JP4668572B2 - Method for producing containerized beverage - Google Patents

Method for producing containerized beverage Download PDF

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JP4668572B2
JP4668572B2 JP2004255727A JP2004255727A JP4668572B2 JP 4668572 B2 JP4668572 B2 JP 4668572B2 JP 2004255727 A JP2004255727 A JP 2004255727A JP 2004255727 A JP2004255727 A JP 2004255727A JP 4668572 B2 JP4668572 B2 JP 4668572B2
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beverage
container
sterilized
bottle
hot water
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JP2006069624A (en
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繁 坂井
克己 千本
健 岩下
亮 阿部
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Toyo Seikan Kaisha Ltd
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Description

本発明は、容器詰め飲料、特に容器詰め茶飲料の製造方法に関する。 The present invention is packed beverage, a method for manufacturing a particular packaged tea beverage.

従来PETボトル詰めの茶飲料や酸性飲料等の容器詰め飲料の製造法としてアセプテイック充填法と呼ばれる方法が知られている。この方法は、予め熱交換等の手段により高温短時間殺菌した後常温まで急速冷却した飲料を、過酸化水素や過酢酸等の薬剤で殺菌し無菌水で洗浄した耐熱性のない容器に無菌環境を維持した中で常温で充填・密封するものである。   Conventionally, a method called an aseptic filling method is known as a method for producing a container-packed beverage such as a PET bottled tea beverage or an acidic beverage. In this method, beverages that have been sterilized at high temperature for a short time by means such as heat exchange and then rapidly cooled to room temperature are sterilized with chemicals such as hydrogen peroxide and peracetic acid and washed with sterile water in a non-heat resistant container. Fill and seal at room temperature while maintaining

この方法は、容器殺菌のための薬剤処理装置および殺菌用薬剤が必要であり、また容器洗浄のための洗浄装置およびに大量の無菌水が必要である上に、飲料の加熱殺菌後常温まで急速冷却する冷却装置が必要であり、これらの工程を実現するための装置およびその制御が大がかりとなる問題点がある。   This method requires a chemical treatment device for sterilizing the container and a sterilizing chemical, and also requires a large amount of sterile water for the cleaning device for cleaning the container, and after the heat sterilization of the beverage, A cooling device for cooling is necessary, and there is a problem that a device for realizing these steps and its control become large.

またこれら容器詰め飲料の製造方法としてホットパックと呼ばれる方法が知られている。1例として特許文献1および2を挙げる。この方法は、水洗浄した耐熱性のある容器に、予め加熱殺菌した飲料をクリーンルーム内で汚染の少ない環境に制御された環境下で充填温度85℃で充填・密封後、30秒程度の転倒殺菌およびパストライザーでの75℃、3分の加熱殺菌を行った後常温に冷却するものである。   In addition, a method called hot pack is known as a method for producing these container-packed beverages. As an example, Patent Documents 1 and 2 are given. In this method, a water-washed heat-resistant container is filled with a pre-heated and sterilized beverage in an environment controlled to a low contamination environment in a clean room at a filling temperature of 85 ° C. and then sterilized for about 30 seconds. In addition, the pasteurizer is sterilized by heating at 75 ° C. for 3 minutes and then cooled to room temperature.

この方法は、充填・密封後の飲料の容器のヘッドスペースが飲料の冷却により減圧することによる容器の凹みを防止できるだけの容器の減圧変形耐性(強度)が必要である上に、充填・密封後のパストライザーによる加熱殺菌工程が大がかりとなり、また高温設備が多く作業環境が悪いという問題点がある。   This method requires the container to have a vacuum deformation resistance (strength) sufficient to prevent the depression of the container due to the decompression of the head space of the beverage container after filling and sealing by cooling the beverage, and after filling and sealing. There are problems that the heat sterilization process by the pastorizer becomes large, and there are many high-temperature facilities and the working environment is bad.

