JP4869478B2 - 間隙率を求める装置及び方法 - Google Patents
間隙率を求める装置及び方法 Download PDFInfo
- Publication number
- JP4869478B2 JP4869478B2 JP2000567934A JP2000567934A JP4869478B2 JP 4869478 B2 JP4869478 B2 JP 4869478B2 JP 2000567934 A JP2000567934 A JP 2000567934A JP 2000567934 A JP2000567934 A JP 2000567934A JP 4869478 B2 JP4869478 B2 JP 4869478B2
- Authority
- JP
- Japan
- Prior art keywords
- room
- pressure
- substance
- temperature
- porosity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims abstract description 40
- 239000000126 substance Substances 0.000 claims abstract description 62
- 239000000758 substrate Substances 0.000 claims abstract description 31
- 238000005259 measurement Methods 0.000 claims abstract description 20
- 230000003287 optical effect Effects 0.000 claims abstract description 20
- 239000000463 material Substances 0.000 claims description 33
- 238000004458 analytical method Methods 0.000 claims description 23
- 238000002336 sorption--desorption measurement Methods 0.000 claims description 9
- 238000002159 adsorption--desorption isotherm Methods 0.000 claims description 7
- 239000004020 conductor Substances 0.000 claims description 5
- 239000013013 elastic material Substances 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 2
- 238000001704 evaporation Methods 0.000 claims 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract description 48
- 239000010408 film Substances 0.000 abstract description 28
- 239000010409 thin film Substances 0.000 abstract description 21
- 239000011148 porous material Substances 0.000 abstract description 7
- 230000001066 destructive effect Effects 0.000 abstract description 5
- 238000011065 in-situ storage Methods 0.000 abstract description 2
- 238000000572 ellipsometry Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 40
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 15
- 238000009826 distribution Methods 0.000 description 15
- 229910004298 SiO 2 Inorganic materials 0.000 description 11
- 238000001179 sorption measurement Methods 0.000 description 11
- 239000010410 layer Substances 0.000 description 9
- 235000012239 silicon dioxide Nutrition 0.000 description 9
- 230000005499 meniscus Effects 0.000 description 8
- 238000005229 chemical vapour deposition Methods 0.000 description 7
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 5
- 238000000691 measurement method Methods 0.000 description 5
- 239000010453 quartz Substances 0.000 description 5
- 229910052710 silicon Inorganic materials 0.000 description 5
- 239000010703 silicon Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 238000003795 desorption Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000011800 void material Substances 0.000 description 3
- 239000003463 adsorbent Substances 0.000 description 2
- 239000003989 dielectric material Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 229910052814 silicon oxide Inorganic materials 0.000 description 2
- 238000004088 simulation Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000005094 computer simulation Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000007405 data analysis Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 238000004518 low pressure chemical vapour deposition Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000012454 non-polar solvent Substances 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/21—Polarisation-affecting properties
- G01N21/211—Ellipsometry
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N2015/0846—Investigating permeability, pore-volume, or surface area of porous materials by use of radiation, e.g. transmitted or reflected light
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/21—Polarisation-affecting properties
Landscapes
- Chemical & Material Sciences (AREA)
- Immunology (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pathology (AREA)
- General Physics & Mathematics (AREA)
- Dispersion Chemistry (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Length Measuring Devices By Optical Means (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Formation Of Insulating Films (AREA)
