow rate is determined based on the measurement result of each coating liquid flow rate in the branch flow rate measuring means. Set the target flow rate value to be the adjustment target.

  In an eighteenth aspect based on the twelfth aspect, a valve is further provided. The valve is provided in each branch pipe, and switches between application liquid flowing through the branch pipe to the connection pipe or the nozzle of the branch pipe according to control of the control unit. The control unit supplies the coating liquid from a supply source to one of the plurality of branch pipes, switches the valve and sequentially flows the supply liquid to the other branch pipes via the connection pipe, and then flows the coating liquid. A plurality of branch flow rate measuring means are respectively connected in series by discharging the coating liquid from a nozzle provided on the most downstream branch.

  According to the first aspect of the present invention, a plurality of branch pipe flow rate measuring means connected in parallel are connected in series, whereby all the branch pipe flow rate measuring means can be adjusted by one flow of the coating liquid. For example, the time required for adjustment work performed for each branch flow rate measuring means provided in each of the multiple systems can be reduced to the time for one system, and the amount of flow of the coating liquid for the adjustment work can be greatly reduced. can do.

  According to the second aspect, among the plurality of branch flow rate measuring means connected in parallel, the branch flow rate measuring means of the other branch is calibrated on the basis of the flow rate measurement value of one branch flow rate measuring means. Therefore, it is not necessary to weigh and calibrate the actual discharge flow rate for each nozzle system. For example, when the coating liquid to be applied is changed, the branch flow rate measuring means of other branch pipes are calibrated based on the flow rate measurement value of the reference branch pipe flow rate measuring means even after the change of the coating liquid. The number of man-hours for managing flow rate is drastically reduced In addition, since it is possible to calibrate the branch flow rate measuring means using the coating liquid used in the actual coating operation, it is possible to calibrate with high accuracy that matches the actual work compared to the flow rate setting using the alternative coating liquid. No conversion work is required. In addition, it is possible to eliminate unstable elements of flow rate management due to fluctuations in the actual discharge flow rate due to the increase in the actual discharge flow rate measurement time as in the past, making it possible to set an accurate actual discharge flow rate. Become.

  According to the third aspect, among the plurality of branch flow rate measuring means connected in parallel, the branch flow rate measuring means of other branch pipes are calibrated on the basis of the flow rate measurement value of the branch flow rate measuring means for measuring the mass flow rate. The Therefore, the work of weighing and calibrating the actual discharge flow rate becomes unnecessary. Also, when changing the coating liquid to be applied, since the branch flow rate measuring means of other branch pipes are calibrated based on the flow rate measurement value of the branch flow rate measuring means for measuring the mass flow rate even after the change of the coating liquid, The flow control man-hours of the coating device are drastically reduced. In addition, since it is possible to calibrate the branch flow rate measuring means using the coating liquid used in the actual coating operation, it is possible to calibrate with high accuracy that matches the actual work compared to the flow rate setting using the alternative coating liquid. No conversion work is required.

  According to the fourth aspect of the invention, the branch flow rate measuring means is calibrated on the basis of the flow rate measurement value of the main flow rate measuring means provided on the main pipe. Therefore, it is not necessary to weigh and calibrate the actual discharge flow rate for each nozzle system. For example, when changing the coating liquid to be applied, the branch flow rate measuring means is calibrated based on the flow rate measurement value of the main main flow rate measuring means even after the change of the coating liquid. Man-hours are drastically reduced. In addition, since it is possible to calibrate the branch flow rate measuring means using the coating liquid used in the actual coating operation, it is possible to calibrate with high accuracy that matches the actual work compared to the flow rate setting using the alternative coating liquid. No conversion work is required. In addition, it is possible to eliminate unstable elements of flow rate management due to fluctuations in the actual discharge flow rate due to the increase in the actual discharge flow rate measurement time as in the past, making it possible to set an accurate actual discharge flow rate. Become.

  According to the fifth aspect, the branch flow rate measuring means is calibrated with reference to the flow rate measurement value of the main flow rate measuring means for measuring the mass flow rate of the coating liquid flowing through the main pipe. Therefore, the work of weighing and calibrating the actual discharge flow rate becomes unnecessary. Further, when changing the coating liquid to be applied, the branch flow rate measuring means is calibrated based on the flow rate measurement value of the main flow rate measuring means for measuring the mass flow rate even after the change of the coating liquid. The flow management man-hours are drastically reduced. In addition, since it is possible to calibrate the branch flow rate measuring means using the coating liquid used in the actual coating operation, it is possible to calibrate with high accuracy that matches the actual work compared to the flow rate setting using the alternative coating liquid. No conversion work is required.

  According to the sixth invention, a set of a plurality of branch pipe flow rate measuring means and branch pipe flow rate adjusting means connected in parallel is connected in series, so that the target flow rate value of each branch pipe can be obtained by the flow of the coating liquid once. Can be set individually. For example, it is possible to reduce the time of adjustment work performed for each branch pipe flow rate measuring means and branch pipe flow rate adjustment means provided in each of the multiple systems to one system time, and to flow the coating liquid for the adjustment work The amount can also be greatly reduced.

  According to the seventh aspect, it is not necessary to measure the actual discharge flow rate for each nozzle system and derive the relational expressions. For example, when changing the coating liquid to be applied in the coating apparatus, the target flow rate value of the branch pipe is set based on the reference flow rate value even after the change of the coating liquid, and the flow management man-hour of the coating apparatus is drastically reduced. In addition, since it is possible to set the target flow rate using the coating liquid used in the actual coating operation, compared to the flow setting using the alternative coating liquid, the target flow rate setting with high accuracy that matches the actual work can be achieved. This is possible, and conversion work is not necessary.

  According to the eighth aspect of the invention, even when a coating liquid having different characteristics is used, a relational expression corresponding to the coating liquid to be used is set, so that an accurate target flow rate value is set according to the coating liquid to be used. It becomes possible.

  According to the ninth aspect of the invention, the target flow rate can be set by matching the flow rate of the coating liquid with the discharge flow rate discharged in the actual coating operation, so that pinpoint flow rate management in accordance with the actual operation is possible. In addition, the man-hour for flow rate management is further reduced.

  According to the tenth aspect, even when a coating liquid having different characteristics is used, an accurate target flow rate value can be set according to the coating liquid to be used.

  According to the eleventh aspect, by connecting a plurality of branch pipes with connecting pipes, a plurality of branch pipe flow rate measuring means connected in parallel can be easily connected in series.

  Moreover, according to the coating apparatus of this invention, the effect similar to the flow volume setting method mentioned above can be acquired.

The top view and front view which show the principal part schematic structure of the coating device 1 which concerns on one Embodiment of this invention. The block diagram which shows schematic structure of the supply part 54 which concerns on one Embodiment of this invention. The block diagram which shows the control function of the coating device 1 of FIG. The flowchart which shows an example of the flow volume setting procedure in the coating device 1 of FIG. Subroutine showing an example of operation of actual flow rate measurement mode processing in step S82 of FIG. Subroutine showing an example of the operation of the branch flow rate setting mode processing in step S83 of FIG. The figure which shows an example of the connection state of piping in an actual flow measurement mode process The figure which shows an example of the connection state of the piping in branch flow rate setting mode processing The figure which shows an example of the connection state of piping in a coating process A graph showing an example of a relational expression between the actual discharge flow rate R and the flow rate measurement value F The graph which shows an example of the relational expression of the flow measurement value F and the flow measurement value f The figure which shows an example of the relational expression each set according to the kind of coating liquid to be used The figure which shows an example of the state of each flow control valve 546 and the branch flow meter 547 in the branch flow rate setting mode and during the coating operation The block diagram which shows an example of the coating device which branches and supplies to the several nozzles 108a-108n from the conventional single supply source 101 The figure which shows an example of the relational expression of the value of the conventional flowmeter, and an actual discharge flow rate

  Hereinafter, a coating apparatus 1 according to an embodiment of the present invention will be described with reference to the drawings. In order to make the description concrete, the following description will be given using an example in which the coating apparatus 1 is applied to a coating apparatus that manufactures an organic EL device that uses a solution in which an organic EL material is dissolved as a coating liquid. Note that the organic EL material in this specification is a material for forming an organic layer (a layer containing an organic substance among a light emitting layer, a charge transport layer, a charge injection layer, and the like). It is a material that is soluble in solvents. The coating apparatus 1 forms an organic layer by applying a coating solution containing an organic EL material in a predetermined pattern shape on an object to be coated (for example, a glass substrate) placed on a stage, thereby forming an organic EL device. Is to be manufactured. FIG. 1A is a plan view showing a schematic configuration of a main part of the coating apparatus 1. FIG. 1B is a front view illustrating a schematic configuration of a main part of the coating apparatus 1. As described above, the coating apparatus 1 uses a plurality of types of coating liquid containing an organic EL material. As a representative of these, a coating solution (hereinafter referred to as an organic EL material) is used as a representative solution. It will be described as an example of use as a coating liquid that may be described.

