JP3532687B2 - Propolis concentrated extract with low ethanol content - Google Patents

Propolis concentrated extract with low ethanol content

Info

Publication number
JP3532687B2
JP3532687B2 JP03535396A JP3535396A JP3532687B2 JP 3532687 B2 JP3532687 B2 JP 3532687B2 JP 03535396 A JP03535396 A JP 03535396A JP 3535396 A JP3535396 A JP 3535396A JP 3532687 B2 JP3532687 B2 JP 3532687B2
Authority
JP
Japan
Prior art keywords
propolis
extract
concentrated
ethanol
propolis extract
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP03535396A
Other languages
Japanese (ja)
Other versions
JPH09206002A (en
Inventor
俊雄 森川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
MORIKAWA KENKODO CO., LTD.
Original Assignee
MORIKAWA KENKODO CO., LTD.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by MORIKAWA KENKODO CO., LTD. filed Critical MORIKAWA KENKODO CO., LTD.
Priority to JP03535396A priority Critical patent/JP3532687B2/en
Publication of JPH09206002A publication Critical patent/JPH09206002A/en
Application granted granted Critical
Publication of JP3532687B2 publication Critical patent/JP3532687B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Landscapes

  • Jellies, Jams, And Syrups (AREA)

Description

【発明の詳細な説明】 【0001】 【発明の属する技術分野】本発明は、プロポリス濃縮エ
キス(プロポリスコンクエキス)に関し、特に、エタノ
ール濃度を低く抑えたプロポリス濃縮エキスに関する。 【0002】 【従来の技術とその課題】プロポリスは、一般にハチヤ
ニとも呼ばれ、ミツバチが花や樹脂のヤニ状成分をかみ
続けることにより、該成分とミツバチの唾液中の酵素と
が混ぜ合わされて生じる物質である。このプロポリス
は、フラボノイド類、ミネラル、ビタミンなどの微量栄
養素を含有しているため、健康増進や疾病治療を促進す
る食品素材として注目されている。 【0003】このプロポリスは、一般に、原料プロポリ
スからエタノールを用いて有用成分を抽出してプロポリ
スエキスとし、これからエタノールを蒸発、濃縮したプ
ロポリス濃縮エキスとして供される。従来のこのような
プロポリス濃縮エキスは、エタノールを高濃度で含有
(一般に20〜30重量%)しており、アルコール臭気が残
存している点において必ずしも満足できるものではな
い。この際、無理にエタノールを蒸発させると流動性が
なくなり、他の添加成分と混合しにくくなって食品素材
として使用に適さなくなる。 【0004】 【課題を解決するための手段】本発明者は、特定成分を
加えることにより、アルコール含有量を低くしても、他
の添加成分との混合を容易にするような流動性を保持す
る優れたプロポリス濃縮エキスが得られることを見出し
た。 【0005】かくして、本発明に従えば、プロポリスエ
キスに対して、小麦胚芽油を15〜30重量%含有し、エタ
ノール含有量が5重量%以下であることを特徴とするプ
ロポリス濃縮エキスが提供される。 【0006】 【発明の実施の形態】本発明に従うエタノール含有量の
低いプロポリス濃縮エキスは、異物を除去したプロポリ
ス原料をエタノールで抽出して得たプロポリスエキスを
濃縮する際に、小麦胚芽油を加えることによって得られ
る。 【0007】小麦胚芽油は、プロポリスエキスに対し
て、15〜30重量%、好ましくは、20〜30重量%添加す
る。この小麦胚芽油の添加により、エタノール含有量を
その臭気を感じさせないような5重量%以下(プロポリ
スエキス基準)になるように濃縮を行っても、得られる
プロポリス濃縮エキスは充分な流動性を保持している。
従って、たとえば、プロポリス製品に多用されている他
の添加成分、たとえば、乳糖、β−CD(サイクロデキ
ストリン)、またはハチミツなどを均質に混合すること
ができる。このようにして得られたプロポリス製品は、
一般に、最終の製品形態(例えば、カプセル)にするに
際してさらにエタノールが除去される。 【0008】以下、本発明の特徴をさらに明らかにする
ため、実施例に沿って本発明を説明する。 【0009】 【実施例】天然のプロポリスを目視にて選別し、鉄など
の金属、石や木屑等の夾雑物を除去したものを凍結後、
0.8mmのフィルターをセットした粉砕機で粉砕し、プロ
ポリス粉末とした。 【0010】プロポリス粉末13kgに原液(99.5%)の一
級エタノール45リットルを加え、撹拌機で10時間混合撹
拌した後、120時間静置して抽出した。抽出残さにエタ
ノールを45リットル加え、撹拌機で撹拌し、120時間静
置して再抽出を行った。これを2回繰り返して抽出した
ものを吸引濾過器で濾過してブリックス30に調製し、粗
プロポリスエキスとした。 【0011】粗プロポリスエキス7.0kg、小麦胚芽油
(サミット製油社製)0.25kgを秤量し、蒸発濃縮機のフ
ラスコに入れ、ウォーターバスの温度を40℃にセット
し、1kgになるまでエタノールを蒸発・濃縮し、本発明
に従う小麦胚芽油添加プロポリス濃縮エキスを得た。プ
ロポリス濃縮エキス中のエタノール含有率3.5重量%、
小麦胚芽油含有率25重量%であった。 【0012】同様に、粗プロポリスエキス7.0kgを秤量
し、蒸発濃縮機のフラスコに入れ、ウォーターバスの温
度を40℃にセットし、小麦胚芽油を加えずに1kgになる
までエタノールを蒸発・濃縮して得たプロポリス濃縮エ
キスを対照とした。 【0013】本発明に従う小麦胚芽油添加プロポリス濃
縮エキス、および対照のプロポリス濃縮エキスをそれぞ
れ0.8mmになるまで粉状化し、これに乳糖またはβ−サ
イクロデキストリンを添加、混合してみた。 【0014】対照のプロポリス濃縮エキスの場合、乳糖
またはβ−サイクロデキストリンを添加すると、混合す
る力がなく、乳糖やβ−サイクロデキストリン(β−C
D)がダマ状になってしまい、均一な混合物は得られな
かった。特に、この傾向は、対照のプロポリスエキスに
対して等重量以上の乳糖またはβ−CDを添加すると顕
著であった。 【0015】これに対して、本発明の小麦胚芽油添加プ
ロポリス濃縮エキスは、濃縮エキス1kgに対して乳糖や
β−CDを3.5kgまで加えても均質な混合物を得ること
ができた。
Description: BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a concentrated propolis extract (propolis conc extract), and more particularly to a concentrated propolis extract with a low ethanol concentration. 2. Description of the Related Art Propolis, which is also commonly referred to as bee syrup, is produced when a bee continues to bite a flower-like or resin-like component of a flower, and this component is mixed with an enzyme in the saliva of the bee. Is a substance. Since propolis contains trace nutrients such as flavonoids, minerals, and vitamins, it has been attracting attention as a food material that promotes health promotion and disease treatment. [0003] This propolis is generally used as a propolis extract by extracting useful components from raw propolis using ethanol to produce a propolis extract, and then evaporating and concentrating the ethanol to provide a propolis concentrate extract. Such a conventional concentrated propolis