- Testing Or Measuring Of Semiconductors Or The Like (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US9824798P | 1998-08-28 | 1998-08-28 | |
| US60/098,247 | 1998-08-28 | ||
| PCT/EP1999/006299 WO2000012999A1 (en) | 1998-08-28 | 1999-08-27 | Apparatus and method for determining porosity |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011081804A Division JP2011237411A (ja) | 1998-08-28 | 2011-04-01 | 間隙率を求める装置及び方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2002523773A JP2002523773A (ja) | 2002-07-30 |
| JP4869478B2 true JP4869478B2 (ja) | 2012-02-08 |
Family
ID=22268341
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000567934A Expired - Lifetime JP4869478B2 (ja) | 1998-08-28 | 1999-08-27 | 間隙率を求める装置及び方法 |
| JP2011081804A Pending JP2011237411A (ja) | 1998-08-28 | 2011-04-01 | 間隙率を求める装置及び方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011081804A Pending JP2011237411A (ja) | 1998-08-28 | 2011-04-01 | 間隙率を求める装置及び方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US6319736B1 (enExample) |
| EP (1) | EP1032816B1 (enExample) |
| JP (2) | JP4869478B2 (enExample) |
| AT (1) | ATE475879T1 (enExample) |
| AU (1) | AU5855799A (enExample) |
| DE (1) | DE69942632D1 (enExample) |
| WO (1) | WO2000012999A1 (enExample) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1172847A3 (en) | 2000-07-10 | 2004-07-28 | Interuniversitair Micro-Elektronica Centrum Vzw | A method to produce a porous oxygen-silicon layer |
| US7042570B2 (en) * | 2002-01-25 | 2006-05-09 | The Regents Of The University Of California | Porous thin film time-varying reflectivity analysis of samples |
| EP1369682A3 (en) * | 2002-06-07 | 2004-12-01 | Interuniversitair Microelektronica Centrum Vzw | A method for wafer level detection of integrity of a layer |
| US7016028B2 (en) | 2002-06-07 | 2006-03-21 | Interuniversitair Microelektronica Centrum (Imec) | Method and apparatus for defect detection |
| EP1722213B1 (en) * | 2005-05-12 | 2019-10-16 | IMEC vzw | Method for the quantification of hydrophilic properties of porous materials |
| JP4528279B2 (ja) * | 2005-05-12 | 2010-08-18 | アイメック | 多孔性材料の親水性の定量化のための方法 |
| FR2886015B1 (fr) * | 2005-05-18 | 2007-07-13 | Commissariat Energie Atomique | Procede de mesure de la porosite par ellipsometrie et dispositif mettant en oeuvre un tel procede |
| US7363161B2 (en) * | 2005-06-03 | 2008-04-22 | Baker Hughes Incorporated | Pore-scale geometric models for interpretation of downhole formation evaluation data |
| GB0516477D0 (en) * | 2005-08-11 | 2005-09-14 | Optical Reference Systems Ltd | Apparatus for measuring semiconductor physical characteristics |
| DE602006015595D1 (de) * | 2005-12-22 | 2010-09-02 | Imec | Verfahren zur Bestimmung der Lösungsmitteldurchlässigkeit von Filmen |
| US7808657B2 (en) * | 2007-06-28 | 2010-10-05 | International Business Machines Corporation | Wafer and stage alignment using photonic devices |
| JP5555908B2 (ja) * | 2007-08-08 | 2014-07-23 | 独立行政法人産業技術総合研究所 | 光学的測定室 |
| JP5120927B2 (ja) * | 2007-08-08 | 2013-01-16 | 独立行政法人産業技術総合研究所 | 薄膜の物性評価方法および評価装置 |
| US7907264B1 (en) * | 2007-09-07 | 2011-03-15 | Kla-Tencor Corporation | Measurement of thin film porosity |
| RU2374625C1 (ru) * | 2008-05-05 | 2009-11-27 | Институт физики полупроводников Сибирского отделения Российской академии наук | Устройство для определения пористых характеристик тонких слоев (варианты) |
| FR2948192B1 (fr) | 2009-07-20 | 2011-07-22 | Commissariat Energie Atomique | Procede de caracterisation optique |
| US9618441B2 (en) | 2010-04-30 | 2017-04-11 | National University Of Singapore | Determination of pore size in porous materials by evaporative mass loss |
| WO2012012437A2 (en) * | 2010-07-20 | 2012-01-26 | The Regents Of The University Of California | Temperature response sensing and classification of analytes with porous optical films |
| US9546943B1 (en) * | 2015-03-21 | 2017-01-17 | J.A. Woollam Co., Inc | System and method for investigating change in optical properties of a porous effective substrate surface as a function of a sequence of solvent partial pressures at atmospheric pressure |