  In FIG. 1A and FIG. 1B, the coating apparatus 1 generally includes a substrate mounting device 2 and an organic EL coating mechanism 5. The organic EL coating mechanism 5 includes a nozzle moving mechanism 51, a nozzle unit 50, and liquid receivers 53L and 53R. The nozzle moving mechanism 51 has a guide member 511 extending in the X-axis direction in the figure, and moves the nozzle unit 50 in the X-axis direction in the figure along the guide member 511. The nozzle unit 50 includes, for example, a plurality of nozzles 52 that discharge a coating liquid containing an organic EL material of any one of red, green, and blue (in FIG. 1, only three nozzles 52a, 52b, and 52c are shown). Are held side by side. In FIG. 1, the coating apparatus 1 showing only the three nozzles 52 a, 52 b, and 52 c is shown, but in the coating apparatus 1, more nozzles 52 are arranged in parallel and held by the nozzle unit 50. It is possible. In the coating apparatus 1, n (for example, 10 to 20) nozzles 52 (hereinafter referred to as nozzles 52a to 52n) can be arranged in parallel. In this case, any of red, green, and blue A coating liquid containing one color organic EL material is discharged from the nozzles 52a to 52n. In addition, each nozzle 52a to 52n is supplied with a coating liquid containing an organic EL material of any one of red, green, and blue from a single supply source 541 (see FIG. 2). As described above, the coating liquid containing the organic EL material of the same color is ejected from the plurality of nozzles 52, but the coating liquid containing the red organic EL material is ejected from the nozzles 52a to 52n for specific description. An example is used.

  The substrate mounting apparatus 2 includes a stage 21, a turning unit 22, a parallel movement table 23, a guide receiving unit 24, and a guide member 25. The stage 21 places a substrate P such as a glass substrate to be coated on the upper surface of the stage. The lower part of the stage 21 is supported by the turning unit 22, and the stage 21 is configured to be rotatable in the θ direction shown in the figure by the turning operation of the turning unit 22. The stage 21 is provided with a heating mechanism for preheating the substrate P coated with a coating solution containing an organic EL material on the stage surface, a suction mechanism for the substrate P, a delivery pin mechanism, and the like. Yes.

  The guide member 25 extends in the Y-axis direction perpendicular to the X-axis direction and is fixed horizontally so as to pass under the organic EL coating mechanism 5. A guide receiving portion 24 that abuts on the guide member 25 and slides on the guide member 25 is fixed to the lower surface of the translation table 23. In addition, the swivel unit 22 is fixed on the upper surface of the translation table 23. Accordingly, the parallel movement table 23 can be moved in the Y-axis direction along the guide member 25 by receiving a driving force from, for example, a linear motor (not shown), and the stage 21 supported by the turning unit 22 can be moved. Horizontal movement is also possible.

  When the substrate P is placed on the stage 21 via the delivery pin mechanism, the substrate P is sucked and fixed, and the parallel movement table 23 moves to the lower side of the organic EL coating mechanism 5, the substrate P becomes red organic. This is the position where the coating liquid containing the EL material is applied from the nozzles 52a to 52n. Then, the control unit 3 (see FIG. 3) controls the nozzle moving mechanism unit 51 so as to reciprocate the nozzle unit 50 in the X-axis direction, and moves the stage 21 by a predetermined pitch in the Y-axis direction every linear movement. Thus, the translation table 23 is controlled so that the coating liquid containing the organic EL material at a predetermined flow rate is discharged from the nozzles 52a to 52n. Further, at the discharge positions in the X-axis direction of the nozzles 52a to 52n, the liquid that receives the coating liquid containing the organic EL material discharged out of the substrate P is disposed in both side spaces deviating from the substrate P placed on the stage 21. Receiving portions 53L and 53R are fixed. The nozzle moving mechanism 51 is disposed outside the other side of the substrate P from the upper space of the liquid receiving portion 53 (for example, the liquid receiving portion 53L) disposed outside the one side of the substrate P across the substrate P. The nozzle unit 50 is reciprocated to the upper space of the liquid receiver 53 (for example, the liquid receiver 53R) provided. The translation table 23 moves the stage 21 by a predetermined pitch in a predetermined direction (Y-axis direction in the drawing) perpendicular to the nozzle reciprocating direction when the nozzle unit 50 is disposed in the upper space of the liquid receiving portion 53. Let Simultaneously with the operation of the nozzle moving mechanism 51 and the parallel movement table 23, the coating liquid containing the organic EL material is ejected from the nozzles 52a to 52n in a liquid column state, so that the coating liquid containing the red organic EL material becomes the substrate. A stripe-shaped coating row is formed on P.

  Next, a schematic configuration of the coating liquid supply unit 54 in the coating apparatus 1 will be described with reference to FIG. FIG. 2 is a block diagram illustrating a schematic configuration of the supply unit 54 of the coating apparatus 1.

  In FIG. 2, the coating apparatus 1 includes a supply unit 54. The supply unit 54 divides a coating solution (for example, a coating solution containing a red organic EL material) supplied from a single supply source 541 into a plurality of nozzles 52 a to 52 n (a plurality of nozzles 52 a to 52 n (in the manifold 544). To the nozzle unit 50). Here, in the supply unit 54, a supply pipe from the supply source 541 until the coating liquid is branched into a plurality of pipes is referred to as a main pipe, and the supply pipe from the branching of the coating liquid to a plurality of nozzles is supplied to the nozzles 52a to 52n. Are described as branch pipes, and the pipes connecting the branch pipes are referred to as connection pipes.

  The supply unit 54 includes a supply source 541, a pressurization unit 542, a filter 543, a manifold 544, a plurality of first on-off valves 545a to 545n, a plurality of flow control valves 546a to 546n, a plurality of branch flow meters 547a to 547n, and A plurality of second on-off valves 548a to 548n are provided. The supply unit 54 includes third open / close valves 549ab to 549mn in connection pipes that connect the branch pipes. The supply source 541 stores a coating liquid containing an organic EL material to be applied by the coating apparatus 1, and stores, for example, a coating liquid containing the organic EL material in a flexible pack. The pressurizing unit 542 takes out the coating liquid containing the organic EL material stored in the supply source 541 by pressurizing the supply source 541 in accordance with the operation signal Cp (see FIG. 3) output from the control unit 3. Flow into the main. The filter 543 removes foreign matters in the coating liquid containing the organic EL material that flows in the main pipe. Then, the coating liquid containing the organic EL material flowing through the main pipe is supplied to the manifold (manifold pipe) 544.

  The manifold 544 branches the coating liquid containing the organic EL material supplied from the main pipe into a plurality of (for example, 10 to 20) branch pipes. Here, the plurality of branch pipes from which the manifold 544 branches are connected to the nozzles 52a to 52n, respectively, and in the following description, the branch pipes connected to the nozzles 52a to 52n are described as a-system branch pipes to n-system branch pipes. To do.

  The first opening / closing valve 545a opens and closes the flow path from the manifold 544 to the a-system branch pipe in accordance with an operation signal Cv1a (see FIG. 3) output from the control unit 3, and applies a coating liquid containing an organic EL material to a Supply or stop the system branch. The flow rate control valve 546a controls the flow rate of the coating liquid containing the organic EL material flowing through the a system branch pipe in accordance with the operation signal Cfa (see FIG. 3) output from the control unit 3. The branch pipe flow meter 547a detects the flow rate of the coating liquid containing the organic EL material in the a system branch pipe, and outputs the flow rate information Ifa (see FIG. 3) to the control unit 3. As will be apparent from the description below, the control unit 3 generates the operation signal Cfa to control the operation of the flow rate control valve 546a based on the flow rate information Ifa, and controls the operation of the flow rate control valve 546a. The control valve 546a and the branch flow meter 547a together function as a mass flow controller. The target flow rate value fac becomes an adjustment target of the flow rate control valve 546a in the coating operation.

  The second opening / closing valve 548a opens and closes the flow path from the system a branch pipe to the nozzle 52a in accordance with the operation signal Cv2a (see FIG. 3) output from the control unit 3, and the coating liquid containing the organic EL material is nozzled. Supply to 52a or stop. The nozzle 52a receives the supply of the coating liquid containing the organic EL material from the a-system branch pipe via the second opening / closing valve 548a, and discharges the coating liquid containing the organic EL material in the liquid column state from the tip. . The nozzle 52a has a filter 521a (not shown) for removing foreign substances in the coating liquid containing the organic EL material supplied from the a-system branch pipe.

  Other b system branch pipes-n system branch pipes also have the same components as the a system branch pipes. That is, the first open / close valves 545b to 545n open and close the flow paths from the manifold 544 to the b system branch pipe to the n system branch pipe according to the operation signals Cv1b to Cv1n output from the control unit 3, respectively. Is supplied to or stopped from the b-system branch pipe to the n-system branch pipe. Further, the flow rate control valves 546b to 546n control the flow rate of the coating liquid containing the organic EL material flowing through the b system branch pipe to the n system branch pipe, respectively, according to the operation signals Cfb to Cfn output from the control unit 3, respectively. . The branch pipe flow meters 547b to 547n detect the flow rate of the coating liquid containing the organic EL material in the b system branch pipe to the n system branch pipe, respectively, and output the flow rate information Ifb to Ifn to the control unit 3, respectively. Accordingly, the control unit 3 also generates the operation signals Cfb to Cfn so that the target flow rate values fbc to fnc are obtained based on the flow rate information Ifb to Ifn, and the flow rate control valve 546b for the other b system branches to the n system branches. In order to control the operation of ˜546n, the control unit 3, the flow rate control valves 546b to 546n, and the branch flow meters 547b to 547n respectively function as mass flow controllers. The target flow rate values fbc to fnc are also adjustment targets for the flow rate control valves 546b to 546n in the application work, respectively.

