JP4253236B2 - Production method of tea extract - Google Patents

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JP4253236B2
JP4253236B2 JP2003315287A JP2003315287A JP4253236B2 JP 4253236 B2 JP4253236 B2 JP 4253236B2 JP 2003315287 A JP2003315287 A JP 2003315287A JP 2003315287 A JP2003315287 A JP 2003315287A JP 4253236 B2 JP4253236 B2 JP 4253236B2
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tea
extraction solvent
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green tea
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紀子 古市
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Kao Corp
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Description

本発明は、茶葉由来の自然な香気と味が良好な茶抽出物の製造法及びそれを用いた茶系飲料に関する。   The present invention relates to a method for producing a tea extract having a natural aroma and a good taste derived from tea leaves, and a tea-based beverage using the same.

緑茶、烏龍茶、紅茶等の茶系飲料は、通常それぞれ対応する茶葉から温水で抽出した抽出物を配合して製造され、苦み、滋味等を調整する目的で種々の抽出条件が検討されている。エタノールを用いた茶の抽出技術については、広範囲の動植物から水溶性エキスを抽出する目的で50重量%以上のエタノール水溶液を用いる方法(特許文献1)が知られている。また、茶系抽出液にエタノールを添加して、品質の保持された茶系アルコール飲料用の濃縮液を得る技術(特許文献2)及び甜茶の風味改善を目的として甜茶抽出物にエタノールを配合する技術(特許文献3)が知られている。
特許第3342235号公報 特開2002−209519号公報 特開2000−41639号公報
Tea-based beverages such as green tea, oolong tea, and black tea are usually produced by blending extracts extracted from the corresponding tea leaves with warm water, and various extraction conditions have been studied for the purpose of adjusting bitterness, taste, and the like. As for tea extraction technology using ethanol, a method (Patent Document 1) using an aqueous ethanol solution of 50% by weight or more for the purpose of extracting a water-soluble extract from a wide range of animals and plants is known. Also, ethanol is added to tea extract for the purpose of adding a tea-based extract to obtain a concentrated liquid for tea-based alcoholic beverages that maintains quality (Patent Document 2) and improving the flavor of tea tea. A technique (Patent Document 3) is known.
Japanese Patent No. 3342235 JP 2002-209519 A JP 2000-41639 A

お茶のフレーバー感は、ボディ感、フレッシュ感、焙焼香、発酵感等からなり、これらのバランスによりお茶らしい風味が得られる。ところが、温水抽出では焙焼香や発酵感は得られるが、フレッシュ感が得られにくく、一方前記特許文献1のような高濃度エタノール水溶液抽出ではフレッシュ感は得られるが、焙焼香や発酵感が得られにくく、いずれの場合もボディ感、フレッシュ感、焙焼香、発酵感等をバランス良く有するお茶独特のフレーバー感の良好な茶抽出物は得られなかった。また、前記特許文献2及び3はエタノールを添加する技術であり、茶系飲料に適用できるものではない。
従って、本発明の目的は、バランスの良い香気と風味を有し、茶系飲料に配合できる茶抽出物の製造法を提供することにある。
The flavor of tea consists of a body feeling, a fresh feeling, a roasted incense, a fermented feeling, and the like, and a tea-like flavor can be obtained by balancing these. However, the hot water extraction provides a roasted aroma and a feeling of fermentation, but it is difficult to obtain a fresh feeling. On the other hand, a high-concentration aqueous ethanol extraction as in Patent Document 1 provides a fresh feeling, but a roasted aroma and a feeling of fermentation are obtained. In any case, a tea extract with a good flavor feeling peculiar to tea having a well-balanced body feeling, fresh feeling, roasted incense, fermentation feeling and the like could not be obtained. Moreover, the said patent documents 2 and 3 are the techniques which add ethanol, and are not applicable to a tea-type drink.
Accordingly, an object of the present invention is to provide a method for producing a tea extract that has a well-balanced aroma and flavor and can be blended into a tea-based beverage.