また、アセプテイック充填法の1種として、特許文献3に開示された酸性飲料のPETボトル充填法がある。この方法は、倒立状態に保持されたPETボトルの口部から65℃ないし85℃の熱水を間欠的に噴射して少なくともボトル内壁全面を洗浄し、次いで加熱殺菌された酸性飲料を無菌環境内でボトルに常温で充填し、密封するものである。この方法によれば、容器の薬剤による殺菌処理工程と無菌水による洗浄工程をより簡単な熱水による加熱殺菌処理によって置換することができる点で有利であるが、飲料の加熱殺菌後常温まで急速冷却するための装置およびその制御が大がかりとなる問題点は解消されていない。
特開2001−278225号公報 特開平8−309841号公報 特許第2844983号公報
Further, as one type of aseptic filling method, there is a PET bottle filling method for acidic beverages disclosed in Patent Document 3. In this method, hot water at 65 ° C. to 85 ° C. is intermittently sprayed from the mouth of a PET bottle held in an inverted state to wash at least the entire inner wall of the bottle, and then the heat-sterilized acidic beverage is placed in a sterile environment. The bottle is filled at room temperature and sealed. This method is advantageous in that it can replace the sterilization process of the container with the chemical and the cleaning process with sterile water by a simpler heat sterilization process with hot water. The problem that the apparatus for cooling and its control become a major issue has not been solved.
JP 2001-278225 A JP-A-8-309841 Japanese Patent No. 2844983

本発明は、従来の容器詰め飲料の製造方法における上記問題点にかんがみなされたものであって、アセプテイック充填法に対しては薬剤や無菌水の使用を不要とするとともに飲料の加熱殺菌後常温まで急速冷却するための装置およびその制御を簡素化することにより設備の簡素化を図るとともに、ホットパック法に対しては容器の減圧変形耐性に関する条件を緩和するとともに充填・密封後の加熱殺菌工程をなくし設備を簡素化し作業環境を改善することができる新規な容器詰め飲料の製造方法を提供しようとするものである。   The present invention has been considered in view of the above-mentioned problems in the conventional method for producing a container-packed beverage, and does not require the use of chemicals or sterile water for the aseptic filling method, and after the beverage is heat-sterilized to room temperature. The equipment for rapid cooling and its control are simplified to simplify the equipment, and the hot pack method relaxes the conditions related to the resistance to vacuum deformation of the container and the heat sterilization process after filling and sealing. It is an object of the present invention to provide a novel method for producing a container-packed beverage that can simplify equipment and improve the working environment.

上記目的を達成するため、本発明者らは、鋭意研究と実験を重ねた結果、容器内容物である飲料をpH4.6以上の低酸性飲料中カテキン含有量が30mg%以上の緑茶、ウーロン茶等の茶飲料およびpH4.6未満の酸性飲料に限定すれば、薬剤による容器の殺菌を必要とせず、飲料の加熱殺菌後の常温までの急速冷却を必要とせず、また容器の減圧耐性に関する条件を緩和するとともに充填・密封後の加熱殺菌工程をなくすことができることを見出し、本発明に到達した。   In order to achieve the above object, the present inventors have conducted intensive research and experiments, and as a result, the beverage as a container content is a green tea, oolong tea or the like having a catechin content of 30 mg% or more in a low-acid beverage having a pH of 4.6 or more. If limited to tea beverages and acidic beverages with a pH of less than 4.6, it is not necessary to sterilize the container with chemicals, do not require rapid cooling to room temperature after heat sterilization of the beverage, and It has been found that the heat sterilization step after filling and sealing can be eliminated, and the present invention has been achieved.

すなわち、上記本発明の目的を達成する容器詰め飲料の製造方法の第1の構成は、pH4.6以上でカテキン含有量が30mg%以上の茶飲料を135℃、7.58秒の加熱殺菌と同等以上の殺菌値で加熱殺菌した後60℃〜70℃の温度に維持する一方、容器の少なくとも内面を65℃〜100℃の熱水で加熱殺菌し洗浄し、予め充填・密封装置およびその周辺環境を65℃〜100℃の熱水で加熱殺菌し洗浄した外界と隔離した環境管理空間の中で該飲料を充填温度60℃〜70℃で該殺菌済み容器に充填し、密封後40℃以下の常温まで冷却することを特徴とするものである。   That is, the first configuration of the method for producing a container-packed beverage that achieves the object of the present invention is to sterilize a tea beverage having a pH of 4.6 or more and a catechin content of 30 mg% or more at 135 ° C. for 7.58 seconds. After heat sterilization with the same or better sterilization value, the temperature is maintained at 60 ° C to 70 ° C, while at least the inner surface of the container is heat sterilized with hot water at 65 ° C to 100 ° C and washed beforehand. The beverage is filled into the sterilized container at a filling temperature of 60 ° C. to 70 ° C. in an environmental management space separated from the outside where the environment is sterilized by heating with hot water of 65 ° C. to 100 ° C. It is characterized by cooling to room temperature.