  Further, the second on-off valves 548b to 548n respectively open and close the b-system branch pipes to the n-system branch pipes according to the operation signals Cv2b to Cv2n output from the control unit 3, respectively, and apply the coating liquid containing the organic EL material to the nozzles. Supply or stop to 52b to 52n. The nozzles 52b to 52n receive the supply of the coating liquid containing the organic EL material from the b system branch pipe to the n system branch pipe through the second opening / closing valves 548b to 548n, respectively, A coating solution containing an organic EL material is discharged. The nozzles 52b to 52n also have filters 521b to 521n (not shown) for removing foreign substances in the coating liquid containing the organic EL material supplied from the b system branch pipe to the n system branch pipe, respectively. In addition, each piping from the supply source 541 to the nozzles 52a to 52n uses a pipe member made of PE (polyethylene), PP (polypropylene), Teflon (registered trademark), or the like.

  Moreover, the a system branch pipe-n system branch pipe is provided with the connection pipe which connects between each branch pipe. Specifically, a-b connecting the a-system branch pipe between the branch flow meter 547a and the second on-off valve 548a and the b-system branch pipe between the first on-off valve 545b and the flow control valve 546b. A system branch connection pipe is provided. The ab system branch pipe connection pipe is provided with a third on-off valve 549ab. The third on-off valve 549ab opens and closes the connection pipe from the a-system branch pipe to the b-system branch pipe in accordance with an operation signal Cv3ab (see FIG. 3) output from the control unit 3, and applies a coating liquid containing an organic EL material. Supply or stop from the a system branch pipe to the b system branch pipe.

  The other b system branch pipes-n system branch pipes also have connection pipes similar to the ab system branch connection pipes. That is, a bc system branch connection that connects a b system branch between the branch flow meter 547b and the second on-off valve 548b and a c system branch between the first on-off valve 545c and the flow control valve 546c. A tube is provided. The bc system branch pipe connection pipe is provided with a third on-off valve 549bc. The third opening / closing valve 549bc opens and closes the connection pipe from the b-system branch pipe to the c-system branch pipe in accordance with the operation signal Cv3bc output from the control unit 3, and allows the application liquid containing the organic EL material to be transferred from the b-system branch pipe to the c-system branch pipe. Supply or stop the system branch. Also, a cd system branch connection that connects the c system branch pipe between the branch flow meter 547c and the second on-off valve 548c and the d system branch pipe between the first on-off valve 545d and the flow control valve 546d. A tube is provided. The cd system branch pipe connection pipe is provided with a third on-off valve 549cd. The third on-off valve 549 cd opens and closes the connection pipe from the c-system branch pipe to the d-system branch pipe in accordance with the operation signal Cv3cd output from the control unit 3, and applies the coating liquid containing the organic EL material from the c-system branch pipe to d. Supply or stop the system branch. A similar connecting pipe and third on-off valves 549de to 549lm are provided between the d-system branch pipe and the m-system branch pipe, and the m-system branch pipe between the branch flow meter 547m and the second on-off valve 548m, An mn system branch pipe connection pipe that connects the n system branch pipe between the first opening / closing valve 545n and the flow rate control valve 546n is provided. The mn system branch pipe connection pipe is provided with a third opening / closing valve 549mn. The third on-off valve 549 mn opens and closes the connection pipe from the m-system branch to the n-system branch in accordance with the operation signal Cv3mn output from the control unit 3, and allows the coating liquid containing the organic EL material to Supply or stop the system branch. In addition, the connection pipe which connects n system branch pipe and a system branch pipe is not provided in the coating device 1 of this embodiment.

  Next, with reference to FIG. 3, a schematic configuration of the control function in the coating apparatus 1 will be described. FIG. 3 is a block diagram showing a control function of the coating apparatus 1.

  In FIG. 3, the coating apparatus 1 includes a control unit 3 that controls each component described above. For example, the control unit 3 is configured by a general computer system, and includes a storage medium such as a hard disk and a memory used by a built-in computer, and an input device through which a user inputs measurement results and the like. The control unit 3 includes a pressurizing unit 542, first on-off valves 545a to 545n, flow rate control valves 546a to 546n, second on-off valves 548a to 548n, third on-off valves 549ab to 549mn, swivel unit 22, and parallel movement. The operations of the table 23 and the nozzle moving mechanism unit 51 are controlled. In particular, the control unit 3 controls the operation of the pressurizing unit 542 by outputting the operation signal Cp. The controller 3 controls the operations of the first on-off valves 545a to 545n by outputting the operation signals Cv1a to Cv1n, respectively. The controller 3 controls the operations of the flow control valves 546a to 546n by outputting the operation signals Cfa to Cfn, respectively. The controller 3 controls the operations of the second on-off valves 548a to 548n by outputting the operation signals Cv2a to Cv2n, respectively. And the control part 3 controls operation | movement of 3rd on-off valve 549ab-549mn by outputting the operation signals Cv3ab-Cv3mn, respectively.

  In addition, the control unit 3 acquires flow rate information Ifa to Ifn indicating the branch flow rates output from the branch flow meters 547b to 547n, respectively. The operation of the flow rate control valves 546a to 546n is controlled according to the flow rate information Ifa to Ifn so that the target flow rate (target flow rate value fac to fnc) set for each of the a system branch pipe to the n system branch pipe is obtained.

  Here, as an example, a plurality of stripe-shaped grooves corresponding to a predetermined pattern shape to which the coating liquid containing the organic EL material is to be applied are formed on the surface of the substrate P that receives the coating liquid containing the red organic EL material. It may be formed so as to be arranged side by side. In this case, as the coating liquid containing the organic EL material, for example, an organic EL material having a viscosity enough to flow so as to spread in the groove on the substrate P is used, and specifically, a polymer for each color. A coating solution containing a type of organic EL material is used.

  The nozzle unit 50 can adjust the coating pitch interval of the nozzles 52a to 52n. In the nozzle unit 50, the nozzles 52a to 52n are arranged substantially linearly apart with respect to the X-axis direction in FIG. 1 and are slightly shifted in the Y-axis direction in FIG. The distance between the adjacent two nozzles 52 in the Y-axis direction is adjusted so as to correspond to the desired interval between the application rows. For example, it is set to be equal to several times (for example, 3 times, etc.) the stripe-shaped groove pitch formed in advance on the surface of the substrate P. Further, even when there is no such groove, the Y-axis direction pitch of the nozzles 52 is similarly adjusted so as to correspond to a desired stripe-shaped application row interval.

  Various configurations for adjusting the pitch in the Y-axis direction of the nozzle 52 described above are conceivable. For example, by configuring the nozzles 52a to 52n to be movable in the Y-axis direction (sub-scanning direction), the Y-axis direction pitch of each nozzle 52 can be adjusted. As another example, the nozzle unit 50 is supported so as to be rotatable around a predetermined vertical support shaft, and the coating pitch interval is adjusted by rotating the nozzle unit 50 around the support shaft under the control of the control unit 3. can do.

  Based on the position and direction of the substrate P placed on the stage 21, the control unit 3 is configured to form a coating row on the substrate P (for example, when the groove is formed on the substrate P, the direction of the groove). ) Is adjusted so as to be in the X-axis direction, and a coating start point, that is, a coating start position at which coating is started at one end side forming the coating row on the substrate P is calculated. . The application start position is an upper space of one liquid receiving portion 53. Then, the control unit 3 drives the parallel movement table 23 and the nozzle movement mechanism unit 51 as described above.

  At the application start position, the control unit 3 instructs the supply unit 54 to start discharging the application liquid containing the organic EL material from the nozzles 52a to 52n. At this time, the control unit 3 makes the nozzle so that the coating amount of the coating liquid containing the organic EL material becomes uniform at each point of the striped coating row, and the coating liquid containing the organic EL material is discharged in a liquid column state. The application amount is controlled according to the moving speed of 52a to 52n, and the flow rate information Ifa to Ifn from the branch pipe flow meters 547a to 547n is fed back and controlled. Then, the control unit 3 causes the nozzle unit 50 to move to the guide member 511 while discharging the coating liquid containing the organic EL material onto the substrate P in order to form a coating row of the coating liquid containing the organic EL material on the substrate P. Control to move along. By this operation, the application liquid containing the red organic EL material discharged from the nozzles 52a to 52n in the liquid column state is simultaneously discharged onto the substrate P, and the application row of the application liquid containing the red organic EL material is formed. To go.

  When the control unit 3 is positioned on the other liquid receiving portion 53 fixed on the outside of the other end portion of the substrate P across the substrate P, the organic EL material from the nozzles 52a to 52n. The movement of the nozzle unit 50 by the nozzle moving mechanism unit 51 is stopped while the discharge of the coating liquid containing is continued. By this one movement, the application liquid containing the organic EL material is applied simultaneously to a plurality of application rows (for example, 10 to 20 application rows). Specifically, since the coating liquid containing the organic EL material of the same color is discharged from each of the nozzles 52a to 52n, for example, a total of 10 to 20 rows of coatings with one row of coatings being applied every 3 rows. A coating liquid containing an organic EL material is applied to the columns.

  Next, the control unit 3 pitches the parallel movement table 23 by a predetermined distance in the positive direction of the Y axis so that the application liquid containing the organic EL material can be applied to the application row to be applied next. . Then, when the control unit 3 positions the nozzle unit 50 across the substrate P in the opposite direction from the upper space of the other liquid receiving unit 53 and is positioned on the one liquid receiving unit 53, the organic material from the nozzles 52a to 52n. While the discharge of the coating liquid containing the EL material is continued, the movement of the nozzle unit 50 by the nozzle moving mechanism 51 is stopped. By this second movement, the application of the application liquid containing the organic EL material to the next application row is completed. By repeating such an operation, a coating row coated with a coating liquid containing a red organic EL material is formed.

