JP4974160B2 - Continuous degassing deaerator - Google Patents

Description

  The present invention relates to a continuous deaeration and deaeration apparatus that removes a gas component from a liquid, and in particular, prevents generation of fine bubbles due to shearing with a take-out pipe, and the tip of the liquid take-out pipe is buried in the liquid. The present invention relates to a continuous deaeration and deaeration device that can eliminate the structure and facilitate maintenance such as cleaning.

For example, it takes a long time to degas small bubbles contained in a high viscosity, and in general, the bubbles are often degassed by being left overnight.
Moreover, when defoaming is attempted in a short time, a batch type defoaming apparatus is used, but an efficient defoaming apparatus aimed at continuous mass processing is demanded.

In the case of continuous processing, there is a device that rotates a liquid in a vacuum can and defoams by centrifugal force. For example, a continuous deaeration and defoaming device disclosed in Patent Document 1 below is known.
This continuous degassing defoaming device continuously injects liquid into a rotating body in a vacuum can and defoams the liquid by applying centrifugal force. At the same time, the rotating liquid is taken out from the inside through a tube. It has a structure to take out.

However, in this conventional continuous deaeration device, there is a problem in that fine liquid bubbles are generated in the liquid because the liquid outlet is in contact with the liquid rotating at a high speed and shear is applied.
Further, in the production of food, the tip of the take-out tube is buried in the liquid, and there is a problem that the tip of the tube cannot be cleaned.
JP 2000-246008 A

  In view of the problems of the conventional continuous deaeration and deaeration apparatus, the present invention has a structure that prevents the generation of fine bubbles due to shearing with the take-out pipe and that the tip of the liquid take-out pipe is buried in the liquid. An object of the present invention is to provide a continuous deaeration and deaeration device that can easily eliminate maintenance such as cleaning.

In order to achieve the above object, a continuous degassing defoaming apparatus according to the present invention is a continuous degassing defoaming apparatus in which liquid is continuously injected into a rotating cylinder and defoamed by applying centrifugal force to the liquid. And at least one annular groove serving as a liquid pool is formed inside, and a disk that rotates together with the rotating cylinder is provided so that the peripheral edge is submerged in the annular groove, and directed toward the center of rotation at the top of the annular groove. the length of the formed side wall by greater than the length of the side wall which is formed toward the center of rotation to the bottom, the forming a sidewall of the top in the wall have higher than the side wall of the bottom, the top of the A liquid supply unit for supplying liquid onto the disk is provided on the rotation center side surrounded by the side wall.

  In this case, a plurality of disks can be provided in one annular groove.

  Moreover, the reverse funnel-shaped rotation guide can be extended from the lowest side wall of the annular groove.

  Moreover, a reverse funnel-shaped liquid receiving guide can be installed as a fixed side under the lowermost side wall of the annular groove.

According to the continuous deaeration and deaeration apparatus of the present invention, in the continuous deaeration and deaeration apparatus that continuously injects liquid into the rotating cylinder and defoams by applying centrifugal force to the liquid, the liquid pool is stored inside the rotating cylinder. And at least one annular groove is formed, and a disk that rotates together with the rotating cylinder is provided so that the peripheral edge is submerged in the annular groove, and the length of the side wall formed at the uppermost part of the annular groove toward the rotation center. by larger than the length of the sidewall formed toward the center of rotation at the bottom of the form a side wall of the top in the wall have higher than the bottom of the side wall, said enclosed by the top of the side wall Since a liquid supply unit that supplies liquid on the disk is provided on the rotation center side, the liquid supplied from the liquid supply unit is moved to the annular groove by centrifugal force, and defoamed by centrifugal force above the circular groove disk. And defoaming the disk as a dam plate The liquid alone was preferably under, can be made to flow naturally without giving shear from the inside of the bottom of the side wall.
As a result, it is possible to prevent generation of fine bubbles due to shearing of the take-out pipe as in the prior art, and to eliminate the structure in which the tip of the take-out pipe is buried in the liquid, thereby facilitating maintenance such as cleaning.
In this case, by providing a plurality of annular grooves and disks on the rotating cylinder, the liquid can be degassed continuously in a stepwise manner.

  Further, by providing a plurality of disks in one annular groove, the liquid can be degassed minutely and stepwise.

  In addition, by extending a reverse funnel-shaped rotation guide from the lowest side wall of the annular groove, the defoamed liquid that flows down in a state where centrifugal force is applied can be guided radially and flowed smoothly. it can.

