JP4067074B2 - Skin cosmetics - Google Patents
Skin cosmetics Download PDFInfo
- Publication number
- JP4067074B2 JP4067074B2 JP31208199A JP31208199A JP4067074B2 JP 4067074 B2 JP4067074 B2 JP 4067074B2 JP 31208199 A JP31208199 A JP 31208199A JP 31208199 A JP31208199 A JP 31208199A JP 4067074 B2 JP4067074 B2 JP 4067074B2
- Authority
- JP
- Japan
- Prior art keywords
- skin
- vegetation water
- present
- sensory evaluation
- examples
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Description
【0001】
【発明の属する技術分野】
本発明は、皮膚化粧料に関し、詳しくは、皮膚刺激がなく肌荒れ予防効果を有する皮膚化粧料に関する。
【0002】
【従来の技術及び発明が解決しようとする課題】
オリーブの実は約15〜30重量%(以下、重量%と記載あるは全て質量%を意味する)の脂質成分とともに約70重量%の水分が含まれている。このオリーブ(Olea europaea Linne)の実を圧搾して得られるオリーブ油には、ステアリン酸やパルミチン酸等のの固形グリセリドが約25%、リノール酸やオレイン酸等の液状グリセリドが約75%含まれており、古来、食用油、化粧料、セッケン原料や薬用等に広く用いられているが、このオリーブ油の生産過程においてベジテーション水と呼ばれる多量の水が産する。換言すれば、オリーブを圧搾して得られる水性部である。このベジテーション水には約3%の糖類、約1%の有機酸、約1%脂質とともに約1%のポリフェノールが含まれていることが知られている。しかしながら、このベジテーション水はオリーブ油生産過程における不要物であり廃棄物とされており、その応用に関する検討は全くなされていない。
【0003】
そこで、本発明者等は、ベジテーション水の応用について鋭意検討を行った結果、ベジテーション水を配合することにより優れた肌荒れ予防効果を有する皮膚化粧料が得られることを確認し、本発明を完成した。
【0004】
即ち、本発明の目的は、皮膚刺激がなく優れた肌荒れ予防効果を有する皮膚化粧料を提供することにある。
【0005】
【課題を解決するための手段】
上記目的は、オリーブ油を生産する過程において産するベジテーション水を含有することによって達成される。即ち、本発明はオリーブ油を生産する過程において産するベジテーション水を含有することを特徴とする皮膚化粧料にある。
【0006】
【発明の実施の形態】
本発明の用いるベジテーション水は、通常のオリーブ油を得る過程において産する水溶液部を直接用いることも可能であるが、混入する脂質成分、繊維質成分や種子殻等を濾過や遠心分離を行うことにより除去、精製して用いることが好ましい。また、雑菌の混入による異臭の発生等を抑える目的で水溶液部にアルコール類を添加した後に濾過や遠心等により分離・精製することも可能である。また、得られたベジテーション水を常法により濃縮又は乾固させて用いることもできる。
【0007】
本発明に係るベジテーション水を含有することを特徴とする皮膚化粧料は、必要に応じ、その効果を損なわない範囲で一般に化粧料組成物に用いられる各種成分、すなわち油分、界面活性剤、保湿剤、増粘剤、防腐剤、酸化防止剤、紫外線吸収剤、香料、色素等を組み合わせて配合することができる。本発明に係る皮膚化粧料は、軟膏類、ローション類、乳液類、クリーム類、パック類、ハップ類、顆粒類、ベースメークアップ類等の任意の剤型とすることができる。また、本発明の皮膚化粧料は、粉末、顆粒、錠剤又は液状の入浴剤とすることもできる。そして本発明の皮膚化粧料は、固形、クリーム状又は液状等各種剤型の石鹸、洗顔料、身体用洗浄剤等の洗浄剤とすることもできる。
【0008】
また、上記ベジテーション水の本発明の皮膚化粧料への配合量は、皮膚化粧料の目的、剤形により千差万別であり一概に規定できるものではないが、一般的には乾固物換算で0.001〜10重量%が好ましく、特に好ましくは0.01〜5重量%である。0.001重量未満では、肌荒れ防止効果が不十分な場合が有り、10重量%を越えて配合しても、配合量に見合った効果が得られない場合がある。
【0009】
【実施例】
以下、実施例を挙げて本発明を更に詳細に説明するが、本発明は、これらによって限定されるものではない。また、実施例に示すwt%は、重量%を意味する。
【0010】
実施例1;ベジテーション水の製造例
通常のオリーブ油製造過程において産した水溶液部8リットルに未変性エタノール2リットルを加えた。得られたエタノール水溶液部を4℃、回転数10000rpmにて15分間遠心分離を行い、約1.5kgの固形物と約8.5リットルの水層部とに分離した。得られた水層部を常法に従い、セライト濾過することにより淡褐色のベジテーション水を約8.5リットル得た。得られたベジテーション水を精製水にて100倍希釈した後に分光光度計にてUVスペクトルを測定した結果を図1に示す。
【0011】
実施例2〜4、比較例1(クリーム)
下記の組成からなる、美肌用皮膚化粧料を通常の乳化物の製造方法にて調製し、試料とした。
【0012】