| US10281263B2 (en) | 2016-05-02 | 2019-05-07 | Kla-Tencor Corporation | Critical dimension measurements with gaseous adsorption |
| US10041873B2 (en) * | 2016-05-02 | 2018-08-07 | Kla-Tencor Corporation | Porosity measurement of semiconductor structures |
| US10145674B2 (en) | 2016-05-02 | 2018-12-04 | Kla-Tencor Corporation | Measurement of semiconductor structures with capillary condensation |
| CN107552258B (zh) * | 2016-07-01 | 2019-06-07 | 江苏鲁汶仪器有限公司 | 气体喷射装置 |
| CN106990255B (zh) * | 2017-04-07 | 2018-08-28 | 鲁汶仪器有限公司(比利时) | 样品分析系统 |
| WO2019100070A1 (en) * | 2017-11-20 | 2019-05-23 | Energy Everywhere, Inc. | Method and system for pervoskite solar cell with scaffold structure |
| CN109164030A (zh) * | 2018-10-17 | 2019-01-08 | 西南交通大学 | 一种用于观测岩石吸水渗透过程的实验装置 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0579973A (ja) * | 1991-09-20 | 1993-03-30 | Olympus Optical Co Ltd | 金属微粒子の光学定数測定方法 |
| JPH0693972A (ja) * | 1992-09-11 | 1994-04-05 | Seiko Epson Corp | マイクロポンプ及びその製造方法 |
| JPH08304204A (ja) * | 1995-05-12 | 1996-11-22 | Mitsubishi Cable Ind Ltd | ダイヤフラムユニットの作製方法及びそのダイヤフラムユニットを用いた圧力センサ |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3976450A (en) * | 1973-01-02 | 1976-08-24 | Roland Marcote | Gas sample preparation system and method |
| US4246775A (en) * | 1979-06-08 | 1981-01-27 | Philip Morris Incorporated | Porosity measuring apparatus and perforating system using same |
| US4304122A (en) * | 1980-05-06 | 1981-12-08 | E. I. Du Pont De Nemours And Company | Deep well simulator |
| US4389878A (en) * | 1981-05-01 | 1983-06-28 | The Dow Chemical Company | Dynamic gas transmission measuring apparatus |
| IT1138019B (it) * | 1981-07-09 | 1986-09-10 | Erba Strumentazione | Procedimento e apparecchiatura per l'effettuazione di analisi porosimetriche |
| GB8313635D0 (en) * | 1983-05-17 | 1983-06-22 | Whatman Reeve Angel Plc | Porosimeter |
| US4531404A (en) * | 1983-12-29 | 1985-07-30 | Mobil Oil Corporation | Flow cell assembly |
| US5002399A (en) | 1987-07-23 | 1991-03-26 | Mufit Akinc | Thermoporosimeter |
| DE4003619A1 (de) * | 1990-02-07 | 1991-08-14 | Bosch Gmbh Robert | Mikroventil |
| US5342580A (en) | 1990-04-17 | 1994-08-30 | Alan Brenner | Apparatus and method for measuring the amount of gas adsorbed on or desorbed from a solid and reactions of a gas with a solid |
| SE9504417D0 (sv) | 1995-12-11 | 1995-12-11 | Siemens Elema Ab | Metod för att bestämma koncentrationen av en specifik gas och en analysapparat |
| US6245690B1 (en) * | 1998-11-04 | 2001-06-12 | Applied Materials, Inc. | Method of improving moisture resistance of low dielectric constant films |
-
1999
- 1999-08-27 AU AU58557/99A patent/AU5855799A/en not_active Abandoned
- 1999-08-27 JP JP2000567934A patent/JP4869478B2/ja not_active Expired - Lifetime
- 1999-08-27 EP EP99946042A patent/EP1032816B1/en not_active Expired - Lifetime
- 1999-08-27 US US09/529,390 patent/US6319736B1/en not_active Expired - Lifetime
- 1999-08-27 AT AT99946042T patent/ATE475879T1/de not_active IP Right Cessation
- 1999-08-27 DE DE69942632T patent/DE69942632D1/de not_active Expired - Lifetime
- 1999-08-27 WO PCT/EP1999/006299 patent/WO2000012999A1/en not_active Ceased
-
2001
- 2001-08-16 US US09/931,419 patent/US6435008B2/en not_active Expired - Lifetime
-
2011
- 2011-04-01 JP JP2011081804A patent/JP2011237411A/ja active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0579973A (ja) * | 1991-09-20 | 1993-03-30 | Olympus Optical Co Ltd | 金属微粒子の光学定数測定方法 |
| JPH0693972A (ja) * | 1992-09-11 | 1994-04-05 | Seiko Epson Corp | マイクロポンプ及びその製造方法 |
| JPH08304204A (ja) * | 1995-05-12 | 1996-11-22 | Mitsubishi Cable Ind Ltd | ダイヤフラムユニットの作製方法及びそのダイヤフラムユニットを用いた圧力センサ |
Also Published As
| Publication number | Publication date |
|---|---|
| EP1032816A1 (en) | 2000-09-06 |
| JP2002523773A (ja) | 2002-07-30 |
| WO2000012999A1 (en) | 2000-03-09 |
| JP2011237411A (ja) | 2011-11-24 |
| ATE475879T1 (de) | 2010-08-15 |
| US6319736B1 (en) | 2001-11-20 |
| DE69942632D1 (de) | 2010-09-09 |
| EP1032816B1 (en) | 2010-07-28 |
| US20010054306A1 (en) | 2001-12-27 |
| US6435008B2 (en) | 2002-08-20 |
| AU5855799A (en) | 2000-03-21 |
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