本発明の好ましい実施態様においては、該飲料を加熱殺菌後65℃〜67℃に維持し容器に充填する。   In a preferred embodiment of the invention, the beverage is maintained at 65-67 ° C. after heat sterilization and filled into a container.

また、本発明の好ましい他の実施態様においては、該環境管理空間はボックス内に収容された空間である。   In another preferred embodiment of the present invention, the environmental management space is a space accommodated in a box.

本発明によれば、容器を熱水で加熱殺菌・洗浄し、飲料を充填温度60℃〜70℃、好ましくは65℃〜67℃で容器に充填するので、アセプテイック充填法に対しては、薬剤や無菌水の使用を不要とするとともに飲料の加熱殺菌後常温まで急速冷却するための装置およびその制御を不要とすることにより設備を大幅に簡素化することができる。また、ホットパック法に対しては、飲料を従来のホットパック法よりも有意に低い充填温度で充填するので、容器の減圧変形耐性に関する条件を緩和することができ、それだけ容器の肉厚を薄くすることにより材料費の軽減を実現することができる。また、充填・密封後の加熱殺菌工程が不要であるので、ホットパック法に比べて設備を簡素化し作業環境を改善することができる。   According to the present invention, the container is sterilized and washed with hot water, and the beverage is filled into the container at a filling temperature of 60 ° C to 70 ° C, preferably 65 ° C to 67 ° C. The facility can be greatly simplified by eliminating the need to use a device for controlling the rapid cooling to room temperature after heat sterilization of beverages and the control thereof. In addition, for the hot pack method, since the beverage is filled at a significantly lower filling temperature than the conventional hot pack method, the conditions regarding the resistance to vacuum deformation of the container can be relaxed, and the thickness of the container is reduced accordingly. By doing so, the material cost can be reduced. Moreover, since the heat sterilization process after filling and sealing is unnecessary, the equipment can be simplified and the working environment can be improved as compared with the hot pack method.

以下添付図面を参照して、本発明の実施の形態について説明する。
本発明が適用される飲料は、pH4.6以上でカテキン含有量が30mg%以上の緑茶、ウーロン茶等の茶飲料、およびpH4.6未満の酸性飲料である。この酸性飲料には、天然果汁、果汁飲料、果肉飲料、果汁入り清涼飲料、果粒入り果実飲料、レモンテイー、スポーツドリンク等が含まれる。
Embodiments of the present invention will be described below with reference to the accompanying drawings.
Beverages to which the present invention is applied include tea beverages such as green tea and oolong tea having a catechin content of 30 mg% or more at pH 4.6 or more, and acidic beverages having a pH of less than 4.6. Examples of the acidic beverage include natural fruit juice, fruit juice beverage, fruit beverage, soft drink with fruit juice, fruit drink with fruit granules, lemon tea, sports drink and the like.

本発明の方法に使用する容器は、PETボトル等のポリエステルボトルの他ポリエステル製カップ、トレー等のポリエステル容器を含むプラスチック容器、ガラス瓶、金属ボトル、食缶等である。本発明は特にPETボトルの減圧耐性に関する条件を緩和し、その薄肉化が図れる点でPETボトル詰めの上記飲料の製造に好適である。   Containers used in the method of the present invention include polyester bottles such as PET bottles, polyester cups, plastic containers including polyester containers such as trays, glass bottles, metal bottles, food cans, and the like. Especially this invention is suitable for manufacture of the said drink of PET bottle filling at the point which eases the conditions regarding the decompression tolerance of PET bottle, and can achieve the thinning.

本発明の製造方法においては、内容物となる飲料を加熱殺菌した後60℃〜70℃、好ましくは65℃〜67℃の温度に維持する一方、容器の少なくとも内面を65℃〜100℃の熱水で加熱殺菌し洗浄し、予め充填・密封装置およびその周辺環境を65℃〜100℃未満の熱水で加熱殺菌し洗浄した外界と隔離した環境管理空間の中で該飲料を充填温度60℃〜70℃、好ましくは65℃〜67℃で殺菌済み容器に充填し、密封後40℃以下の常温まで冷却する。   In the production method of the present invention, the beverage to be the contents is sterilized by heating and maintained at a temperature of 60 ° C to 70 ° C, preferably 65 ° C to 67 ° C, while at least the inner surface of the container is heated to 65 ° C to 100 ° C. Water sterilized and washed with water. Filling and sealing device and its surrounding environment were pre-heated and sterilized with hot water at 65 ° C to less than 100 ° C. Fill the sterilized container at ˜70 ° C., preferably 65 ° C. to 67 ° C., and after sealing, cool to room temperature of 40 ° C. or lower.