そこで本発明者は、お茶らしい香気と風味を基準として茶葉からの抽出手段について検討したところ、エタノール水溶液の濃度だけでなく、抽出溶媒量及び抽出温度を特定の範囲とすることにより、お茶らしい香気を有し、青臭さがなく、かつ風味の強い茶抽出物が得られ、これを用いれば天然感に富んだ香気を持ったボディ感のある茶系飲料が製造可能になることを見出した。
すなわち、本発明は、カメリア シネンシスに属する茶葉から茶抽出物を製造する方法であって、抽出溶媒として0.5〜5重量%のエタノール水溶液を用い、該抽出溶媒に対して茶葉を0.5〜20重量%用い、抽出温度0〜77℃で抽出する茶抽出物の製造法を提供するものである。
また本発明は、前記方法により得られた茶抽出物を配合してなる茶系飲料を提供するものである。
Therefore, the present inventor examined the extraction means from tea leaves on the basis of tea-like aroma and flavor. Not only the concentration of the ethanol aqueous solution but also the amount of extraction solvent and the extraction temperature within a specific range, the smell like tea It has been found that a tea extract having a fragrance, a blue odor, and a strong flavor can be obtained, and by using this, a tea-based beverage having a body feeling with a rich natural flavor can be produced.
That is, the present invention is a method for producing a tea extract from tea leaves belonging to Camellia sinensis, wherein 0.5 to 5% by weight ethanol aqueous solution is used as an extraction solvent, and 0.5% of tea leaves are added to the extraction solvent. The present invention provides a method for producing a tea extract which is extracted at an extraction temperature of 0 to 77 ° C. using ˜20% by weight.
Moreover, this invention provides the tea-type drink formed by mix | blending the tea extract obtained by the said method.

本発明によれば茶葉由来の自然な香気を有し、青臭さなどがなく、風味の良好な茶抽出物が効率良く抽出され、これを用いれば天然感に富んだ香気を持ちボディ感のある茶系飲料が製造できる。   According to the present invention, a tea extract having a natural aroma derived from tea leaves, having no blue odor, and a good flavor is efficiently extracted, and if used, it has a natural aroma and a body feeling. Tea-based beverages can be manufactured.

本発明に用いられる茶葉としては、カメリア シネンシス(Camellia sinensis)に属する茶葉から製茶された、煎茶、玉露、てん茶などの緑茶類、総称して烏龍茶と呼ばれる鉄観音、色種、黄金桂、武夷岩茶等の半発酵茶、総称して紅茶と呼ばれるアッサム、キーモン、ダージリン、セイロン等の発酵茶等が挙げられる。   As tea leaves used in the present invention, green teas such as Sencha, Gyokuro, Tencha, etc., made from tea leaves belonging to Camellia sinensis, iron kannon, color species, golden katsura, martial arts, which are collectively called Oolong tea Semi-fermented teas such as Iwacha, fermented teas such as Assam, Kemon, Darjeeling, and Ceylon, which are collectively called black tea, and the like.

抽出溶媒としては、エタノール水溶液を使用し、そのエタノール濃度は0.5〜5重量%、好ましくは1.5〜5重量%、より好ましくは2〜4重量%である。エタノール濃度が0.5重量%未満では、得られる茶抽出物の香気が十分でなく、5重量%を超えると青臭く、生臭い、茶らしくない香気が抽出される。   As the extraction solvent, an aqueous ethanol solution is used, and the ethanol concentration is 0.5 to 5% by weight, preferably 1.5 to 5% by weight, and more preferably 2 to 4% by weight. When the ethanol concentration is less than 0.5% by weight, the aroma of the obtained tea extract is not sufficient, and when it exceeds 5% by weight, an aroma that is bluish, fresh, or not tea-like is extracted.

茶葉の量は、抽出溶媒に対して、0.5〜20重量%、好ましくは1〜10重量%、より好ましくは1.5〜6重量%である。茶葉量が0.5重量%未満では、得られる茶抽出物の香気が十分でなく、20重量%を超えると茶の呈味成分が十分に抽出されず、香気とのバランスが良くない。   The amount of tea leaves is 0.5 to 20% by weight, preferably 1 to 10% by weight, more preferably 1.5 to 6% by weight, based on the extraction solvent. When the amount of tea leaves is less than 0.5% by weight, the aroma of the obtained tea extract is not sufficient, and when it exceeds 20% by weight, the taste components of tea are not sufficiently extracted and the balance with the aroma is not good.

