JPH09206002A - Propolis concentrated extract with low ethanol content - Google Patents

Propolis concentrated extract with low ethanol content

Info

Publication number
JPH09206002A
JPH09206002A JP8035353A JP3535396A JPH09206002A JP H09206002 A JPH09206002 A JP H09206002A JP 8035353 A JP8035353 A JP 8035353A JP 3535396 A JP3535396 A JP 3535396A JP H09206002 A JPH09206002 A JP H09206002A
Authority
JP
Japan
Prior art keywords
propolis
extract
concentrated extract
ethanol
wheat germ
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP8035353A
Other languages
Japanese (ja)
Other versions
JP3532687B2 (en
Inventor
Toshio Morikawa
俊雄 森川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
MORIKAWA KENKOUDOU KK
Original Assignee
MORIKAWA KENKOUDOU KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by MORIKAWA KENKOUDOU KK filed Critical MORIKAWA KENKOUDOU KK
Priority to JP03535396A priority Critical patent/JP3532687B2/en
Publication of JPH09206002A publication Critical patent/JPH09206002A/en
Application granted granted Critical
Publication of JP3532687B2 publication Critical patent/JP3532687B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

PROBLEM TO BE SOLVED: To obtain a propolis concentrated extract having the fluidity for facilitating the mixing of other additive ingredients even when the alcohol content is reduced by adding a specific ingredient thereto. SOLUTION: This propolis concentrated extract with a low ethanol content comprises 15-30wt.% wheat germ oil and has <=5wt.% ethanol content. This extract is obtained by adding the wheat germ oil to a propolis extract prepared by extraction thereof from a raw material with ethanol when concentrating the propolis extract and providing the concentrated extract, containing 15-30wt.% wheat germ oil and having <=5wt.% ethanol content. For example, honey is homogeneously mixed with the concentrated extract to afford a propolis product.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、プロポリス濃縮エ
キス(プロポリスコンクエキス)に関し、特に、エタノ
ール濃度を低く抑えたプロポリス濃縮エキスに関する。
TECHNICAL FIELD The present invention relates to a propolis concentrated extract (propolis conch extract), and more particularly to a propolis concentrated extract having a low ethanol concentration.

【0002】[0002]

【従来の技術とその課題】プロポリスは、一般にハチヤ
ニとも呼ばれ、ミツバチが花や樹脂のヤニ状成分をかみ
続けることにより、該成分とミツバチの唾液中の酵素と
が混ぜ合わされて生じる物質である。このプロポリス
は、フラボノイド類、ミネラル、ビタミンなどの微量栄
養素を含有しているため、健康増進や疾病治療を促進す
る食品素材として注目されている。
2. Description of the Related Art Propolis, which is generally called "honeybee", is a substance formed by the honeybees continuing to bite the resinous and resinous resinous components and mixing them with the enzymes in the saliva of the honeybees. . Since this propolis contains micronutrients such as flavonoids, minerals and vitamins, it has attracted attention as a food material that promotes health promotion and disease treatment.

【0003】このプロポリスは、一般に、原料プロポリ
スからエタノールを用いて有用成分を抽出してプロポリ
スエキスとし、これからエタノールを蒸発、濃縮したプ
ロポリス濃縮エキスとして供される。従来のこのような
プロポリス濃縮エキスは、エタノールを高濃度で含有
(一般に20〜30重量%)しており、アルコール臭気が残
存している点において必ずしも満足できるものではな
い。この際、無理にエタノールを蒸発させると流動性が
なくなり、他の添加成分と混合しにくくなって食品素材
として使用に適さなくなる。
This propolis is generally used as a propolis concentrated extract obtained by extracting useful components from raw material propolis with ethanol to obtain a propolis extract, and then evaporating and concentrating ethanol from the propolis extract. Such a conventional propolis concentrated extract contains ethanol at a high concentration (generally 20 to 30% by weight), and is not necessarily satisfactory in that alcohol odor remains. At this time, if ethanol is forcibly evaporated, it loses fluidity, becomes difficult to mix with other additive components, and becomes unsuitable for use as a food material.