内容物が茶飲料の場合は、茶飲料を熱交換機による公知の高温短時間殺菌法(HTST殺菌)等により135℃、7.58秒の加熱殺菌と同等以上の殺菌値で加熱殺菌した後ヘッドタンクユニット内で60℃〜70℃、好ましくは65℃〜67℃の温度に維持する。内容物が酸性飲料の場合は、酸性飲料を高温短時間殺菌法等により93℃〜95℃で加熱殺菌した後ヘッドタンクユニット内で60℃〜70℃、好ましくは65℃〜67℃の温度に維持する。   If the content is a tea beverage, the tea beverage is sterilized by heating at a sterilization value equivalent to or higher than that at 135 ° C for 7.58 seconds by a known high-temperature, short-time sterilization method (HTST sterilization) using a heat exchanger. It is maintained at a temperature of 60 ° C to 70 ° C, preferably 65 ° C to 67 ° C in the tank unit. When the content is an acidic beverage, the acidic beverage is sterilized by heating at 93 ° C. to 95 ° C. by a high temperature short time sterilization method or the like, and then the temperature in the head tank unit is 60 ° C. to 70 ° C., preferably 65 ° C. to 67 ° C. maintain.

以下代表的な例としてPETボトルにこれらの飲料を充填する場合について図1のフローチャートを参照して説明する。なお、本明細書において、「環境管理空間」とは、予め充填・密封装置およびその周辺環境を65℃〜100℃の熱水で加熱殺菌し洗浄した外界と隔離した空間を意味する。   Hereinafter, the case where these beverages are filled in a PET bottle will be described as a typical example with reference to the flowchart of FIG. In the present specification, the “environmental management space” means a space isolated from the outside where the filling / sealing device and the surrounding environment are preliminarily heat-sterilized and washed with hot water of 65 ° C. to 100 ° C.

本実施形態において、環境管理空間外のボトル供給装置から環境管理空間内のボトル殺菌・洗浄装置に移送されたボトルの殺菌は、少なくともボトルの内面、好ましくは内外面を65℃〜100℃の熱水で加熱殺菌することにより行う。殺菌時間は3秒ないし10秒である。この方法によれば、熱水によりボトルの殺菌と殺菌後の洗浄を同時に行うので、殺菌後のボトルを別途洗浄する工程は不要である。   In this embodiment, the sterilization of the bottle transferred from the bottle supply device outside the environment management space to the bottle sterilization / cleaning device inside the environment management space is performed at a temperature of 65 ° C. to 100 ° C. at least on the inner surface of the bottle, preferably the inner and outer surfaces. Perform by heat sterilization with water. The sterilization time is 3 to 10 seconds. According to this method, since the bottle is sterilized with hot water and cleaned after sterilization at the same time, a step of separately cleaning the sterilized bottle is unnecessary.

熱水によるボトル内外面の殺菌は、たとえば図2に示すように、ボトルを倒立状態に配置し、熱水スプレーノズルから熱水を噴射することにより行うことができる。   Sterilization of the inner and outer surfaces of the bottle with hot water can be performed, for example, by placing the bottle in an inverted state and injecting hot water from a hot water spray nozzle as shown in FIG.

ボトル内外面の殺菌を終了後ボトルは環境管理空間内に設けられたフイラーに移送され、ヘッドタンクユニット内に保持された飲料がボトル内に充填される。ヘッドタンクユニットにおいては、上記のとおり飲料が60℃〜70℃,好ましくは65℃〜67℃の温度で保持されているので、飲料はこの範囲内の選択された温度でボトルに充填される。70℃を超える充填温度は本発明の選択された種類の飲料にとっては不必要であり、エネルギーの浪費である上に、ボトルの減圧変形耐性についての条件も厳しくなるので不利である。また、充填温度が60℃未満では、充分な殺菌を達成することが困難である。   After the sterilization of the inner and outer surfaces of the bottle is completed, the bottle is transferred to a filler provided in the environmental management space, and the beverage held in the head tank unit is filled into the bottle. In the head tank unit, since the beverage is held at a temperature of 60 ° C. to 70 ° C., preferably 65 ° C. to 67 ° C. as described above, the beverage is filled into the bottle at a selected temperature within this range. Filling temperatures above 70 ° C. are not necessary for the selected type of beverage of the present invention, which is disadvantageous because it is a waste of energy and the requirements for bottle deformation resistance are also severe. Further, if the filling temperature is less than 60 ° C., it is difficult to achieve sufficient sterilization.