抽出温度は0〜77℃、好ましくは0〜75℃、より好ましくは5〜70℃である。抽出温度が0℃未満では得られる茶抽出物の香気が十分でなく、77℃を超えるとエタノールの添加効果が減少する。   The extraction temperature is 0 to 77 ° C, preferably 0 to 75 ° C, more preferably 5 to 70 ° C. If the extraction temperature is less than 0 ° C, the aroma of the obtained tea extract is not sufficient, and if it exceeds 77 ° C, the effect of adding ethanol decreases.

茶を抽出する方法は、撹拌抽出など従来の方法により行うことができる。また、抽出時、抽出溶媒にあらかじめアスコルビン酸ナトリウムなどの有機酸又は有機酸塩類を添加してもよい。また、煮沸脱気や窒素ガス等の不活性ガスを通気して溶存酸素を除去しつついわる非酸化的雰囲気下で抽出する方法も併用して良い。   The method for extracting tea can be performed by a conventional method such as stirring extraction. Moreover, you may add organic acids or organic acid salts, such as sodium ascorbate, to an extraction solvent previously at the time of extraction. Moreover, you may use together the method extracted in non-oxidative atmosphere which ventilates inert gas, such as boiling deaeration and nitrogen gas, and removes dissolved oxygen.

得られた抽出液は、減圧濃縮(薄膜濃縮、フラッシュ濃縮)、RO膜濃縮等の濃縮、遠心分離、濾過等の処理を行うことができる。   The obtained extract can be subjected to treatment such as concentration under reduced pressure (thin film concentration, flash concentration), RO membrane concentration, centrifugation, filtration, and the like.

茶系飲料を得る場合には、得られた抽出液を3〜70%に希釈し、必要に応じて茶由来の成分に合わせて、酸化防止剤、香料、各種エステル類、有機酸類、有機酸塩類、無機酸類、無機酸塩類、無機塩類、色素類、乳化剤、保存料、調味料、甘味料、酸味料、果汁エキス類、野菜エキス類、花蜜エキス類、pH調整剤、品質安定剤などの添加剤を単独、あるいは併用して添加しても良い。   In the case of obtaining a tea-based beverage, the obtained extract is diluted to 3 to 70%, and if necessary, in accordance with the components derived from tea, antioxidants, fragrances, various esters, organic acids, organic acids Salts, inorganic acids, inorganic acid salts, inorganic salts, pigments, emulsifiers, preservatives, seasonings, sweeteners, acidulants, fruit juice extracts, vegetable extracts, nectar extracts, pH adjusters, quality stabilizers, etc. Additives may be added alone or in combination.

例えば甘味料としては、砂糖、ぶどう糖、果糖、異性化液糖、グリチルリチン、ステビア、アスパルテーム、フラクトオリゴ糖、ガラクトオリゴ糖、その他のオリゴ糖としてシクロデキストリン及び、分岐α−、β−、γ−シクロデキストリンが使用できる。またスクラロース、アセスルファムカリウム等の人工甘味料も使用できる。   For example, sweeteners include sugar, glucose, fructose, isomerized liquid sugar, glycyrrhizin, stevia, aspartame, fructooligosaccharide, galactooligosaccharide, and other oligosaccharides such as cyclodextrin and branched α-, β-, and γ-cyclodextrin. Can be used. Artificial sweeteners such as sucralose and acesulfame potassium can also be used.

酸味料としては、天然成分から抽出した果汁類のほか、クエン酸、酒石酸、リンゴ酸、乳酸、フマル酸、リン酸が挙げられる。
無機酸類、無機酸塩類としてはリン酸、リン酸2ナトリウム、メタリン酸ナトリウム、ポリリン酸ナトリウムなどが、有機酸類、有機酸塩類としては、クエン酸、コハク酸、イタコン酸、リンゴ酸、クエン酸ナトリウムなどが挙げられる。
Examples of acidulants include fruit juices extracted from natural ingredients, citric acid, tartaric acid, malic acid, lactic acid, fumaric acid, and phosphoric acid.
Inorganic acids and inorganic acid salts include phosphoric acid, disodium phosphate, sodium metaphosphate, and sodium polyphosphate. Organic acids and organic acid salts include citric acid, succinic acid, itaconic acid, malic acid, and sodium citrate. Etc.