  Next, an example of a flow rate setting procedure of the coating apparatus 1 according to an embodiment will be described with reference to FIGS. FIG. 4 is a flowchart showing an example of the flow rate setting procedure of the coating apparatus 1. FIG. 5 is a subroutine showing an example of the actual flow rate measurement mode processing in step S82 of FIG. FIG. 6 is a subroutine showing an example of the operation of the branch pipe flow rate setting mode process in step S83 of FIG. FIG. 7 is a diagram illustrating an example of a pipe connection state in the actual flow rate measurement mode process. FIG. 8 is a diagram illustrating an example of a pipe connection state in the branch pipe flow rate setting mode process. FIG. 9 is a diagram illustrating an example of a pipe connection state in the coating process.

  In FIG. 4, the control unit 3 operates the pressurizing unit 542 to cause the coating liquid containing the organic EL material stored in the supply source 541 to flow into the main pipe (step S80), and the process proceeds to the next step. . For example, the control unit 3 outputs an operation signal Cp for operating the pressurizing unit 542 to the pressurizing unit 542 to cause the pressurizing unit 542 to perform a pressurizing operation.

  Next, the control unit 3 determines the relationship between the actual flow rate R and the flow measurement value F of the reference branch flow meter 547 (for example, the branch flow meter 547a of the a system branch pipe among the plurality of branch flow meters 547). It is determined whether the formula has been set (step S81). For example, the control unit 3 sets a relational expression between the actual flow rate R and the flow rate measurement value F of the branch flow meter 547 serving as a reference for each type of coating liquid used by the coating device 1, and is installed in the memory. The relational expression is stored in the medium. And the control part 3 advances a process to following step S82, when the said relational expression is not set with respect to the coating liquid apply | coated with the coating device 1. FIG. On the other hand, when the above relational expression is set for the coating liquid applied by the coating apparatus 1, the control unit 3 advances the process to the next step S83.

  In step S82, the control unit 3 performs an actual flow rate measurement mode process and proceeds to the next step. The detailed operation of the actual flow rate measurement mode process will be described below with reference to FIG.

  In FIG. 5, the control unit 3 selects a branch pipe that measures an actual flow rate (actual discharge flow rate), that is, a branch pipe (for example, a system branch pipe) to which a reference branch flow meter 547 is connected, and sets a discharge flow rate range. Then (step S91), the process proceeds to the next step. Here, the discharge flow rate range indicates a range of discharge flow rate that may be applied when the coating apparatus 1 applies a coating liquid to be used in the future.

  Next, the control unit 3 includes a first on-off valve 545 (for example, a first on-off valve 545a) and a second on-off valve 548 provided in series with the target branch pipe selected in step S91. (For example, the second open / close valve 548a of the a system) is fully opened, the other open / close valves are fully closed (step S92), and the process proceeds to the next step.

  Next, the control unit 3 sets the reference branch pipe so that the flow rate measurement value F of the reference branch flow meter 547 (for example, the a-system branch pipe flow meter 547a) becomes an arbitrary value within the discharge flow rate range. The flow control valve 546 (for example, the a system flow control valve 546a) of the same branch as the flow meter 547 is operated (step S93), and the process proceeds to the next step. By the operation of step S93, the coating liquid containing the organic EL material that flows into the main pipe flows only to the target branch pipe (for example, a branch pipe of system a) selected in step S91, so that one nozzle 52 (for example, , The nozzle 52a) is discharged. Specifically, when the system a branch pipe is selected in step S91, the coating liquid containing the organic EL material flows as shown by the thick line in FIG. That is, the coating liquid containing the organic EL material that has flowed from the supply source 541 to the manifold 544 flows to the flow rate control valve 546a and the branch flow meter 547a via the first opening / closing valve 545a, and the second opening / closing valve 548a. A flow path that flows to the nozzle 52a is formed. In FIG. 7, the branch pipes and connection pipes in which the coating liquid containing the organic EL material does not flow in the actual flow rate measurement mode process are indicated by broken lines.

  Next, the control unit 3 acquires the actual discharge flow rate R measured by weighing and the flow rate measurement value F of the branch flow meter 547 serving as a reference at that time (for example, the flow rate measurement value fa of the branch flow meter 547a) ( Step S94), the process proceeds to the next step. For example, the user of the coating apparatus 1 measures the actual discharge flow rate R by weighing the coating liquid discharged from the nozzle 52 discharging the coating liquid in the operation state of step S93. For example, the actual discharge flow rate R of the coating liquid discharged from the nozzle 52 is such that the coating liquid is discharged from the nozzle 52 into a predetermined container, and the weight of the coating liquid in the container with respect to the unit discharge time (for example, milligram / minute). Weighed by Then, the user inputs the measured actual discharge flow rate R via the input device of the control unit 3. Note that the flow rate measurement value F of the branch flow meter 547 serving as a reference at that time may be automatically acquired by the control unit 3 using the flow rate information If output from the branch flow meter 547, or the user May be input via an input device.

  Next, the control unit 3 determines whether or not the actual flow rate measurement has been completed (step S95). For example, the weighing of the actual discharge flow rate R performed in step S93 and step S94 is performed corresponding to a plurality of points (for example, 3 to 5 points) in the discharge flow rate range. In step S95, when the weighing of the actual discharge flow rate R is performed corresponding to all the plurality of points, the control unit 3 proceeds to the next step S96. On the other hand, when the weighing of the actual discharge flow rate R is not performed on any of the plurality of points, the control unit 3 returns to step S93 and performs processing for other values within the discharge flow rate range.

  In step S <b> 96, the control unit 3 sets a relational expression between the actual discharge flow rate R and the flow rate measurement value F of the reference branch flow meter 547 and stores it in the storage medium, and ends the processing by the subroutine. Hereinafter, a relational expression between the actual discharge flow rate R and the flow rate measurement value F of the branch pipe flow meter 547 serving as a reference will be described with reference to FIG. FIG. 10 is a graph showing an example of the relational expression obtained from the result of weighing the actual discharge flow rate R.

In FIG. 10, the measurement result of the actual discharge flow rate R is plotted with the flow rate measurement value F of the branch flow meter 547 on the horizontal axis and the actual discharge flow rate R as the vertical axis. Specifically, the actual discharge flow rate weighed when the flow rate measurement value of the reference branch flow meter 547 is F1 by the processing of step S93 and step S94 is R1. The actual discharge flow rate weighed when the flow rate measurement value of the reference branch flow meter 547 is F2 is R2. The actual discharge flow rate weighed when the flow rate measurement value of the reference branch flow meter 547 is F3 is R3. An approximate curve (for example, a straight line) passing through these three plot points (point F1-R1, point F2-R2, and point F3-R3) is the actual discharge flow rate R and the flow rate measurement value of the branch flow meter 547 serving as a reference. It is derived as a relational expression with F. For example, the above relational expression is
R = A * F + B
Indicated by Here, A and B are constants derived from the plot points, respectively. In the coating apparatus 1, such a relational expression is set and stored for each type of coating liquid used.

  Returning to FIG. 4, after the actual flow rate measurement mode process of step S82, the controller 3 performs a branch flow rate setting mode process (step S83), and proceeds to the next step. The detailed operation of the branch flow rate setting mode process will be described below with reference to FIG.

  In FIG. 6, the control unit 3 sets a discharge flow rate range for setting the branch pipe flow rate (step S101), and advances the processing to the next step. Here, the range of the discharge flow rate is the same as the range described in step S91, and the range of the discharge flow rate that can be applied when the coating apparatus 1 applies a coating liquid to be used from now on through each branch pipe. Is shown.

  Next, the control unit 3 fully opens the first opening / closing valve 545a, the second opening / closing valve 548n, and all the third opening / closing valves (that is, the third opening / closing valves 549ab to 549mn), and then opens the other opening / closing valves. (That is, the first opening / closing valves 545b to 545n and the second opening / closing valves 548a to 548m) are fully closed (step S102), and the process proceeds to the next step.

  Next, the control unit 3 controls the flow rate control valves 546 (for example, the flow rate control valves 546b to 546n of the b system to the n system) provided in the branch pipes other than the branch pipe used as a reference in the actual flow rate measurement mode processing in the step S82. ) Are fully opened (step S103), and the process proceeds to the next step.

  Next, the control unit 3 controls the branch pipe so that the flow rate measurement value F of the reference branch flow meter 547 (for example, the flow rate measurement value fa of the branch flow meter 547a) becomes an arbitrary value within the discharge flow rate range. The flow control valve 546 (for example, the a-system flow control valve 546a) is operated (step S104), and the process proceeds to the next step. By the operation of step S104, the coating liquid containing the organic EL material flowing in the main pipe passes through all the flow control valves 546a to 546n and the branch pipe flow meters 547a to 547n provided in each branch pipe. It discharges from the nozzle 52n connected to the n system branch pipe. Specifically, the coating liquid containing the organic EL material flows as shown by the thick line in FIG. 8 by the valve opening / closing process in steps S102 to S104. That is, the coating liquid containing the organic EL material that has flowed from the supply source 541 to the manifold 544 flows to the flow control valve 546a and the branch flow meter 547a via the first opening / closing valve 545a, and the a system branch pipe and the b system branch pipe It flows to the b system branch pipe through the connecting pipe connecting the two. Then, the coating liquid containing the organic EL material that has flowed to the b system branch flows to the flow control valve 546b and the branch flow meter 547b, and to the c system branch through the connecting pipe that connects the b system branch and the c system branch. To flow. Thereafter, the coating liquid containing the organic EL material flows in the same manner to the flow control valves 546c to 546m and the branch flow meters 547c to 547m provided in the c to m system branch pipes, and then the m system branch pipes and the n system branch pipes. It flows to the n system branch pipe through the connecting pipe to be connected. Then, a flow path is formed in which the coating liquid containing the organic EL material that finally flows to the n-system branch pipe flows to the nozzle 52n via the flow rate control valve 546n and the branch flow meter 547n. In FIG. 8 as well, the branch pipes and connection pipes in which the coating liquid containing the organic EL material does not flow in the branch pipe flow rate setting mode process are indicated by broken lines.