【0013】
・官能評価試験
パネル3名の頬に試料0.4gを一日2回、一週間連用塗布した。その後、下記に示す項目について官能評価により判定し、その効果を評価した。
【0014】
評価項目・評価基準
・刺激感
全く刺激感を感じなかった ○
やや刺激感を感じた △
刺激感を感じた ×
【0015】
・美肌効果
肌がなめらかになった ○
肌がややなめらかになった △
変化なし ×
【0016】
実施例2〜4及び比較例1の官能評価結果を以下に示す。
【0017】
【0018】
上記に示す如く、本発明の実施例2〜4は、前記評価項目についての官能評価により、安全性が高く優れた美肌効果を有していることが明らかとなった。
【0019】
実施例5、6(エッセンス化粧料)
下記組成からなる美肌用エッセンス化粧料を通常のエッセンス化粧料の製造方法にて製造し、実施例2〜4と同一条件で、連用試験・官能評価を実施した。
【0020】
【0021】
本発明に係る皮膚化粧料である実施例5,6は官能評価試験により、高い安全性と優れた美肌効果を有していることが確認された。
【0022】
実施例7(洗顔料)
下記組成からなる洗顔料を常法により調製し、パネル10名にて通常の方法で洗顔を行い、使用中の刺激感と、使用から30分経過した後の刺激感と美肌効果について実施例2〜4と同様の官能評価試験を行った。
【0023】
【0024】
本発明の係る洗顔料である実施例7は官能評価試験により、高い安全性と優れた美肌効果を有していることが確認された。
【0025】
実施例8(身体用洗浄剤;ボディーシャンプー)
下記組成からなる身体用洗浄剤を常法により調製し、パネル10名にて通常の方法で使用し、使用中の刺激感と、使用から30分経過した後の刺激感と美肌効果について実施例2〜4と同様の官能評価試験を行った。
【0026】
【0027】
本発明の係る身体用洗浄剤である実施例8は官能評価試験により、高い安全性と優れた美肌効果を有していることが確認された。
【0028】
実施例9、10
実施例1で得たベジテーション水5.0リットルを凍結乾燥することにより、ベジテーション乾固物220gを得た。実施例7の処方中ベジテーション水30.0wt%に代えこの乾固物3.0wt%を用い洗顔料を、実施例8の処方中ベジテーション水10.0wt%に代えこの乾固物0.5wt%を用い身体用洗浄剤を、それぞれ実施例7、8と同様に調製した。これらを用い実施例7、8と同様の官能評価試験を行い高い安全性と優れた美肌効果を有していることを確認した。
【0029】
【発明の効果】
以上記載の如く、本発明に係るベジテーション水を含有する皮膚化粧料は皮膚刺激がなく優れた美肌効果を示すことは明らかである。
【図面の簡単な説明】
【図1】実施例1で得たベジテーション水のUVスペクトルを示す図である。[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a skin cosmetic, and more particularly, to a skin cosmetic that has no skin irritation and has an effect of preventing rough skin.
[0002]
[Prior art and problems to be solved by the invention]
The fruit of olive contains about 70 to 30% by weight of water together with about 15 to 30% by weight (hereinafter referred to as “% by weight” means lipid percentage). Olive oil obtained by squeezing the fruit of this olive (Olea europaea Linne) contains about 25% solid glycerides such as stearic acid and palmitic acid, and about 75% liquid glycerides such as linoleic acid and oleic acid. Since ancient times, it has been widely used in edible oils, cosmetics, soap raw materials and medicinal products, but a large amount of water called vegetation water is produced in the production process of olive oil. In other words, it is an aqueous part obtained by squeezing olives. This vegetation water is known to contain about 3% saccharides, about 1% organic acids, about 1% lipids with about 1% polyphenols. However, this vegetation water is an unnecessary product in the olive oil production process and is considered a waste product, and its application has not been studied at all.