extract contains ethanol at a high concentration (generally 20 to 30% by weight) and is not always satisfactory in that alcohol odor remains. At this time, if ethanol is forcibly evaporated, the fluidity is lost, and it becomes difficult to mix with other additive components, which makes the material unsuitable for use as a food material. SUMMARY OF THE INVENTION The present inventor has found that by adding a specific component, even if the alcohol content is reduced, the fluidity that facilitates mixing with other additional components is maintained. It has been found that an excellent concentrated propolis extract can be obtained. Thus, according to the present invention, there is provided a concentrated propolis extract containing 15 to 30% by weight of wheat germ oil and 5% by weight or less of ethanol based on the propolis extract. You. The concentrated propolis extract having a low ethanol content according to the present invention is obtained by adding wheat germ oil when the propolis extract obtained by extracting a propolis raw material from which foreign substances have been removed with ethanol is concentrated. Obtained by: [0007] Wheat germ oil is added to the propolis extract in an amount of 15 to 30% by weight, preferably 20 to 30% by weight. By adding this wheat germ oil, even if concentration is performed so that the ethanol content is 5% by weight or less (based on propolis extract) so that the odor is not felt, the obtained concentrated propolis extract retains sufficient fluidity. are doing.
Therefore, for example, other additive components frequently used in propolis products, such as lactose, β-CD (cyclodextrin), or honey, can be mixed homogeneously. The propolis product thus obtained is
Generally, more ethanol is removed in the final product form (eg, capsules). Hereinafter, the present invention will be described with reference to Examples to further clarify the features of the present invention. [0009] [Example] Natural propolis is selected by visual observation, and after removing metals such as iron and impurities such as stones and wood chips, freezing,
It was pulverized with a pulverizer equipped with a 0.8 mm filter to obtain propolis powder. To 13 kg of propolis powder was added 45 liters of a stock solution (99.5%) of primary ethanol, mixed and stirred for 10 hours with a stirrer, and allowed to stand for 120 hours to extract. To the extraction residue, 45 liters of ethanol was added, stirred with a stirrer, and allowed to stand for 120 hours for re-extraction. This was repeated twice, and the extract was filtered through a suction filter to prepare Brix 30, which was used as a crude propolis extract. [0011] 7.0 kg of crude propolis extract and 0.25 kg of wheat germ oil (manufactured by Summit Oil Co., Ltd.) are weighed, placed in a flask of an evaporating concentrator, the temperature of a water bath is set at 40 ° C, and ethanol is evaporated to 1 kg. Concentrated to obtain a concentrated propolis extract containing wheat germ oil according to the present invention. Ethanol content 3.5% by weight in concentrated propolis extract,
The wheat germ oil content was 25% by weight. Similarly, 7.0 kg of the crude propolis extract is weighed, placed in a flask of an evaporating concentrator, the temperature of the water bath is set at 40 ° C., and ethanol is evaporated and concentrated to 1 kg without adding wheat germ oil. The concentrated propolis extract obtained as a control was used as a control. The concentrated propolis extract containing wheat germ oil and the concentrated propolis extract of the control according to the present invention were each powdered to 0.8 mm, and lactose or β-cyclodextrin was added thereto and mixed. In the case of the control propolis concentrated extract, when lactose or β-cyclodextrin is added, there is no mixing power and lactose or β-cyclodextrin (β-C
D) became lumpy and a uniform mixture could not be obtained. In particular, this tendency was remarkable when lactose or β-CD was added in an amount equal to or more than that of the control propolis extract. On the other hand, the concentrated propolis extract containing wheat germ oil of the present invention could obtain a homogeneous mixture even if lactose or β-CD was added up to 3.5 kg per 1 kg of the concentrated extract.