  Next, the control unit 3 acquires the flow rate measurement value F of the reference branch flow meter 547 and the flow rate measurement value f of another branch flow meter 547 (step S105), and advances the processing to the next step. For example, the control unit 3 acquires the flow rate measurement value F using the flow rate information Ifa of the branch pipe flow meter 547a that is the reference output in the state of step S104, and the flow rate information Ifb of the other branch flow meters 547b to 547n. The flow rate measurement values fb to fn are acquired using Ifn, respectively.

  Next, the control unit 3 determines whether or not the branch pipe flow rate setting has been completed (step S106). For example, the branch pipe flow rate setting performed in step S104 and step S105 is also performed corresponding to a plurality of points (for example, 3 to 5 points) in the discharge flow rate range, similarly to the weighing of the actual discharge flow rate R described above. In step S106, when the branch pipe flow rate setting is performed corresponding to all the plurality of points, the control unit 3 advances the processing to the next step S107. On the other hand, when the branch pipe flow rate setting is not performed for any of the plurality of points, the control unit 3 returns to step S104 and performs processing for other values within the discharge flow rate range.

  In step S107, the control unit 3 fully closes all the open / close valves and advances the process to the next step.

  Next, the control unit 3 sets a relational expression between the flow rate measurement value F of the branch flow meter 547 serving as a reference and the flow rate measurement value f of another branch flow meter 547, and stores it in the storage medium (step S108). ), The process by the subroutine is terminated. Hereinafter, a relational expression between the flow rate measurement value F of the branch pipe flow meter 547 and the flow rate measurement value f of another branch flow meter 547 will be described with reference to FIG. FIG. 11 is a graph showing an example of the relational expression obtained from the measurement results of step S104 and step S105.

In FIG. 8, the horizontal axis is a flow rate measurement value fb of a branch flow meter 547b which is an example of another branch flow meter 547, and the vertical axis is a flow rate measurement value F of a branch flow meter 547 serving as a reference. The measurement results are plotted. Specifically, the flow rate measurement value of the branch flow meter 547 serving as a reference when the flow rate measurement value of the branch flow meter 547b is fb1 is F1 by the processing of Step S104 and Step S105. Further, the flow rate measurement value of the branch flow meter 547 serving as a reference when the flow rate measurement value of the branch flow meter 547b is fb2 is F2. Further, the flow rate measurement value of the branch flow meter 547 serving as a reference when the flow rate measurement value of the branch flow meter 547b is fb3 is F3. An approximate curve (for example, a straight line) passing through these three plot points (point fb1-F1, point fb2-F2, and point fb3-F3) is a reference flow rate measurement value F of the branch flow meter 547 and a branch flow meter. It is derived as a relational expression with the flow rate measurement value fb of 547b. For example, the above relational expression is
F = Cb * fb + Db
Indicated by Here, Cb and Db are constants of the b system derived from the plot points, respectively. In the coating apparatus 1, such a relational expression is set and stored for each other branch flow meter 547 according to the type of coating liquid to be used.

  Returning to FIG. 4, after the branch flow rate setting mode processing in step S83, the control unit 3 sets a target flow rate value fc of each branch for a discharge flow rate used in a coating operation (step S85) described later (step S84). The process proceeds to the next step. Hereinafter, the target flow rate value fc will be described with reference to FIGS. In addition, FIG. 12 is a figure which shows an example of the relational expression each set according to the classification of the coating liquid to be used.

The control unit 3 sets a relational expression as shown in FIG. 12 by the processing in steps S80 to S83. FIG. 12 shows an example of a relational expression set and stored for each of the coating liquids q to t used by the control unit 3. For example, with respect to the coating liquid q, the relational expression between the actual discharge flow rate R and the flow rate measurement value F of the reference branch flow meter 547 (in FIG. 12, a branch flow meter 547a as an example) is
R = Aq * F + Bq
Is set in Here, Aq and Bq indicate the constants A and B set for the coating solution q, respectively. For the coating liquid q, the relational expression between the flow rate measurement value F of the branch flow meter 547a and the flow rate measurement value fb of the branch flow meter 547b is:
F = Cbq * fb + Dbq
Is set in Here, Cbq and Dbq are constants of the b system set for the coating liquid q, respectively. For the coating liquid q, the relational expression between the flow rate measurement value F of the branch flow meter 547a and the flow rate measurement value fc of the branch flow meter 547c is:
F = Ccq * fc + Dcq
Is set in Here, Ccq and Dcq are constants of the c system set for the coating solution q, respectively. The flow rate measurement values fd to fn of the branch flow meters 547d to 547n in the other d systems to n systems are also related to the flow measurement value F of the branch flow meter 547a in the coating liquid q in the same manner as the b system and c system. An expression is set.

で設定される。また、上述したように各関係式が塗布液の種別毎に設定されている。したがって、塗布液ｑを吐出流量Ｒｐで吐出する場合のｂ系統の目標流量値ｆｂｃｑは、

で設定される。 The control unit 3 sets the target flow rate value fc of each branch for the discharge flow rate by appropriately combining the above-described relational expressions. In order to make the description more specific, the target flow rate value fc when the discharge flow rate from the b-system nozzle 52b in the coating operation is the actual discharge flow rate Rp will be described. For example, as shown in FIG. 10, using a relational expression R = A * F + B between the actual discharge flow rate R and the flow measurement value F of the reference branch flow meter 547, the reference branch corresponding to the actual discharge flow rate Rp. A flow rate measurement value Fp of the flow meter 547 is derived. Then, as shown in FIG. 11, using the relational expression F = Cb * fb + Db between the flow rate measurement value F of the branch flow meter 547 serving as a reference and the flow rate measurement value fb of the branch flow meter 547b, it corresponds to the flow rate measurement value Fp. The flow rate measurement value fbp of the branch pipe flow meter 547b is derived. That is, as is clear from these relational expressions, when it is desired to discharge the coating liquid at the actual discharge flow rate Rp from the b-system nozzle 52b, the target flow value fbc of the coating liquid flowing through the b-system is set to the flow measurement value fbp. You can set it. Therefore, the target flow rate value fbc of the b system when discharging at the discharge flow rate Rp is

Set by. Further, as described above, each relational expression is set for each type of coating liquid. Therefore, the target flow rate value fbcq of the b system when the coating liquid q is discharged at the discharge flow rate Rp is:

Set by.

  Returning to FIG. 4, after setting the target flow rate value fc of each branch pipe in step S <b> 84, the control unit 3 performs a coating operation on an object to be coated (for example, a glass substrate) using the target flow rate value fc. S85). In this coating operation, the control unit 3 fully opens all the first opening / closing valves 545a to 545n and all the second opening / closing valves 548a to 548n, and fully closes all the third opening / closing valves 549ab to 549mn. . Further, the control unit 3 uses the flow rate information Ifa output from the branch pipe flow meter 547a of the a system so that the flow rate measurement value fa indicated by the branch flow meter 547a becomes the target flow rate value fac. To control. Thus, the target flow rate value fac becomes a flow rate adjustment target of the flow rate control valve 546a. Further, the control unit 3 uses the flow rate information Ifb output from the b-system branch flow meter 547b so that the flow rate measurement value fb indicated by the branch flow meter 547b becomes the target flow rate value fbc. To control. Thus, the target flow rate value fbc becomes a flow rate adjustment target of the flow rate control valve 546b. Further, the control unit similarly uses the flow rate information Ifc to Ifn output from the branch flowmeters 547c to 547n to measure the flow rate measurement values fc to fn indicated by the branch flowmeters 547c to 547n, respectively. The flow rate control valves 546c to 546n are controlled so that the target flow rate values fcc to fnc are obtained. In this manner, the target flow rate values fcc to fnc are flow rate adjustment targets of the flow rate control valves 546c to 546n, respectively.

  During the application work, the control unit 3 determines whether or not the branch flow rate needs to be reset (step S86) and whether or not the application work is to be ended (step S87). For example, the control unit 3 needs to reset the branch flow rate when the coating liquid used in the coating apparatus 1 is replaced or when a periodical management (for example, daily management) time for checking the branch flow rate comes. (Yes in step S86). And when it is judged that the reset of the branch pipe flow rate is required, the control part 3 returns to said step S81, and repeats a process. Moreover, the control part 3 returns to the said step S85, and repeats a process, when resetting of a branch pipe flow rate is unnecessary and continues an application | coating operation | work (both step S86 and step S87 are No). On the other hand, when ending the application work (Yes in Step S87), the control unit 3 stops the pressurization by the pressurizing unit 542 (Step S88), and ends the process according to the flowchart.

  In the flow rate setting method according to the above-described embodiment, the branch flow meter 547 (for example, the branch flow meter 547a) serving as a reference is measured using the measurement of the actual discharge flow rate, and calibrated by performing the pricing, The reference branch flow meter 547 is handled as a standard device in the coating apparatus 1. Then, by further calibrating another branch flow meter 547 using this standard device (for example, branch flow meter 547a), a stepwise calibration system is established, and a number of flow rates installed in the coating apparatus 1 are established. The flow of the meter is managed.

