JP4160067B2 - 水分散性改良プロポリス抽出物、含プロポリス飲料、及び、プロポリス抽出物の水分散性改良方法 - Google Patents
水分散性改良プロポリス抽出物、含プロポリス飲料、及び、プロポリス抽出物の水分散性改良方法 Download PDFInfo
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- JP4160067B2 JP4160067B2 JP2005257081A JP2005257081A JP4160067B2 JP 4160067 B2 JP4160067 B2 JP 4160067B2 JP 2005257081 A JP2005257081 A JP 2005257081A JP 2005257081 A JP2005257081 A JP 2005257081A JP 4160067 B2 JP4160067 B2 JP 4160067B2
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- propolis
- propolis extract
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 79
- 238000000034 method Methods 0.000 title claims description 17
- 235000013361 beverage Nutrition 0.000 title claims description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 68
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 40
- 238000000605 extraction Methods 0.000 claims description 30
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 28
- 239000011259 mixed solution Substances 0.000 claims description 23
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 20
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 18
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 14
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 13
- 238000005187 foaming Methods 0.000 claims description 9
- NGSWKAQJJWESNS-UHFFFAOYSA-N 4-coumaric acid Chemical compound OC(=O)C=CC1=CC=C(O)C=C1 NGSWKAQJJWESNS-UHFFFAOYSA-N 0.000 description 25
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 18
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- NGSWKAQJJWESNS-ZZXKWVIFSA-M 4-Hydroxycinnamate Natural products OC1=CC=C(\C=C\C([O-])=O)C=C1 NGSWKAQJJWESNS-ZZXKWVIFSA-M 0.000 description 12
- DFYRUELUNQRZTB-UHFFFAOYSA-N Acetovanillone Natural products COC1=CC(C(C)=O)=CC=C1O DFYRUELUNQRZTB-UHFFFAOYSA-N 0.000 description 12
- 239000000243 solution Substances 0.000 description 12
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- 230000000694 effects Effects 0.000 description 11
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 11
- 230000035622 drinking Effects 0.000 description 10
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 9
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
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- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 4
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- UBSCDKPKWHYZNX-UHFFFAOYSA-N Demethoxycapillarisin Natural products C1=CC(O)=CC=C1OC1=CC(=O)C2=C(O)C=C(O)C=C2O1 UBSCDKPKWHYZNX-UHFFFAOYSA-N 0.000 description 2
- ONIBWKKTOPOVIA-BYPYZUCNSA-N L-Proline Chemical compound OC(=O)[C@@H]1CCCN1 ONIBWKKTOPOVIA-BYPYZUCNSA-N 0.000 description 2
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- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 description 2
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- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 206010028813 Nausea Diseases 0.000 description 1
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- 235000006468 Thea sinensis Nutrition 0.000 description 1
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- 235000020279 black tea Nutrition 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
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- 235000015872 dietary supplement Nutrition 0.000 description 1
- 229930004069 diterpene Natural products 0.000 description 1
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- 238000004945 emulsification Methods 0.000 description 1
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- 230000003631 expected effect Effects 0.000 description 1
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- 230000037406 food intake Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
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- 239000000052 vinegar Substances 0.000 description 1
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Images
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- Non-Alcoholic Beverages (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Jellies, Jams, And Syrups (AREA)
Description
<プロポリス抽出液の調整>
プロポリス抽出液としては、アレクリン(バッカーリス ドラクンクリ フォーリア)由来のプロポリスに対して80体積%エタノール−水混合溶媒を用いて抽出して得た、不揮発成分32重量%を含むプロポリス抽出液を用いた。
ここで、炭酸水素ナトリウムを2質量%添加し、60℃で加熱処理を行った水分散性改良プロポリス抽出物(A)について、水分散性改良処理の処理前後の、その成分の変化の有無の検討を高速液体クロマトグラフィーにより行った。
予め質量を測定した透明なプラスチック製コップ12個にそれぞれ水道水を100mL入れ、これらのうち6個に水分散性改良処理前のプロポリス抽出液(プロポリス成分含有量32質量%:0.48)を、他の6個に上記水分散性改良プロポリス抽出物A(プロポリス成分含有量32質量%:0.48g(添加した炭酸水素ナトリウムは全量反応したとし、かつ、添加した炭酸水素ナトリウム由来のナトリウム成分質量は微量であるとして無視した))をそれぞれ1.5g(約60滴分であり、健康維持に充分であるとされている1日量に相当する)ずつ滴下した。
これに対して、本発明に係る水分散性改良プロポリス抽出物Aの場合にはコップの付着残留物質量の平均は0.002gと、付着残留物が事実上ない状態であることが確認された。なお、このときのわずかな付着残留物は流水で手洗浄することにより、容易に除去可能であることが確認された。
プロポリス抽出液としては、アレクリン由来のプロポリスに対して80体積%のエタノール水溶液で、常法に従って浸漬抽出して得られた、不揮発分285.9g(サンプリングした少量のサンプルを蒸発乾固させたときの残留分からの換算値。以下同)を含むプロポリス抽出液(「抽出原液」)1444g(エタノール濃度63体積%)を得た。
Claims (5)
- エタノール−水混合溶液を抽出溶媒とする抽出によって得られたプロポリス抽出液を、炭酸ナトリウム、及び/または、炭酸水素ナトリウム存在下で、40℃以上70℃以下の温度で加熱処理することを特徴とするプロポリス抽出物の水分散性改良方法。
- 上記エタノール−水混合溶液を抽出溶媒とする抽出によって得られたプロポリス抽出液が、エタノール濃度が60容積%以上であるエタノール−水混合溶液を用いて得られたプロポリス抽出液であることを特徴とする請求項1に記載のプロポリス抽出物の水分散性改良方法。
- エタノール濃度が60体積%以上であるエタノール−水混合溶液を抽出溶媒とする抽出によって得られたプロポリス抽出液であって、前記抽出後に炭酸ナトリウム、及び/または、炭酸水素ナトリウム存在下で、40℃以上70℃以下の温度で加熱処理されたことを特徴とする水分散性改良プロポリス抽出物。
- 上記加熱処理が、発泡が終了するまで行われたことを特徴とする請求項3に記載の水分散性改良プロポリス抽出物。
- 請求項3または請求項4に記載の水分散性改良プロポリス抽出物を含有することを特徴とする含プロポリス飲料。
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JP2005257081A JP4160067B2 (ja) | 2004-12-06 | 2005-09-05 | 水分散性改良プロポリス抽出物、含プロポリス飲料、及び、プロポリス抽出物の水分散性改良方法 |
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JP2005257081A JP4160067B2 (ja) | 2004-12-06 | 2005-09-05 | 水分散性改良プロポリス抽出物、含プロポリス飲料、及び、プロポリス抽出物の水分散性改良方法 |
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