飲料が充填されたボトルはフイラーから環境管理空間内に設けられたキャッパーに移送され、環境管理空間外に配置されたキャップ供給装置から環境管理空間内に配置されたキャップ殺菌・洗浄装置に供給されたキャップ殺菌・洗浄装置においてボトルと同一条件で殺菌・洗浄されたキャップで完全に密封される。その後密封されたボトルは環境管理空間外に配置された簡易的な冷却水シャワー等の冷却装置により40℃以下の常温まで冷却され、検査・箱詰め工程を経て製品として出荷される。   The bottle filled with the beverage is transferred from the filler to a capper provided in the environmental management space, and supplied from a cap supply device arranged outside the environmental management space to a cap sterilization / washing device arranged in the environmental management space. The cap sterilization / cleaning device is completely sealed with a cap sterilized and cleaned under the same conditions as the bottle. Thereafter, the sealed bottle is cooled to a room temperature of 40 ° C. or less by a cooling device such as a simple cooling water shower arranged outside the environmental management space, and is shipped as a product through an inspection / boxing process.

ボトル内外面殺菌、飲料充填、キャッピング(密封)工程を行う装置の1具体例を図3の概略図に示す。   A specific example of an apparatus for performing bottle inner and outer surface sterilization, beverage filling, and capping (sealing) steps is shown in the schematic diagram of FIG.

図3において、飲料充填装置10は飲料をPETボトルに充填するための充填装置であって、PETボトルの搬送方向の順にボトルの内外面を殺菌するボトルリンサー11、フイラー12、キャッパー13、ボトルを2列に振り分けるための振り分け装置14が配列されている。飲料充填装置10は鋼板からなるカバー15によって覆われており、このカバー15によって環境管理空間を構成するボックス16が形成されている。   In FIG. 3, a beverage filling device 10 is a filling device for filling a PET bottle with a beverage, and a bottle rinser 11, a filler 12, a capper 13, and a bottle for sterilizing the inner and outer surfaces of the bottle in the order of the PET bottle conveyance direction. A sorting device 14 for sorting in two rows is arranged. The beverage filling device 10 is covered with a cover 15 made of a steel plate, and a box 16 constituting an environment management space is formed by the cover 15.

なお、カバー15にはボトル導入口15aとボトル排出口15bが形成されているが、ボックス16は実質的に密閉されている。   The cover 15 has a bottle inlet 15a and a bottle outlet 15b, but the box 16 is substantially sealed.

環境管理空間殺菌装置1は、ボックス16内において熱水を散布する手段を構成する複数の回転ノズル2および複数の固定ノズル3を備えている。回転ノズル2はスプレーボールからなり、噴射口を下方に向けてボックス16内の上部に配置されている。固定ノズル3はフルコーンノズルからなり、噴射口を斜め上方に向けてボックス16内の下部の床面付近に配置されている。回転ノズル2および固定ノズル3はそれぞれ配管4により弁7および加温ヒーター6を介して熱水供給源5に接続されており、該供給源5から熱水の供給を受けることができる。   The environment management space sterilization apparatus 1 includes a plurality of rotating nozzles 2 and a plurality of fixed nozzles 3 that constitute a means for spraying hot water in the box 16. The rotary nozzle 2 is formed of a spray ball, and is arranged in the upper portion of the box 16 with the spray port facing downward. The fixed nozzle 3 is composed of a full cone nozzle, and is disposed near the floor surface in the lower part of the box 16 with the injection port directed obliquely upward. The rotary nozzle 2 and the fixed nozzle 3 are connected to a hot water supply source 5 through a valve 4 and a heating heater 6 via a pipe 4, respectively, and can be supplied with hot water from the supply source 5.