  As described above, in the coating apparatus according to the above-described embodiment, a plurality of branch flow meters connected in parallel are connected in series via the connecting pipe, whereby all branch flow rates are obtained by one flow of the coating liquid. Calibration of the meter becomes possible. Specifically, the time required for calibration work for each branch flow meter provided in each of the multiple systems can be shortened to one system time, and the amount of flow of the coating liquid for calibration work is also greatly increased. Can be reduced. In the above-described embodiment, the target flow rate values of the other branch pipes are set based on the flow rate measurement value of one branch flow meter among the plurality of branch pipe flow meters connected in parallel. Therefore, it is not necessary to weigh the actual discharge flow rate for each nozzle system and derive the relational expressions. For example, when changing the coating liquid to be applied in the coating apparatus (for example, changing from a coating liquid containing a red organic EL material to a coating liquid containing a green organic EL material), even after the change of the coating liquid Since the target flow rate value of the other branch pipes is set based on the flow rate measurement value of the branch pipe flow meter, the flow management man-hour of the coating apparatus is drastically reduced. In addition, since it is possible to set the target flow rate using the coating liquid used in the actual coating operation, compared to the flow setting using the alternative coating liquid, the target flow rate setting with high accuracy that matches the actual work can be achieved. This is possible, and conversion work is not necessary. In addition, since the actual discharge flow rate measurement time of the coating device becomes longer as in the past, unstable elements of flow management caused by fluctuations in the actual discharge flow rate can be eliminated, so accurate actual discharge flow rate setting Is possible.

  In the above-described embodiment, a plurality of points (for example, 3 to 5 points) in the discharge flow rate range are plotted to derive various relational expressions, but only one point may be plotted to derive a relational expression. It doesn't matter. For example, assuming that the relational expression to be derived is always a straight line passing through a predetermined origin (for example, (0, 0)), the relational expression can be derived by plotting one point. In this case, since the measurement of the actual discharge flow rate R and the branch pipe flow rate setting for deriving the relational expression are performed corresponding to one point, the flow rate management man-hour of the coating apparatus is further reduced.

  In the above-described embodiment, the example in which the actual flow rate measurement mode process is performed when the relational expression between the actual flow rate R and the flow rate measurement value F of the reference branch flow meter 547 is not set has been described. The actual flow rate measurement mode process may be performed according to other modes. For example, even if the relational expression between the actual flow rate R and the flow rate measurement value F of the reference branch flowmeter 547 has been set, the actual flow rate measurement mode process is performed to periodically reset the relational expression. You can go. Thereby, the reliability of the relational expression set by the actual flow rate measurement mode processing is increased, and more accurate flow rate management can be performed.

  In the above-described embodiment, an example in which the relational expression between the actual flow rate R and the flow rate measurement value F of the branch flowmeter 547 serving as a reference is set for each coating solution is described. The actual flow rate measurement mode process may not be performed. In this case, the other branch flowmeter 547 is priced based on the flow rate measurement value F of the reference branch flowmeter 547, but is not a price based on the measured measurement value of the actual discharge flow rate. Strictly speaking, the management is different from general calibration. Therefore, each branch flow meter 547 is subjected to relative evaluation based on the flow rate measurement value F instead of absolute evaluation as in the flow rate setting method described above. However, even with such a relative evaluation, it is possible to detect variations and fluctuations in the flow rate measurement value f of each branch flow meter 547 with reference to the flow rate measurement value F, and a target that eliminates these factors. By setting the flow rate value, each nozzle 52a to 52n can perform a coating operation with a uniform discharge flow rate.

  Further, when the branch pipe flow meter 547 serving as a reference is constituted by a mass flow meter or the like, the above-described actual flow measurement mode processing is not necessary. For example, when the reference branch flow meter 547 (for example, the branch flow meter 547a) is composed of a Coriolis mass flow meter or the like, the measurement value of the actual discharge flow rate by the actual flow measurement mode processing described above is used as a reference. No pricing is required. Therefore, when the reference branch flow meter 547 is composed of a mass flow meter or the like, the flow rate setting method described above is applied to other branch flow meters 547 without performing the actual flow measurement mode processing described above. Absolute evaluation is possible.

  Further, the branch flow rate setting described above is performed corresponding to a plurality of points in the discharge flow rate range used in the application work, but the branch flow rate may be set using other points. For example, when the discharge flow rates from the nozzles 52 of each system in the application operation in step S85 are all determined to be the same actual discharge flow rate Rp, the discharge flow rate in the application operation (that is, the actual discharge flow rate Rp) is determined. You can set the branch flow rate. Hereinafter, another example in the branch flow rate setting will be described.

  In this case, in the process in step S93, the control unit 3 determines that the flow rate measurement value F of the branch pipe flow meter 547 serving as a reference (for example, the flow rate measurement value fa of the branch flow meter 547a) is the discharge flow rate (ie, the actual flow rate). The branch flow control valve 546 (for example, the a system flow control valve 546a) provided with the branch pipe flowmeter 547 is operated so as to have a value corresponding to the discharge flow rate Rp).

  Here, the relationship between the flow rate measurement value F of the reference branch flow meter 547 and the discharge flow rate in the coating operation will be described. In the actual flow rate measurement mode processing in step S82 described above, a relational expression between the actual discharge flow rate R and the flow rate measurement value F of the branch pipe flow meter 547 is set. This relational expression is an example shown in FIG. 10, and it is assumed that the discharge flow rate from the nozzles 52 of each system in the coating operation is the actual discharge flow rate Rp. In this case, the flow rate measurement value of the branch flow meter 547 serving as a reference corresponding to the discharge flow rate (that is, the actual discharge flow rate Rp) in the coating operation is Fp. Therefore, the control unit 3 sets the flow rate measurement value Fp of the branch flow meter 547 serving as a reference according to the discharge flow rate in the coating operation using the above relational expression, and sets the flow rate measurement value Fp as a target when setting the branch flow rate. The flow rate control valve 546 (for example, the a-system flow rate control valve 546a) is operated as the flow rate value. That is, by this operation, the coating liquid containing the organic EL material that flows into the main pipe flows to each branch pipe connected in series via the connecting pipe and is discharged from one nozzle 52 (for example, the nozzle 52n). The coating liquid and the discharge flow rate become the coating liquid and the actual discharge flow rate used in the actual coating operation. And the control part 3 acquires the flow measurement value f of the branch flow meter 547 of each branch, and sets the obtained flow measurement value f to the target flow value fc of each branch in an actual application | coating operation, respectively.

  With reference to FIG. 13, the state of each flow control valve 546 and branch pipe flowmeter 547 during the above-described operation will be described. FIG. 13 is a diagram illustrating an example of the state of each flow control valve 546 and the branch flow meter 547 during the above-described branch flow rate setting mode and during the coating operation.

  In FIG. 13, when the flow rate of each branch pipe is set in the branch flow rate setting mode process described above, the flow rate measurement value F of the reference branch flow meter 547 (in FIG. 13, the branch flow meter 547a of the a-system branch pipe) is The branch flow control valve 546 provided with the branch flow meter 547 (in FIG. 13, the a-system flow control valve 546a) is controlled to operate at Fp (that is, a value corresponding to the actual discharge flow rate Rp). ing. Further, the flow rate control valve 546 (that is, the flow rate control valves 546b to 546n) of the other system branch pipes is fully opened. At that time, the flow rate measurement value in the reference branch flowmeter 547 indicates Fp, and the flow rate measurement values fb to fn in the branch flowmeters 547b to 547n of the other system branch lines indicate fbp to fnp, respectively. These flow rate measurement values fbp to fnp are set to target flow rate values fbc to fnc in the b system to n system branch pipes, respectively. In addition, the flow rate measurement value Fp of the a-system branch pipe flowmeter 547a is set to the target flow rate value fac in the a-system branch pipe as it is.

  On the other hand, when the coating liquid is discharged from all the a-system to n-system branch pipes in the application operation, the flow rate measurement value fa of the branch-flow meter 547a of the a-system branch pipe is the target flow value fac (that is, a value corresponding to the actual discharge flow rate Rp). Thus, the flow control valve 546a of the a system branch pipe is controlled. Further, the flow control valve 546b of the b system branch is controlled so that the measured flow value fb of the branch flow meter 547b of the b system branch becomes the target flow value fbc (that is, a value corresponding to the actual discharge flow rate Rp). Yes. Further, the flow rate measurement values fc to fn of the branch flow meters 547c to 547n of the c to n system branch pipes are respectively the target flow rate values fcc to fnc (that is, values corresponding to the actual discharge flow rate Rp), respectively. The flow control valves 546c to 546n of the n system branch pipes are in control operation.

  As described above, the coating apparatus of another example in setting the branch flow rate can perform the adjustment work of the branch pipe flow aiming at the pinpoint flow rate (that is, the coating flow rate used in the coating operation). Management man-hours are reduced. In addition, the coating apparatus of the other example does not require a relational expression between the flow rate measurement value of the reference branch flow meter and the flow rate measurement value of another branch flow meter.

  In the above description, the branch flow meter 547a provided in the a-system branch pipe is used as an example of the reference branch flow meter 547. This is based on the branch flow meter 547 that is the head for the flow of the coating liquid containing the organic EL material when a plurality of branch flow meters 547 connected in parallel are connected in series via a connecting tube. Although it is an example set, other branch flowmeters 547 may be used as a reference. For example, when a plurality of branch flow meters 547 are connected in series via a connecting pipe, a branch flow meter 547 (for example, provided in the b-system branch pipe) that does not lead to the flow of the coating liquid containing the organic EL material. Even if the branch pipe flowmeter 547b) is set as a reference, the same branch pipe flow rate can be set.