[0003]
Therefore, as a result of intensive studies on the application of vegetation water, the present inventors confirmed that a skin cosmetic having an excellent skin roughness prevention effect can be obtained by blending vegetation water, and the present invention completed.
[0004]
That is, an object of the present invention is to provide a skin cosmetic that has no skin irritation and has an excellent effect of preventing rough skin.
[0005]
[Means for Solving the Problems]
The above objective is accomplished by containing vegetation water produced in the process of producing olive oil. That is, the present invention provides a skin cosmetic characterized by containing vegetation water produced in the process of producing olive oil.
[0006]
DETAILED DESCRIPTION OF THE INVENTION
The vegetation water used in the present invention can be directly used as an aqueous solution produced in the process of obtaining ordinary olive oil. However, the contaminated lipid component, fiber component, seed shell, etc. are filtered or centrifuged. It is preferable to remove and purify by using In addition, for the purpose of suppressing the generation of a strange odor due to contamination with various bacteria, it is possible to separate and purify by filtration or centrifugation after adding alcohols to the aqueous solution part. Moreover, the obtained vegetation water can also be used by concentrating or drying by a conventional method.
[0007]
Skin cosmetics characterized by containing vegetation water according to the present invention are various components that are generally used in cosmetic compositions, that is, oils, surfactants, and moisturizers as long as they do not impair the effects. Agents, thickeners, preservatives, antioxidants, ultraviolet absorbers, fragrances, pigments and the like can be combined. The skin cosmetic according to the present invention can be in any dosage form such as ointments, lotions, emulsions, creams, packs, haps, granules, base makeups and the like. Moreover, the skin cosmetics of this invention can also be used as a powder, granule, tablet, or a liquid bath agent. And the skin cosmetics of this invention can also be used as detergents, such as soap of various dosage forms, such as solid, cream form, or liquid, a face wash, and a body wash.
[0008]
In addition, the amount of vegetation water added to the skin cosmetic of the present invention varies widely depending on the purpose and dosage form of the skin cosmetic and cannot be generally specified. 0.001-10 weight% is preferable in conversion, Most preferably, it is 0.01-5 weight%. If it is less than 0.001 weight, the rough skin prevention effect may be insufficient, and even if it exceeds 10% by weight, the effect commensurate with the amount may not be obtained.
[0009]
【Example】
EXAMPLES Hereinafter, although an Example is given and this invention is demonstrated further in detail, this invention is not limited by these. Moreover, wt% shown in an Example means weight%.
[0010]
Example 1 Example of Vegitation Water Production 2 liters of unmodified ethanol was added to 8 liters of an aqueous solution produced in the usual olive oil production process. The obtained aqueous ethanol solution was centrifuged at 4 ° C. and a rotational speed of 10,000 rpm for 15 minutes, and separated into about 1.5 kg of solids and about 8.5 liters of an aqueous layer. About 8.5 liters of light brown vegetation water was obtained by carrying out Celite filtration of the obtained water layer part according to a conventional method. FIG. 1 shows the result of measuring the UV spectrum with a spectrophotometer after the obtained vegetation water was diluted 100 times with purified water.
[0011]
Examples 2-4, comparative example 1 (cream)
A skin cosmetic for beautifying skin having the following composition was prepared by a conventional method for producing an emulsion and used as a sample.
[0012]
[0013]
Sensory evaluation test panel A 0.4 g sample was applied to the cheeks of three people twice a day for a week. Thereafter, the following items were judged by sensory evaluation, and the effects were evaluated.
[0014]
Evaluation item / Evaluation criteria / Stimulation
I felt a little irritating △
I felt a sense of irritation ×
[0015]
・ Beautiful skin effect Skin became smooth ○
My skin became slightly smooth △
No change ×
[0016]
The sensory evaluation results of Examples 2 to 4 and Comparative Example 1 are shown below.
[0017]
[0018]
As shown above, Examples 2 to 4 of the present invention were found to have high safety and excellent skin beautifying effects by sensory evaluation of the evaluation items.
[0019]
Examples 5 and 6 (essence cosmetics)
Essence cosmetics for beautiful skin having the following composition were produced by a conventional method for producing essence cosmetics, and subjected to continuous test and sensory evaluation under the same conditions as in Examples 2-4.