茶系飲料は容器詰飲料とするのが好ましく、当該容器詰茶系飲料の容器詰に使用される容器は、一般の飲料と同様にポリエチレンテレフタレートを主成分とする成形容器(いわゆるPETボトル)、金属缶、金属箔やプラスチックフィルムと複合された紙容器、瓶などの通常の形態で提供することができる。ここでいう容器詰飲料とは希釈せずに飲用できるものをいう。   The tea-based beverage is preferably a container-packed beverage, and the container used for container-packing the container-packed tea-based beverage is a molded container (so-called PET bottle) containing polyethylene terephthalate as a main component in the same manner as a general beverage, It can be provided in a normal form such as a metal can, a metal container or a paper container combined with a plastic film, or a bottle. The term “packaged beverage” as used herein means a beverage that can be drunk without dilution.

また本発明の容器詰茶系飲料は、例えば、金属缶のように容器に充填後、加熱殺菌できる場合にあっては食品衛生法に定められた殺菌条件で製造される。PETボトル、紙容器のようにレトルト殺菌できないものについては、あらかじめ上記と同等の殺菌条件、例えばプレート式熱交換器などで高温短時間殺菌後、一定の温度まで冷却して容器に充填する等の方法が採用される。また、無菌下で、充填された容器に別の成分を配合して充填してもよい。さらに、酸性化で加熱殺菌後、無菌化でpHを中性に戻すことや、中性化で加熱殺菌後、無菌下でpHを酸性に戻すなどの操作も可能である。   Moreover, the container-packed tea-based beverage of the present invention is produced under the sterilization conditions defined in the Food Sanitation Law if it can be heat sterilized after filling into a container like a metal can. For PET bottles and paper containers that cannot be sterilized by retort, sterilize under the same conditions as above, for example, sterilize at high temperature and short time with a plate heat exchanger, etc. The method is adopted. Moreover, you may mix | blend another component with the filled container under aseptic conditions. Further, after sterilization by heating after acidification, the pH can be returned to neutrality by sterilization, or after sterilization by heating after neutralization, the pH can be returned to acidity under aseptic conditions.

(1)香気の評価
調製したサンプルは、専門パネルであるフレーバリスト5名による官能評価法によって評価した。評価にあたって以下の基準によって評点をつけた。
(1) Evaluation of aroma The prepared sample was evaluated by a sensory evaluation method by five flavorists who are specialized panels. The evaluation was scored according to the following criteria.

(緑茶らしい香り)
−:香気が感じられない
△:香気がやや弱い
〇:香気がやや強い
◎:香気が強い
(Scent like green tea)
-: Aroma is not felt △: Aroma is slightly weak 〇: Aroma is slightly strong ◎: Aroma is strong

(生臭い又は青臭い香り)
−:香気が感じられない
△:香気がやや弱い
×:香気がやや強い
××:香気が強い
(Raw smell or blue smell)
-: The fragrance is not felt △: The fragrance is slightly weak ×: The fragrance is slightly strong XX: The fragrance is strong

(総合評価)
×:茶風味が非常に悪い
△:茶風味のバランスが悪い
〇:茶風味のバランスが良い
◎:茶風味のバランスが非常に良い
(Comprehensive evaluation)
×: The tea flavor is very bad △: The tea flavor balance is bad 〇: The tea flavor balance is good ◎: The tea flavor balance is very good

実施例1
緑茶200gを70℃、10Lの抽出溶媒にて5分間抽出し、軽く圧搾して搾汁を得た。抽出溶媒として2重量%のエタノール水を用い、本発明品1を得た。
Example 1
200 g of green tea was extracted with an extraction solvent at 70 ° C. and 10 L for 5 minutes, and lightly squeezed to obtain juice. The product 1 of the present invention was obtained using 2% by weight ethanol water as an extraction solvent.

実施例2
紅茶1kgを65℃、20Lの抽出溶媒にて10分間抽出し、軽く圧搾して搾汁を得た。抽出溶媒として5重量%のエタノール水を用い、本発明品2を得た。
Example 2
1 kg of black tea was extracted with a 20 L extraction solvent at 65 ° C. for 10 minutes, and lightly pressed to obtain a juice. The product 2 of the present invention was obtained using 5% by weight ethanol water as an extraction solvent.