この装置を使用して殺菌を行う場合は、弁7を操作して配管4を熱水供給源5に接続する。熱水供給源5からの水は加温ヒーター6により加温され、配管4を経由してボックス16内の回転ノズル2および固定ノズル3に供給され、これらのノズル2、3からボックス内に散布される。散布された熱水はボックス16内のボトルリンサー11、フイラー12、キャッパー13、振り分け装置14等の機器の外表面、ボックス16の内壁面およびボトルリンサー11に熱水を供給するライン配管(図示せず)等の殺菌対象表面の大部分に降りかかってこの部分を濡らす。散布された熱水は殺菌対象表面の大部分を濡らすことによってこの部分を殺菌するとともに、蒸発した水蒸気がボックス16内に充満し、熱水によって濡れていない部分を含む全殺菌対象表面に接触することによってさらなる殺菌が行われる。この熱水の散布を所定時間継続することによって全殺菌対象表面の完全な殺菌が達成される。この場合環境管理空間の内壁面であるボックス16の内壁面も全面が機器表面と同様に充分に殺菌される。   When sterilization is performed using this apparatus, the valve 4 is operated to connect the pipe 4 to the hot water supply source 5. Water from the hot water supply source 5 is heated by a heating heater 6, supplied to the rotating nozzle 2 and the fixed nozzle 3 in the box 16 via the pipe 4, and dispersed in the box from these nozzles 2 and 3. Is done. The sprayed hot water is line piping (not shown) for supplying hot water to the outer surface of the equipment such as the bottle rinser 11, the filler 12, the capper 13, and the sorting device 14 in the box 16, the inner wall surface of the box 16 and the bottle rinser 11. Wet this part of the surface to be sterilized and wet it. The sprayed hot water sterilizes this part by wetting most of the surface to be sterilized, and the evaporated water vapor fills the box 16 and comes into contact with the entire surface to be sterilized including the part not wetted by the hot water. This further sterilizes. By continuing the spraying of the hot water for a predetermined time, complete sterilization of the entire surface to be sterilized is achieved. In this case, the entire inner wall surface of the box 16 which is the inner wall surface of the environmental management space is sufficiently sterilized in the same manner as the device surface.

殺菌温度は殺菌対象表面が65℃以上とし、100℃以下、好ましくは大気圧下で行うために96℃未満となるように熱水の加温を調節する。   The sterilization temperature is adjusted so that the surface to be sterilized is 65 ° C. or higher and 100 ° C. or lower, preferably less than 96 ° C. in order to carry out under atmospheric pressure.

以下本発明の実施例について説明する。   Examples of the present invention will be described below.

実施例1
500mlPETボトルを用いて、緑茶飲料(pH5.9、カテキン含有量52mg%)を上記の製造方法および装置を用いて製造した。すなわち、90℃、3秒の熱水で殺菌・洗浄したボトルに、135℃、30秒のHTST殺菌後65℃まで冷却した緑茶飲料を、予めボックスにより外界と遮断した環境管理空間内に設置され、容器と同一条件で殺菌・洗浄したフイラー、キャッパーにより充填、密封した。その後、簡易的な冷却水シャワーでPETボトル詰め緑茶飲料を常温まで冷却し、30℃、2週間の保管後内容物の微生物変敗状態を目視により観察した。その結果、緑茶飲料の状態は良好で、微生物変敗による濁りはまったく観察されなかった。
Example 1
Using a 500 ml PET bottle, a green tea beverage (pH 5.9, catechin content 52 mg%) was produced using the production method and apparatus described above. That is, a green tea beverage cooled to 65 ° C. after HTST sterilization at 135 ° C. for 30 seconds is placed in an environmental management space where the box is preliminarily blocked from the outside by a box. Filled and sealed with a filler and capper sterilized and washed under the same conditions as the container. Then, the PET bottle-packed green tea beverage was cooled to room temperature with a simple cooling water shower, and the microbial degradation state of the contents was visually observed after storage at 30 ° C. for 2 weeks. As a result, the state of the green tea beverage was good and no turbidity due to microbial degradation was observed.

比較例1
飲料としてカテキン含有量12mg%の混合茶を用いた以外は実施例1と同一条件でPETボトル詰め飲料を製造した。30℃、2週間保管後の飲料は濁りが発生しており、微生物による変敗が生じていることを示した。
Comparative Example 1
A PET bottled beverage was produced under the same conditions as in Example 1 except that mixed tea having a catechin content of 12 mg% was used as the beverage. The beverage after storage at 30 ° C. for 2 weeks had turbidity, indicating that deterioration due to microorganisms had occurred.