  Specifically, when setting the branch pipe flowmeter 547b as a reference, in step S103 (FIG. 6), the flow control valve 546 (that is, the flow control of the a system) provided in the branch pipe other than the reference branch pipe. Valves 546a and c-n flow control valves 546c-546n) are each fully opened. In step S104, the flow rate measurement value fb of the reference branch flow meter 547b is handled as the reference flow rate measurement value F, and the flow control valve 546b of the b system branch is operated. Even in such a valve opening / closing operation, the coating liquid containing the organic EL material flowing in the main pipe is completely supplied to the flow control valves 546a to 546n and the branch pipe flow meters 547a to 547n provided in the respective branch pipes. After passing, it is discharged from the nozzle 52n connected to the n-system branch pipe, and the same branch pipe flow rate setting is possible.

  In the branch flow rate setting mode process described above, the flow control valve 546 of the branch pipe provided with the reference branch flow meter 547 performs a flow control operation, and the flow control valve provided in a branch pipe other than the branch pipe. Each of 546 is fully open. However, the flow rate control valve 546 that performs the flow rate control operation in the above-described branch flow rate setting mode process is one of the flow rate control valves 546 provided in the branch pipes other than the branch pipe in which the reference branch flow meter 547 is provided. It does not matter if there is one.

  In the coating apparatus 1 described above, the two second opening / closing valves 548 and the third opening / closing valve 549 may be configured by one three-way valve valve. Specifically, instead of the second on-off valve 548 and the third on-off valve 549, the control unit 3 connects the connecting pipe connected to the downstream of the branch flow meter 547 provided in each branch pipe. A three-way valve that controls the flow path is installed. Then, during the actual flow rate measurement mode process and the coating operation, the control unit 3 causes the coating liquid flowing in the branch pipe to flow as it is to the nozzle 52 connected to the branch pipe. On the other hand, during the branch pipe flow rate measurement mode process, the control unit 3 causes the coating liquid flowing in each branch pipe to flow into the connecting pipe branched from the downstream of the branch pipe flowmeter 547 of the branch pipe. Flow to the branch pipe. As described above, when the three-way valve valve is used instead of the second on-off valve 548 and the third on-off valve 549, the number of valves provided in the coating apparatus 1 can be reduced and the same calibration work can be performed. It becomes possible.

  Moreover, in embodiment mentioned above, although the coating liquid which contains red organic EL material as an example among red, green, and blue is formed in the board | substrate P using several nozzle 52a-52n, A coating solution containing another organic EL material may be applied to the substrate P at the same time. Specifically, a coating solution containing red, green, and blue organic EL materials may be simultaneously applied to the substrate P using a plurality of nozzles for each color. In this case, since a set of a main pipe and a branch pipe connected to the main pipe is provided for each type of coating liquid to be applied, the connecting pipe described above is provided for each set (that is, for each type of coating liquid to be applied). It goes without saying that the same effects as described above can be obtained by performing the same calibration work.

  Further, a reference flow meter different from the branch flow meter 547 may be provided in the coating apparatus 1 described above. In this case, for example, a reference flow meter is installed on the main pipe between the filter 543 and the manifold 544. Then, the reference flow meter is priced based on the measured value of the actual discharge flow rate in the actual flow rate measurement mode process. In the subsequent branch flow rate setting mode process, the value indicated by the reference flow meter is used as a reference. It is handled as a flow rate measurement value F. Thus, even if the main pipe is provided with a reference flow meter serving as a reference for the flow rate of the coating liquid, the same calibration work can be performed.

  Further, by configuring the reference flow meter with a mass flow meter or the like, the above-described actual flow rate measurement mode process is not necessary. For example, when the reference flow meter is composed of a Coriolis mass flow meter or the like, it is not necessary to price the reference flow meter based on the measurement value of the actual discharge flow rate by the actual flow measurement mode processing described above. . Therefore, when the reference flow meter is composed of a mass flow meter or the like, an absolute evaluation like the flow rate setting method described above can be performed on the branch flow meter 547 without performing the actual flow rate measurement mode process described above. It becomes.

  In the above-described embodiment, each time the nozzle unit 50 linearly moves in the X-axis direction, the stage 21 is moved by a predetermined pitch in the Y-axis direction, so that the nozzle unit 50 and the stage 21 are relative to the Y-axis direction. However, the present invention is not limited to this. For example, each time the nozzle unit 50 linearly moves in the X-axis direction, the nozzle unit 50 is moved by a predetermined pitch in the Y-axis direction (that is, the organic EL coating mechanism 5 moves in the Y-axis direction). The relative positional relationship between the stage 21 and the stage 21 in the Y-axis direction may be changed. In this case, the liquid receiver 53 moves with the organic EL coating mechanism 5 by a predetermined pitch in the Y-axis direction.

  In the above-described embodiment, the example in which the coating apparatus 1 applies the coating liquid containing the organic EL material for forming the light emitting layer to the substrate P is used. It goes without saying that a coating liquid containing a molecular organic EL material and a polymer organic EL material emitting blue light can be applied. In addition, the coating apparatus of the present invention includes a coating solution containing, in addition to the organic light emitting layer material, other organic EL materials such as a hole transport layer material, a hole injection layer material, an electron transport layer material, and an electron injection layer material. It can also be used when coating.

  Specifically, when the coating apparatus 1 in the above-described embodiment applies a coating liquid containing a polymer organic EL material that emits red light out of red, green, and blue light, this coating process includes an organic EL device. It is an intermediate process of manufacturing. When manufacturing an organic EL device, a hole injection layer material coating, a hole transport material (for example, PEDOT) coating, a red light emitting organic EL material coating, a green light emitting organic EL material coating, a blue light emitting organic EL material coating There are coating processes such as application of an electron transport material and coating of an electron injection layer material, and the coating apparatus of the present invention can be used in any coating process.

  In addition, the shape, number, installation position, and the like of each component of the coating apparatus 1 described above are merely examples, and it goes without saying that the present invention can be realized even with other shapes, numbers, and installation positions.

  Moreover, in embodiment mentioned above, although the glass substrate was used as an example of a to-be-coated body, another member can also be used as a to-be-coated body. For example, a flexible substrate made of polyethylene terephthalate (PET), polycarbonate (PC), or the like may be used as the coating object of the coating apparatus 1.

  In the above-described embodiment, the manufacturing apparatus of an organic EL display device that applies a coating liquid containing an organic EL material as a coating liquid has been described as an example. However, the present invention can also be applied to other coating apparatuses. For example, the present invention can be applied to an apparatus for applying a fluorescent material used to manufacture a resist solution, a SOG (Spin On Glass) solution, or a PDP (plasma display panel). Further, the present invention can also be applied to an apparatus for applying a color material used for manufacturing a color filter configured in a liquid crystal cell in order to perform color display on a liquid crystal color display.

  Although the present invention has been described in detail above, the above description is merely illustrative of the present invention in all respects and is not intended to limit the scope thereof. It goes without saying that various improvements and modifications can be made without departing from the scope of the present invention.

  The flow rate setting method and the coating apparatus according to the present invention can facilitate the flow management of the coating apparatus, and are useful as a device for discharging a coating liquid from a plurality of nozzles, a flow management method for the device, and the like.

DESCRIPTION OF SYMBOLS 1 ... Coating apparatus 2 ... Substrate mounting apparatus 21 ... Stage 22 ... Turning part 23 ... Parallel movement table 24 ... Guide receiving part 25, 511 ... Guide member 3 ... Control part 5 ... Organic EL coating mechanism 50 ... Nozzle unit 51 ... Nozzle Moving mechanism 52 ... Nozzles 521 and 543 ... Filter 53 ... Liquid receiving part 54 ... Supply part 541 ... Supply source 542 ... Pressurizing part 544 ... Manifold 545 ... First on-off valve 546 ... Flow control valve 547 ... Branch pipe flow meter 548 ... second on-off valve 549 ... third on-off valve

Claims (18)