[0020]
[0021]
Examples 5 and 6 which are skin cosmetics according to the present invention were confirmed to have high safety and excellent skin beautifying effect by a sensory evaluation test.
[0022]
Example 7 (face wash)
A face wash comprising the following composition was prepared by a conventional method, and the face was washed by a normal method by 10 panelists. Example 2 The sensory evaluation test similar to -4 was performed.
[0023]
[0024]
Example 7 which is the face wash according to the present invention was confirmed to have high safety and an excellent skin beautifying effect by a sensory evaluation test.
[0025]
Example 8 (body cleaning agent; body shampoo)
A body cleaning agent having the following composition was prepared by a conventional method and used in a normal manner by 10 panelists. Example of irritation during use, irritation after 30 minutes from use, and skin beautifying effect The sensory evaluation test similar to 2-4 was done.
[0026]
[0027]
Example 8 which is the body cleaner according to the present invention was confirmed to have high safety and an excellent skin beautifying effect by a sensory evaluation test.
[0028]
Examples 9, 10
By lyophilizing 5.0 liters of vegetation water obtained in Example 1, 220 g of dried vegetation product was obtained. Instead of 30.0 wt% of the vegetation water in the formulation of Example 7 and 3.0 wt% of this dried product, the face wash was replaced with 10.0 wt% of the vegetation water in the formulation of Example 8, and this dried product of 0. A body cleanser was prepared in the same manner as in Examples 7 and 8 using 5 wt%. Using these, the same sensory evaluation test as in Examples 7 and 8 was performed, and it was confirmed that they had high safety and excellent skin beautifying effects.
[0029]
【The invention's effect】
As described above, it is clear that the skin cosmetic containing vegetation water according to the present invention has no skin irritation and exhibits an excellent skin beautifying effect.
[Brief description of the drawings]
1 is a diagram showing a UV spectrum of vegetation water obtained in Example 1. FIG.
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP31208199A JP4067074B2 (en) | 1999-03-09 | 1999-11-02 | Skin cosmetics |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11-61373 | 1999-03-09 | ||
JP6137399 | 1999-03-09 | ||
JP31208199A JP4067074B2 (en) | 1999-03-09 | 1999-11-02 | Skin cosmetics |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2000319161A JP2000319161A (en) | 2000-11-21 |
JP4067074B2 true JP4067074B2 (en) | 2008-03-26 |
Family
ID=26402416
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP31208199A Expired - Fee Related JP4067074B2 (en) | 1999-03-09 | 1999-11-02 | Skin cosmetics |
Country Status (1)
Country | Link |
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JP (1) | JP4067074B2 (en) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2001181197A (en) * | 1999-10-14 | 2001-07-03 | Nisshin Oil Mills Ltd:The | Olive extract |
JP2001181198A (en) * | 1999-10-14 | 2001-07-03 | Nisshin Oil Mills Ltd:The | Skin-beautifying agent, skin aging-preventing agent, bleaching agent and skin care preparation |
JP2001122758A (en) * | 1999-10-22 | 2001-05-08 | Pola Chem Ind Inc | COSMETIC FOR PROTECTING AND IMPROVING AGED SKIN HAVING AGEs DEGRADING ACTIVITY |
FR2825022B1 (en) * | 2001-05-23 | 2005-01-14 | Seppic Sa | COMPOSITION OF OLIVE POLYPHENOLS. USE AS A COSMETIC AND DIETETIC ACTIVE |
FR2867071B1 (en) * | 2004-03-02 | 2006-06-09 | Occitane L | COSMETIC OR DERMATOLOGICAL COMPOSITION BASED ON OLIVE |
JP2006306804A (en) * | 2005-04-28 | 2006-11-09 | Kanebo Cosmetics Inc | Wrinkle formation inhibitor |
US9420820B2 (en) | 2013-08-09 | 2016-08-23 | University Of Tsukuba | Method for isolating polyphenols from olive mill water |
FR3018686B1 (en) | 2014-03-24 | 2017-05-19 | Pierre Fabre Dermo-Cosmetique | COSMETIC USE OF AN OLIVE MARGINS EXTRACT TO REDENSIFY THE HAIR |
-
1999
- 1999-11-02 JP JP31208199A patent/JP4067074B2/en not_active Expired - Fee Related
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Publication number | Publication date |
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JP2000319161A (en) | 2000-11-21 |
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Free format text: JAPANESE INTERMEDIATE CODE: R250 |
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R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
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