実施例3
烏龍茶3gを70℃、200mLの抽出溶媒にて3分間抽出し、軽く圧搾して搾汁を得た。抽出溶媒として4重量%のエタノール水を用い、本発明品3を得た。
Example 3
3 g of oolong tea was extracted with 70 mL of 200 mL of extraction solvent for 3 minutes and squeezed lightly to obtain a juice. The product 3 of the present invention was obtained using 4% by weight ethanol water as an extraction solvent.

比較例1
緑茶200gを70℃、10Lの抽出溶媒にて5分間抽出し、軽く圧搾して搾汁を得た。抽出溶媒として0.2重量%のエタノール水を用い、比較品1を得た。
Comparative Example 1
200 g of green tea was extracted at 70 ° C. with 10 L of extraction solvent for 5 minutes and lightly squeezed to obtain juice. Comparative product 1 was obtained using 0.2 wt% ethanol water as the extraction solvent.

比較例2
緑茶200gを70℃、10Lの抽出溶媒にて5分間抽出し、軽く圧搾して搾汁を得た。抽出溶媒として10重量%のエタノール水を用い、比較品2を得た。
Comparative Example 2
200 g of green tea was extracted at 70 ° C. with 10 L of extraction solvent for 5 minutes and lightly squeezed to obtain juice. Comparative product 2 was obtained using 10 wt% ethanol water as the extraction solvent.

比較例3
緑茶20gを70℃、10Lの抽出溶媒にて5分間抽出し、軽く圧搾して搾汁を得た。抽出溶媒として2重量%のエタノール水を用い、比較品3を得た。
Comparative Example 3
20 g of green tea was extracted with an extraction solvent at 70 ° C. and 10 L for 5 minutes, and lightly pressed to obtain juice. Comparative product 3 was obtained using 2 wt% ethanol water as the extraction solvent.

比較例4
緑茶200gを90℃、10Lの抽出溶媒にて5分間抽出し、軽く圧搾して搾汁を得た。抽出溶媒として2重量%のエタノール水を用い、比較品4を得た。
Comparative Example 4
200 g of green tea was extracted at 90 ° C. with 10 L of extraction solvent for 5 minutes and lightly squeezed to obtain juice. Comparative product 4 was obtained using 2% by weight ethanol water as the extraction solvent.

上記実施例及び比較例で得られた茶抽出物についての味の評価結果を表1に示す。   Table 1 shows the taste evaluation results for the tea extracts obtained in the above Examples and Comparative Examples.

Figure 0004253236
Figure 0004253236

また、本発明品1〜3の抽出物は、そのまま容器詰後、殺菌処理することにより容器詰茶系飲料とすることができた。   Moreover, the extract of this invention products 1-3 was able to be made into a container-packed tea type | system | group drink by sterilizing after container-packing as it is.

Claims (4)

カメリア シネンシスに属する茶葉から茶抽出物を製造する方法であって、抽出溶媒として0.5〜5重量%のエタノール水溶液を用い、該抽出溶媒に対して茶葉を1.5重量%用い、抽出温度〜77℃で抽出する茶抽出物の製造法。 From green tea leaves belonging to Camellia sinensis A method of manufacturing a green tea extract, with 0.5 to 5 wt% aqueous ethanol solution as an extraction solvent, 1.5 to 6 weight green tea leaves against the extraction solvent % used method for producing a green tea extract is extracted with extraction temperature 5 to 77 ° C.. 請求項1記載の方法により得られた茶抽出物を配合してなる茶系飲料。 Tea beverage made by blending the green tea extract obtained by the process of claim 1. 請求項1記載の方法により得られた茶抽出物を3〜70重量%配合したものである請求項2記載の茶系飲料。 Claim 1 obtained by the method described green tea extracts of 3 to 70% by weight compounded those according to claim 2, wherein the tea-based beverage. 容器詰茶系飲料である請求項2又は3記載の茶系飲料。   The tea-based beverage according to claim 2 or 3, which is a packaged tea-based beverage.
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JP5174646B2 (en) * 2007-12-18 2013-04-03 花王株式会社 Method for deodorizing organic solvents
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CN110810581B (en) * 2018-08-09 2023-10-13 湖南中烟工业有限责任公司 Preparation process of tea extract

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