  In addition, by installing a reverse funnel-shaped liquid receiving guide as a fixed side under the lowermost side wall of the annular groove, the defoamed liquid that flows down with centrifugal force applied is guided radially. It can flow smoothly.

  DESCRIPTION OF EMBODIMENTS Hereinafter, embodiments of a continuous deaeration and deaeration apparatus according to the present invention will be described with reference to the drawings.

In FIG. 1, one Example of the continuous deaeration deaerator of this invention is shown.
This continuous degassing deaerator is a device that continuously injects liquid into the rotating cylinder 1 and applies a centrifugal force to the liquid A to defoam. An annular groove 2 is formed, and a disk 3 that rotates together with the rotating cylinder 1 is provided so that a peripheral edge is submerged in the annular groove 2, and an uppermost side wall 21 of the annular groove 2 is formed higher than a lowermost side wall 22. The liquid supply part 4 for supplying the liquid A onto the disk 3 is provided inside the uppermost side wall 21.

The rotating cylinder 1 is disposed inside a vacuum can 5 installed as a fixed side, and is connected via the disk 3 to a rotating shaft 6 penetrating the vacuum can 5 from above.
The vacuum can 5 is connected to a vacuum pump (not shown), and crushes and extinguishes the bubbles B separated from the liquid A by centrifugal force by making the inside vacuum.
In addition, an intermediate cylinder 7 is fixed inside the vacuum can 5 so as to surround the rotating cylinder 1, and a lower portion of the intermediate cylinder 7 is folded inward and spreads downward below the rotating cylinder 1. A funnel-shaped liquid receiving guide 71 is formed.

In addition, as shown in FIG. 2, one or two annular grooves 2 that form a liquid pool during rotation are formed inside the rotating cylinder 1, and each annular groove 2 is coaxial with the rotating cylinder 1. The disc 3 is provided so that its peripheral edge is immersed in the liquid pool of the annular groove 2.
A reverse funnel-shaped rotation guide 23 extending downward is extended from the lowermost side wall 22 of the annular groove 2, and the liquid receiving guide 71 of the intermediate cylinder 7 is disposed outside the rotation guide 23. Has been.

The disk 3 is directly fixed to the rotating shaft 6 and the rotating cylinder 1 is connected to the rotating shaft 6 via a connecting member 31. The disk 3 and the rotating cylinder 1 are integrally rotated at a high speed by a motor (not shown). To do.
Moreover, as shown in FIG. 3, it is also possible to provide a plurality of disks 3 in one annular groove 2, whereby the liquid A can be degassed minutely and stepwise.
Note that a vent (not shown) is provided near the rotary shaft 6 of the disk 3 so as to communicate with the disk 3 and maintain a vacuum.

Next, the operation of the continuous deaeration and deaeration device of this embodiment will be described.
The processing liquid A is supplied onto the disk 3 from the inside of the uppermost side wall 21 of the annular groove 2 with respect to the rotating cylinder 1 that rotates at high speed.
The supplied liquid A moves outward in the form of a thin film on the disk 3 by centrifugal force, is defoamed by centrifugal force in the annular groove 2, and the defoamed liquid A is separated to the outside and the foam B is separated to the inside. .
The liquid A in the annular groove 2 rotates at a high speed, and forms a liquid surface in which a disk 3 provided in the center of the annular groove 2 is buried, as shown in FIGS.
Thereby, the foam B floating inside the liquid surface stays at the position without passing through the disk 3 serving as the weir plate, and is crushed and disappeared by the vacuum of the vacuum can 5.
On the other hand, the liquid A after defoaming moves downward through the outside of the disk 3, overflows from the rotating cylinder 1, reaches the liquid receiving guide 71 on the fixed side, and then drops due to gravity.

  In this case, as shown in FIG. 2, when a plurality of annular grooves 2 and disks 3 are provided in the rotating cylinder 1, such defoaming of the liquid is continuously performed in a stepwise manner.

In addition, as shown in FIG. 3, when a plurality of disks 3 are provided in one annular groove 2, the liquid A that has passed through the first disk 3 further passes between the second disk 3. Defoamed.
Then, the liquid A after defoaming moves further down through the second disk 3, and the bubbles B floating inside the liquid surface are crushed by the vacuum of the vacuum can 5 without going through the disk 3. Disappear.