The coating liquid supplied from the single supply source through the main pipe is divided into a plurality of branch pipes, and the flow rate of the coating liquid flowing through the branch pipes is measured by the branch pipe flow rate measuring means respectively provided in the branch pipes. A method for setting a flow rate of a coating liquid in a coating apparatus that discharges the coating liquid from a nozzle connected to a branch pipe,
Using a connection pipe for connecting the upstream side of the branch pipe flow rate measuring means on the downstream side and the other of the branch pipes of the branch pipe flow rate measuring means in the branch pipe, and connecting the branch pipe flow measurement means in series, the source Supplying the coating liquid to the branch flow rate measuring means connected in series from the series supply step of discharging the supplied coating liquid from one of the nozzles;
In the state where the coating liquid is supplied to the branch flow rate measuring means connected in series in the serial supply step, a flow rate measurement adjusting step for adjusting the measurement result of each coating liquid flow rate in the branch pipe flow rate measuring means, Including flow rate setting method. A selective supply step of supplying the coating liquid supplied from the supply source to the main pipe only to one selected branch pipe selected from the plurality of branch pipes, and closing the supply of the coating liquid to the other branch pipes;
In a state where the coating liquid is supplied only to the selected branch pipe in the selective supply step, the measurement result by the branch pipe flow rate measuring means provided in the selected branch pipe and the actual result of the coating liquid discharged from the nozzle of the selected branch pipe. An actual flow rate measuring step for measuring the relationship between the discharge amount and
In the flow measurement adjustment step, the application of the branch flow rate measuring means provided in the selected branch pipe is measured in the state where the serial supply step supplies the coating liquid to the branch flow rate measurement means connected in series. The flow rate setting method according to claim 1, wherein the measurement result of the coating liquid flow rate in the other branch flow rate measuring means is adjusted with the liquid flow rate as a reference. At least one of the branch pipe flow rate measuring means measures the mass flow rate of the coating liquid flowing through the branch pipe,
In the flow measurement adjustment step, the coating liquid measured by the branch flow rate measuring unit that measures the mass flow rate in a state where the coating liquid is supplied to the branch flow rate measuring unit connected in series in the serial supply step. The flow rate setting method according to claim 1, wherein the measurement result of the coating liquid flow rate in the other branch flow rate measuring means is adjusted with reference to the flow rate. A selective supply step of supplying the coating liquid supplied from the supply source to the main pipe only to one selected branch pipe selected from the plurality of branch pipes, and closing the supply of the coating liquid to the other branch pipes;
In the state where the coating liquid is supplied only to the selected branch pipe in the selective supply step, the measurement result by the main flow rate measuring means for measuring the flow rate of the coating liquid flowing through the main pipe and the nozzle of the selected branch pipe are discharged. And an actual flow rate measuring step for measuring a relationship between the actual discharge amount of the coating liquid and
In the flow measurement adjustment step, in the state in which the serial supply step supplies the coating liquid to the branch flow rate measurement means connected in series, the coating liquid flow rate measured by the main flow rate measurement means is used as a reference. The flow rate setting method according to claim 1, wherein a measurement result of each coating liquid flow rate in the branch flow rate measuring unit is adjusted. The main pipe is provided with main flow rate measuring means for measuring the mass flow rate of the coating liquid flowing through the main pipe,
In the flow measurement adjustment step, in the state in which the serial supply step supplies the coating liquid to the branch flow rate measurement means connected in series, the coating liquid flow rate measured by the main flow rate measurement means is used as a reference. The flow rate setting method according to claim 1, wherein a measurement result of each coating liquid flow rate in the branch flow rate measuring unit is adjusted. Branch pipe flow rate adjusting means for adjusting the flow rate of the coating liquid flowing through the branch pipe to a predetermined flow rate according to the measurement result of the coating liquid flow rate by the branch pipe flow rate measuring means is provided in each of the plurality of branch pipes,
In the serial supply step, the branch flow rate measuring means and the branch flow rate adjusting means are connected in series, respectively, and the coating liquid is supplied from the supply source to the branch flow rate measuring means and the branch flow rate adjusting means connected in series. And discharging the supplied coating liquid from one of the nozzles,
In the flow rate measurement adjustment step, in the state where the serial supply step supplies the coating liquid to the branch flow rate measurement unit and the branch flow rate adjustment unit connected in series, the respective coating liquid flow rates in the branch flow rate measurement unit 6. The flow rate setting method according to claim 1, wherein a target flow rate value, which is an adjustment target of the branch flow rate adjusting means corresponding to the predetermined flow rate, is set based on the measurement result.   In the flow rate measurement adjustment step, a reference flow rate value serving as a reference and the branch flow rate measurement in the state where the series supply step supplies the coating liquid to the branch flow rate measurement unit and the branch flow rate adjustment unit connected in series. Relational expressions between the flow rate values indicated by the means are respectively derived, and based on the relational expressions, the flow rate value of the branch flow rate measuring means corresponding to the reference flow rate value indicating the predetermined flow rate is set as the target flow rate value. The flow rate setting method according to claim 6.   The flow rate setting method according to claim 7, wherein in the flow rate measurement adjustment step, the relational expression is derived for each type of coating liquid used in the coating apparatus, and the target flow rate value is set. In the series supply step, the reference flow rate is adjusted to be the predetermined flow rate by any one of the branch flow rate adjusting means connected in series so that the supplied coating solution flow rate becomes the predetermined flow rate. The flow control by means is fully opened,
In the flow rate measurement adjustment step, the flow rate value indicated by each of the branch flow rate measurement units in a state in which any one of the branch flow rate adjustment units adjusts the reference flow rate value to the predetermined flow rate. The flow rate setting method according to claim 6, wherein the flow rate setting method is set to the target flow rate value.   The flow rate setting method according to claim 9, wherein in the flow rate measurement adjustment step, the target flow rate value is set for each type of coating liquid used in the coating apparatus. Prior SL series supply step, after said plurality of supplying the coating liquid from said source to one of the branch pipes were the feed is sequentially flow to another branch pipe via the connecting pipe, the coating The flow rate setting method according to claim 1, wherein the coating liquid is discharged from the nozzle provided in a branch pipe that is the most downstream in the flow of the liquid. A coating apparatus that discharges coating liquid from a plurality of nozzles,
A single source for storing the coating liquid;
A plurality of nozzles for discharging the coating liquid;
A main for supplying the coating liquid from the supply source;
A plurality of branch pipes for diverting the coating liquid supplied from the main pipe and respectively supplying the plurality of nozzles;
A plurality of branch pipe flow rate measuring means provided on each of the branch pipes to measure the flow rate of the coating liquid flowing through the branch pipe;
A connecting pipe connecting the downstream side of the branch pipe flow rate measuring means in the branch pipe and the upstream side of the branch pipe flow rate measuring means in the other branch pipes;
A control unit for adjusting the measurement result of the coating liquid flow rate measured by the branch flow rate measuring means,
The control unit is configured such that the plurality of branch flow rate measuring means are connected in series via the branch pipe and the connecting pipe, and the coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series. A coating apparatus that adjusts the measurement result of each coating liquid flow rate in the branch flow rate measuring means in a state where the supplied coating liquid is discharged from one of the nozzles. In the control unit, the coating liquid supplied from the supply source to the main pipe is supplied only to one selected branch pipe selected from the plurality of branch pipes, and the supply of the coating liquid to the other branch pipes is closed. In the state, measure the relationship between the measurement result by the branch flow rate measuring means provided in the selected branch and the actual discharge amount of the coating liquid discharged from the nozzle of the selected branch,
The control unit is configured such that the plurality of branch flow rate measuring means are connected in series via the branch pipe and the connecting pipe, and the coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series. In the state where the supplied coating liquid is discharged from one of the nozzles, the other branch flow rate measuring means is based on the coating liquid flow rate measured by the branch flow rate measuring means provided in the selected branch pipe. The coating apparatus of Claim 12 which adjusts the measurement result of a coating liquid flow volume. Of the plurality of branch pipe flow rate measuring means, at least one is a mass flow meter that measures the mass flow rate of the coating liquid flowing through the branch pipe,
The control unit is configured such that the plurality of branch flow rate measuring means are connected in series via the branch pipe and the connecting pipe, and the coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series. In the state where the supplied coating liquid is discharged from one of the nozzles, the measurement result of the coating liquid flow rate in the other branch flow rate measuring means is adjusted based on the coating liquid flow rate measured by the mass flow meter. The coating apparatus according to claim 12. A main flow rate measuring means for measuring the flow rate of the coating liquid that is provided in the main pipe and flows through the main pipe is further provided,
In the control unit, the coating liquid supplied from the supply source to the main pipe is supplied only to one selected branch pipe selected from the plurality of branch pipes, and the supply of the coating liquid to the other branch pipes is closed. In the state, measure the relationship between the measurement result by the main flow rate measuring means and the actual discharge amount of the coating liquid discharged from the nozzle of the selected branch pipe,
The control unit is configured such that the plurality of branch flow rate measuring means are connected in series via the branch pipe and the connecting pipe, and the coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series. In the state where the supplied coating liquid is discharged from one of the nozzles, the measurement result of the coating liquid flow rate in the branch flow rate measuring unit is adjusted based on the coating liquid flow rate measured by the main flow rate measuring unit. The coating apparatus according to claim 12. A mass flow meter that is provided in the main pipe and measures the mass flow rate of the coating liquid flowing through the main pipe,
The control unit is configured such that the plurality of branch flow rate measuring means are connected in series via the branch pipe and the connecting pipe, and the coating liquid is supplied from the supply source to the branch flow rate measuring means connected in series. In the state where the supplied coating liquid is discharged from one of the nozzles, the measurement result of the coating liquid flow rate in the branch flow rate measuring unit is adjusted with reference to the coating liquid flow rate measured by the mass flow meter. The coating device according to claim 12. A plurality of branch pipe flow rate adjusting means each provided in the branch pipe, for adjusting the flow rate of the coating liquid flowing through the branch pipe to a predetermined flow rate according to the measurement result of the flow rate of the coating liquid by the branch pipe flow rate measuring means,
In the control unit, the plurality of branch flow rate measuring means and the branch flow rate adjusting means are respectively connected in series via the branch pipe and the connecting pipe, and the branch flow rate measuring means and the branch flow rate connected in series from the supply source. In a state where the coating liquid is supplied to the adjusting means and the supplied coating liquid is discharged from one of the nozzles, the predetermined liquid flow rate is measured based on the measurement result of each coating liquid flow rate in the branch flow rate measuring means. The coating apparatus according to any one of claims 12 to 16, wherein a target flow rate value that is an adjustment target of the branch pipe flow rate adjusting unit corresponding to the flow rate of each is set. A valve provided on each of the branch pipes for switching whether to flow the coating liquid flowing through the branch pipe to the connection pipe or to the nozzle of the branch pipe according to the control of the control unit;
The control unit supplies the coating liquid from the supply source to one of the plurality of branch pipes, switches the valve, and sequentially flows the supply liquid to other branch pipes via the connection pipe. The coating apparatus according to claim 12, wherein the plurality of branch flow rate measuring units are respectively connected in series by discharging the coating liquid from the nozzle provided in the branch pipe that is most downstream in the flow of the coating liquid. .

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