Claims (1)

(57)【特許請求の範囲】 【請求項1】 小麦胚芽油を15〜30重量%含有し、エタ
ノール含有量が5重量%以下であることを特徴とするプ
ロポリス濃縮エキス。
(57) [Claim 1] A concentrated propolis extract containing 15 to 30% by weight of wheat germ oil and having an ethanol content of 5% by weight or less.
JP03535396A 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content Expired - Lifetime JP3532687B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP03535396A JP3532687B2 (en) 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP03535396A JP3532687B2 (en) 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content

Publications (2)

Publication Number Publication Date
JPH09206002A JPH09206002A (en) 1997-08-12
JP3532687B2 true JP3532687B2 (en) 2004-05-31

Family

ID=12439515

Family Applications (1)

Application Number Title Priority Date Filing Date
JP03535396A Expired - Lifetime JP3532687B2 (en) 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content

Country Status (1)

Country Link
JP (1) JP3532687B2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007530433A (en) * 2004-03-30 2007-11-01 学校法人早稲田大学 Propolis extract and extraction method thereof

Also Published As

Publication number Publication date
JPH09206002A (en) 1997-08-12

Similar Documents

Publication Publication Date Title
JP2007306887A (en) Method for producing feed silage
BR0006040A (en) Dietary supplement derived from fermented milk for the prevention of osteoporosis
JP2017127231A (en) Composition for eating and drinking
JP3532687B2 (en) Propolis concentrated extract with low ethanol content
US5780096A (en) Process for preparation of powdery chlorella extract
EP2178396A1 (en) Method of removal of bitter taste from olive juice extract
JP3225923B2 (en) Food material consisting of cultured kelp rhizome
JP6778922B2 (en) Manufacturing method of natural product-derived ingredient-containing composition, natural product-derived ingredient-containing composition, functional foods and drinks using this
KR100862807B1 (en) Manufacturing method of natural-friendly germicide for agriculture using propolis
JP2515680B2 (en) Freshwater fish feed
JPS63207363A (en) Powder bagasse
JP2002306092A (en) Propolis product having antioxidant activity
JP2002017274A (en) Propolis extract powder and method for producing the same
JPH01181750A (en) Preparation of powdery propolis
CN107927345A (en) A kind of feed addictive and application process for improving quality of fur of furry animal
JP2005145989A (en) Manufacturing method of concentrated liquid for extracting fucoidan from powder of dried nemacystus decipiens
JP2018048101A (en) Eye disease treatment agent and production method thereof
JP2018048102A (en) Eye disease treatment agent and production method thereof
JP2007084460A (en) Skin care composition
JP3442031B2 (en) healthy food
JP2001078714A (en) Food material for magnesium supplement and magnesium- conjugated protein and/or magnesium-conjugated polysaccharide protein, and their production
JP2005021039A (en) Health food and method for producing the same
CN110679767A (en) Mixed pig feed additive and preparation method thereof
JPS62100294A (en) Method of extracting red alga belonging to genus porphyra
JPS63157944A (en) Honey composition

Legal Events

Date Code Title Description
TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20040224

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20040304

R150 Certificate of patent (=grant) or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100312

Year of fee payment: 6

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130312

Year of fee payment: 9

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130312

Year of fee payment: 9

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20150312

Year of fee payment: 11

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term