[Experimental Example 1]
A food additive CMC (sodium carboxymethylcellulose, Nichirin Chemical Industry Co., Ltd., Kikkolate F-120) was dissolved in water in a tank equipped with a stirrer to obtain a raw material solution.
This raw material liquid was introduced into the continuous degassing deaerator of this example with a pump to obtain a sample after defoaming discharged from the continuous degassing deaerator.
A sample of the raw material liquid and a sample of the defoamed liquid were placed under vacuum with a desiccator, and volume expansion was measured to obtain a deaeration rate.
The results are shown in Table 1 below.
The deaeration rate was calculated as follows.
Degassing rate% = (expanded volume of raw material−expanded volume after defoaming) ÷ expanded volume of raw material × 100

Thus, the continuous degassing deaerator of this embodiment is the continuous degassing deaerator in which the liquid A is continuously injected into the rotating cylinder 1 and defoamed by applying centrifugal force to the liquid A. At least one annular groove 2 that forms a liquid pool, and a disk 3 that rotates together with the rotating cylinder 1 is provided so that the peripheral edge is submerged in the annular groove 2. 21 is formed higher than the lowermost side wall 22, and the liquid supply part 4 for supplying the liquid A is provided on the disk 3 inside the uppermost side wall 21, so that the liquid A supplied from the liquid supply part 4 is subjected to centrifugal force. Is moved to the annular groove 2 and defoamed by centrifugal force above the disk 3 of the annular groove 2, and only the liquid A that has been defoamed is passed through the disk 3 as a weir plate. It can flow down naturally without giving shear from the inside.
As a result, it is possible to prevent generation of fine bubbles due to shearing of the take-out pipe as in the prior art, and to eliminate the structure in which the tip of the take-out pipe is buried in the liquid, thereby facilitating maintenance such as cleaning.
In this case, as shown in FIG. 2, by providing a plurality of annular grooves 2 and disks 3 in the rotating cylinder 1, the liquid A can be degassed continuously in a stepwise manner.

  Further, as shown in FIG. 3, by providing a plurality of disks 3 in one annular groove 2, the defoaming of the liquid A can be performed minutely and stepwise.

Further, by extending a reverse funnel-shaped rotation guide 23 from the lowermost side wall 22 of the annular groove 2, the defoamed liquid A flowing down in a state where centrifugal force is applied is radially guided to smoothly. Can flow down.
Further, by installing a reverse funnel-shaped liquid receiving guide 71 as a fixed side under the lowermost side wall 22 of the annular groove 2, the defoamed liquid A that flows down in a state where centrifugal force is applied is radial. It is possible to smoothly flow down by guiding to.

  As mentioned above, although the continuous deaeration deaeration apparatus of this invention was demonstrated based on the Example, this invention is not limited to the structure described in the said Example, In the range which does not deviate from the meaning, the The configuration can be changed.

The continuous deaeration and deaeration device of the present invention prevents the generation of fine bubbles due to shearing with the take-out pipe, and eliminates the structure in which the tip of the liquid take-out pipe is buried in the liquid, facilitating maintenance such as cleaning. For example, it can be suitably used for the defoaming of viscous products in the food industry, the pharmaceutical industry, and the chemical industry.

It is sectional drawing which shows 1st Example of the continuous deaeration deaerator of this invention. It is sectional drawing which shows the 2nd Example. It is sectional drawing which shows the 3rd Example.

DESCRIPTION OF SYMBOLS 1 Rotating cylinder 2 Annular groove 21 Uppermost side wall 22 Lowermost side wall 23 Rotating guide 3 Disc 31 Connecting member 4 Liquid supply part 5 Vacuum can 6 Rotating shaft 7 Intermediate cylinder 71 Liquid receiving guide

Claims (4)

In the continuous deaeration and deaeration device that continuously injects liquid into the rotating cylinder and defoams by applying centrifugal force to the liquid, and forming at least one annular groove serving as a liquid pool inside the rotating cylinder, A disk that rotates with the rotating cylinder is provided so that the peripheral edge is immersed in the annular groove, and the length of the side wall formed in the uppermost part of the annular groove toward the rotation center is formed in the lowermost part in the direction of the rotation center. by greater than the length of the side wall, the top of the upper portion of the side wall is formed in the wall have higher than the side wall of the bottom, the center of rotation side surrounded by the top of the side wall, solution supplying liquid onto the disk A continuous deaeration and deaeration apparatus comprising a supply unit.   The continuous deaeration apparatus according to claim 1, wherein a plurality of disks are provided in one annular groove.   The continuous deaeration and deaeration apparatus according to claim 1 or 2, wherein a reverse funnel-shaped rotation guide is extended from a lowermost side wall of the annular groove.   4. A continuous deaeration / deaeration apparatus according to claim 1, wherein a reverse funnel-shaped liquid receiving guide is provided as a fixed side under the lowermost side wall of the annular groove.

Images