【0004】[0004]

【課題を解決するための手段】本発明者は、特定成分を
加えることにより、アルコール含有量を低くしても、他
の添加成分との混合を容易にするような流動性を保持す
る優れたプロポリス濃縮エキスが得られることを見出し
た。
Means for Solving the Problems The present inventor has found that by adding a specific component, even if the alcohol content is lowered, excellent fluidity is maintained to facilitate mixing with other additive components. It was found that a propolis concentrated extract can be obtained.

【0005】かくして、本発明に従えば、プロポリスエ
キスに対して、小麦胚芽油を15〜30重量%含有し、エタ
ノール含有量が5重量%以下であることを特徴とするプ
ロポリス濃縮エキスが提供される。
Thus, according to the present invention, there is provided a propolis concentrated extract containing 15 to 30% by weight of wheat germ oil and 5% by weight or less of ethanol based on the propolis extract. It

【0006】[0006]

【発明の実施の形態】本発明に従うエタノール含有量の
低いプロポリス濃縮エキスは、異物を除去したプロポリ
ス原料をエタノールで抽出して得たプロポリスエキスを
濃縮する際に、小麦胚芽油を加えることによって得られ
る。
BEST MODE FOR CARRYING OUT THE INVENTION A propolis concentrated extract having a low ethanol content according to the present invention is obtained by adding wheat germ oil when concentrating a propolis extract obtained by extracting a propolis raw material from which foreign substances have been removed with ethanol. To be

【0007】小麦胚芽油は、プロポリスエキスに対し
て、15〜30重量%、好ましくは、20〜30重量%添加す
る。この小麦胚芽油の添加により、エタノール含有量を
その臭気を感じさせないような5重量%以下(プロポリ
スエキス基準)になるように濃縮を行っても、得られる
プロポリス濃縮エキスは充分な流動性を保持している。
従って、たとえば、プロポリス製品に多用されている他
の添加成分、たとえば、乳糖、β−CD(サイクロデキ
ストリン)、またはハチミツなどを均質に混合すること
ができる。このようにして得られたプロポリス製品は、
一般に、最終の製品形態(例えば、カプセル)にするに
際してさらにエタノールが除去される。
[0007] Wheat germ oil is added to the propolis extract in an amount of 15 to 30% by weight, preferably 20 to 30% by weight. By adding this wheat germ oil, even if the ethanol content is concentrated to 5% by weight or less (propolis extract standard) so that the odor is not felt, the obtained propolis concentrated extract retains sufficient fluidity. doing.
Therefore, for example, other additive components often used in propolis products, such as lactose, β-CD (cyclodextrin), or honey, can be mixed homogeneously. The propolis product thus obtained is
Generally, further ethanol is removed in making the final product form (eg, capsule).

【0008】以下、本発明の特徴をさらに明らかにする
ため、実施例に沿って本発明を説明する。
The present invention will be described below with reference to examples in order to further clarify the characteristics of the present invention.

【0009】[0009]

【実施例】天然のプロポリスを目視にて選別し、鉄など
の金属、石や木屑等の夾雑物を除去したものを凍結後、
0.8mmのフィルターをセットした粉砕機で粉砕し、プロ
ポリス粉末とした。
[Examples] Natural propolis was visually selected and freed from metals such as iron and impurities such as stones and wood chips, after freezing,
It was crushed with a crusher having a 0.8 mm filter set to give a propolis powder.

【0010】プロポリス粉末13kgに原液(99.5%)の一
級エタノール45リットルを加え、撹拌機で10時間混合撹
拌した後、120時間静置して抽出した。抽出残さにエタ
ノールを45リットル加え、撹拌機で撹拌し、120時間静
置して再抽出を行った。これを2回繰り返して抽出した
ものを吸引濾過器で濾過してブリックス30に調製し、粗
プロポリスエキスとした。
To 13 kg of propolis powder, 45 liters of a stock solution (99.5%) of primary ethanol was added, mixed and stirred with a stirrer for 10 hours, and then allowed to stand for 120 hours for extraction. 45 liters of ethanol was added to the extraction residue, and the mixture was stirred with a stirrer and left standing for 120 hours for re-extraction. This was repeated twice and the extract was filtered with a suction filter to prepare Brix 30 to obtain a crude propolis extract.