比較例2
飲料として麦茶(カテキン含有量検出不能)を用いた以外は実施例1と同一条件でPETボトル詰め飲料を製造した。30℃、2週間保管後の飲料は濁りが発生しており、微生物による変敗が生じていることを示した。
Comparative Example 2
A PET bottled beverage was produced under the same conditions as in Example 1 except that barley tea (catechin content was not detectable) was used as the beverage. The beverage after storage at 30 ° C. for 2 weeks had turbidity, indicating that deterioration due to microorganisms had occurred.

比較例3
ボトルは熱水による殺菌は行わず、水による洗浄のみとし、充填設備等はボックスで遮断せず、設備も熱水による殺菌を行わず、水による洗浄のみとした以外は実施例1と同一条件で飲料を製造した。30℃、2週間保管後の飲料は濁りが発生しており、微生物による変敗が生じていることを示した。
Comparative Example 3
The bottles are not sterilized with hot water, only washed with water, the filling equipment is not blocked with a box, the equipment is not sterilized with hot water, and only washed with water. Made a beverage. The beverage after storage at 30 ° C. for 2 weeks had turbidity, indicating that deterioration due to microorganisms had occurred.

以上の実験の結果比較例はいずれも製品の微生物による変敗を示しており、実施例の製造方法が優れていることが明らかとなった。   As a result of the above experiments, all of the comparative examples showed deterioration of the product due to microorganisms, and it was revealed that the production methods of the examples were excellent.

本発明にかかる方法の1実施形態を示すフローチャートである。2 is a flowchart illustrating an embodiment of a method according to the present invention. 熱水によるボトルの殺菌方法の1例を示す説明図である。It is explanatory drawing which shows one example of the sterilization method of the bottle by hot water. 環境管理空間殺菌装置の1例を示す概略図である。It is the schematic which shows an example of an environmental management space sterilizer.

Claims (3)

pH4.6以上の低酸性飲料中カテキン含有量が52mg%以上の茶飲料を135℃、7.58秒以上の加熱殺菌条件で加熱殺菌した後60℃〜70℃の温度に維持する一方、容器の少なくとも内面を65℃〜100℃の熱水で加熱殺菌し洗浄し、予め充填・密封装置およびその周辺環境を65℃〜100℃の熱水で加熱殺菌し洗浄した外界と隔離した環境管理空間の中で該飲料を充填温度60℃〜70℃で該殺菌済み容器に充填し、密封後40℃以下の常温まで冷却することを特徴とする容器詰め飲料の製造方法。 While maintaining a temperature of 60 ° C. to 70 ° C. after sterilizing a tea beverage having a catechin content of 52 mg% or more in a low acid beverage of pH 4.6 or more under heat sterilization conditions of 135 ° C. and 7.58 seconds or more , At least the inner surface of the container is heat sterilized and cleaned with hot water of 65 ° C to 100 ° C, and the environmental management is isolated from the outside where the filling and sealing device and its surrounding environment are preheated and cleaned with hot water of 65 ° C to 100 ° C. A method for producing a container-packed beverage, wherein the beverage is filled in the sterilized container at a filling temperature of 60 ° C to 70 ° C in a space, and cooled to a room temperature of 40 ° C or less after sealing. 該飲料を加熱殺菌後65℃〜67℃に維持し容器に充填することを特徴とする請求項1記載の容器詰め飲料の製造方法。 The method for producing a container-packed beverage according to claim 1, wherein the beverage is maintained at 65 ° C to 67 ° C after heat sterilization and filled into a container. 該環境管理空間はボックス内に収容された空間であることを特徴とする請求項1または2に記載の容器詰め飲料の製造方法。 The method for producing a container-packed beverage according to claim 1 or 2, wherein the environmental management space is a space accommodated in a box.
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JP5271490B2 (en) * 2006-10-12 2013-08-21 アサヒ飲料株式会社 Method for producing resin-contained beverage and resin-contained beverage
JP5056000B2 (en) * 2006-12-22 2012-10-24 大日本印刷株式会社 Fluid filling method and apparatus
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WO2015189894A1 (en) * 2014-06-09 2015-12-17 東洋製罐グループホールディングス株式会社 Method and system for aseptic filling of beverage
JP6466158B2 (en) * 2014-12-17 2019-02-06 アサヒ飲料株式会社 Method for producing container-packed coffee beverage and method for suppressing flavor deterioration of container-packed coffee beverage
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