【0011】粗プロポリスエキス7.0kg、小麦胚芽油
(サミット製油社製)0.25kgを秤量し、蒸発濃縮機のフ
ラスコに入れ、ウォーターバスの温度を40℃にセット
し、1kgになるまでエタノールを蒸発・濃縮し、本発明
に従う小麦胚芽油添加プロポリス濃縮エキスを得た。プ
ロポリス濃縮エキス中のエタノール含有率3.5重量%、
小麦胚芽油含有率25重量%であった。
[0011] 7.0 kg of crude propolis extract and 0.25 kg of wheat germ oil (manufactured by Summit Oil & Oil Co., Ltd.) were weighed and placed in a flask of an evaporative concentrator, the temperature of the water bath was set to 40 ° C, and ethanol was evaporated to 1 kg. -Concentrated to obtain a wheat germ oil-added propolis concentrated extract according to the present invention. The ethanol content of the propolis concentrated extract is 3.5% by weight,
The wheat germ oil content was 25% by weight.

【0012】同様に、粗プロポリスエキス7.0kgを秤量
し、蒸発濃縮機のフラスコに入れ、ウォーターバスの温
度を40℃にセットし、小麦胚芽油を加えずに1kgになる
までエタノールを蒸発・濃縮して得たプロポリス濃縮エ
キスを対照とした。
Similarly, 7.0 kg of crude propolis extract was weighed, placed in a flask of an evaporative concentrator, the temperature of the water bath was set to 40 ° C., and ethanol was evaporated and concentrated to 1 kg without adding wheat germ oil. The propolis concentrated extract obtained in this way was used as a control.

【0013】本発明に従う小麦胚芽油添加プロポリス濃
縮エキス、および対照のプロポリス濃縮エキスをそれぞ
れ0.8mmになるまで粉状化し、これに乳糖またはβ−サ
イクロデキストリンを添加、混合してみた。
The wheat germ oil-added propolis concentrated extract according to the present invention and the control propolis concentrated extract were each pulverized to 0.8 mm, and lactose or β-cyclodextrin was added thereto and mixed.

【0014】対照のプロポリス濃縮エキスの場合、乳糖
またはβ−サイクロデキストリンを添加すると、混合す
る力がなく、乳糖やβ−サイクロデキストリン(β−C
D)がダマ状になってしまい、均一な混合物は得られな
かった。特に、この傾向は、対照のプロポリスエキスに
対して等重量以上の乳糖またはβ−CDを添加すると顕
著であった。
In the case of the control propolis concentrated extract, when lactose or β-cyclodextrin was added, there was no mixing power, and lactose or β-cyclodextrin (β-C
D) became lumpy and a uniform mixture could not be obtained. In particular, this tendency was remarkable when an equal weight or more of lactose or β-CD was added to the control propolis extract.

【0015】これに対して、本発明の小麦胚芽油添加プ
ロポリス濃縮エキスは、濃縮エキス1kgに対して乳糖や
β−CDを3.5kgまで加えても均質な混合物を得ること
ができた。
On the other hand, the wheat germ oil-containing propolis concentrated extract of the present invention was able to obtain a homogeneous mixture even if lactose or β-CD was added up to 3.5 kg per 1 kg of the concentrated extract.

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 小麦胚芽油を15〜30重量%含有し、エタ
ノール含有量が5重量%以下であることを特徴とするプ
ロポリス濃縮エキス。
1. A propolis concentrated extract comprising 15 to 30% by weight of wheat germ oil and having an ethanol content of 5% by weight or less.
JP03535396A 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content Expired - Lifetime JP3532687B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP03535396A JP3532687B2 (en) 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP03535396A JP3532687B2 (en) 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content

Publications (2)

Publication Number Publication Date
JPH09206002A true JPH09206002A (en) 1997-08-12
JP3532687B2 JP3532687B2 (en) 2004-05-31

Family

ID=12439515

Family Applications (1)

Application Number Title Priority Date Filing Date
JP03535396A Expired - Lifetime JP3532687B2 (en) 1996-01-29 1996-01-29 Propolis concentrated extract with low ethanol content

Country Status (1)

Country Link
JP (1) JP3532687B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005094853A1 (en) * 2004-03-30 2005-10-13 Waseda University Propolis extract and method for extracting the same

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005094853A1 (en) * 2004-03-30 2005-10-13 Waseda University Propolis extract and method for extracting the same

Also Published As

Publication number Publication date
JP3532687B2 (en) 2004-05-31

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