JP3459617B2 - Processed dried egg yolk - Google Patents

Processed dried egg yolk

Info

Publication number
JP3459617B2
JP3459617B2 JP2000163465A JP2000163465A JP3459617B2 JP 3459617 B2 JP3459617 B2 JP 3459617B2 JP 2000163465 A JP2000163465 A JP 2000163465A JP 2000163465 A JP2000163465 A JP 2000163465A JP 3459617 B2 JP3459617 B2 JP 3459617B2
Authority
JP
Japan
Prior art keywords
egg yolk
dried egg
dried
processed
carbon dioxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2000163465A
Other languages
Japanese (ja)
Other versions
JP2001340064A (en
Inventor
稔秀 佐藤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
QP Corp
Original Assignee
QP Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by QP Corp filed Critical QP Corp
Priority to JP2000163465A priority Critical patent/JP3459617B2/en
Publication of JP2001340064A publication Critical patent/JP2001340064A/en
Application granted granted Critical
Publication of JP3459617B2 publication Critical patent/JP3459617B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、加工乾燥卵黄の新
規な製法に関する。
TECHNICAL FIELD The present invention relates to a novel method for producing processed dried egg yolk.

【0002】[0002]

【従来の技術】低コレステロール食品は、動脈硬化症の
患者のための療養食としてのみならず、最近では健康食
品としてその需要が高まりつつある。ところで、卵黄は
特有の食味と風味を有する食品であり、菓子やマヨネー
ズ等の原料として用いられているが、コレステロールを
比較的多く含むため、コレステロールを低減させたもの
が健康食品や加工食品等の原料として望まれている。従
来より、脱コレステロールをした卵黄を得るには、スプ
レードライした乾燥卵黄を超臨界二酸化炭素処理する方
法(特公昭62−51092)や、ドラムドライした乾
燥卵黄を超臨界二酸化炭素処理する方法(特表平7−5
07930)が提案されている。しかしながら、上記従
来法の前者によると低濃度食塩水に対して戻りはよい
が、脱コレステロール処理をするに当たり、超臨界状態
の二酸化炭素が偏流したり、目詰りしやすいためか脱コ
レステロール率が悪い場合もあった。また、後者による
と脱コレステロール率は良いが、ドラムドライにより卵
黄を過剰に加熱してその蛋白質を熱変性させてしまうた
めか、低濃度食塩水に対して戻りの悪いものしか得られ
ず、いずれにしても健康食品等の原料に適した加工乾燥
卵黄が得にくいという問題があった。
2. Description of the Related Art Low-cholesterol foods are not only used as therapeutic foods for patients with arteriosclerosis, but are recently in high demand as health foods. By the way, egg yolk is a food having a unique taste and flavor, and is used as a raw material for confectionery, mayonnaise, etc., but since it contains a relatively large amount of cholesterol, those with reduced cholesterol such as health foods and processed foods. It is desired as a raw material. Conventionally, to obtain decholesterolized egg yolk, a method of treating spray-dried dry egg yolk with supercritical carbon dioxide (Japanese Patent Publication No. 62-51092) or a method of treating drum-dried dry egg yolk with supercritical carbon dioxide (special Front flat 7-5
07930) has been proposed. However, according to the former of the above-mentioned conventional method, although it is possible to return to low-concentration saline, the decholesterolization rate is poor because the carbon dioxide in the supercritical state is unbalanced or easily clogged during the decholesterolization treatment. In some cases. In addition, according to the latter, the cholesterol removal rate is good, but because the egg yolk is overheated by drum drying and the protein is heat-denatured, only a poor return to low-concentration saline is obtained. However, there is a problem that it is difficult to obtain processed dried egg yolk suitable for raw materials such as health foods.

【0003】[0003]

【発明が解決しようとする課題】そこで、本発明は低濃
度食塩水に対して戻りがよく、かつ、脱コレステロール
率も高い加工乾燥卵黄を製造する方法を提供することを
目的としてなされたものである。
Therefore, the present invention has been made for the purpose of providing a method for producing a processed dried egg yolk which is highly reversible to low-concentration saline and has a high decholesterolization rate. is there.

【0004】[0004]

【課題を解決するための手段】この目的は、 (1)スプレードライして得られる乾燥卵黄を清水のバ
インダーを用いて押出し造粒して多孔性の顆粒とした
後、これを超臨界二酸化炭素で脱コレステロール処理
し、粒径の分布10〜100μmの微粒子にすることを
特徴とする加工乾燥卵黄の製法。 (2)スクリーン径が1.5〜3.0mmの造粒機で押
出し造粒することを特徴とする(1)の加工乾燥卵黄の
製法。によって達成される。
[Means for Solving the Problems] (1) Dry egg yolk obtained by spray drying
Extruded and granulated using an inderPorous granules
After that, decholesterolize it with supercritical carbon dioxide
The particle size distribution is 10-100 μm.
A feature is the manufacturing method of processed dried egg yolk. (2) Press with a granulator with a screen diameter of 1.5 to 3.0 mm.
(1) Processed dried egg yolk
Manufacturing method. Achieved by

【0005】[0005]

【発明の実施の形態】以下、本発明を詳説する。なお、
本発明において「%」とは、「質量%」、を意味する。
本発明の実施に当って、まず原料の卵黄を用意する。こ
の卵黄としては鶏卵を割卵して得た生卵黄や冷凍卵黄を
解凍したものを用いればよい。
BEST MODE FOR CARRYING OUT THE INVENTION The present invention is described in detail below. In addition,
In the present invention, “%” means “mass%”.
In carrying out the present invention, first, a raw material egg yolk is prepared. As this egg yolk, raw egg yolk obtained by breaking chicken eggs or thawed frozen egg yolk may be used.

【0006】次に、原料の卵黄をスプレードライして乾
燥卵黄を得る。この乾燥卵黄は粒径の分布が10〜10
0μmの範囲からなる微粉末である。なお、ドラムドラ
イのように過剰な加熱をする乾燥法は、後の試験例にも
示すように、低濃度食塩水に対する溶解力のない加工乾
燥卵黄しか得られないので、不適である。
Next, the raw egg yolk is spray-dried to obtain dried egg yolk. This dried egg yolk has a particle size distribution of 10 to 10
It is a fine powder having a range of 0 μm. Incidentally, a drying method such as drum drying in which excessive heating is carried out is not suitable because only a processed dried egg yolk having no dissolving power for a low-concentration salt solution can be obtained, as will be shown in the later test examples.

【0007】次に、この乾燥卵黄を清水のバインダーを
用いて押出し造粒し、その後乾燥させ水分7%以下の顆
粒を得る。従来の造粒においては、澱粉や蛋白粉等を加
えたバインダーを用いるのが常識である。しかし、本発
明ではこのようなバインダーを用いると澱粉や蛋白の皮
膜が造粒によって得られる顆粒の表面を覆ってしまうこ
とになる。その結果低コレステロール処理に当って超臨
界状態の二酸化炭素が顆粒内へ侵入せず、コレステロー
ル低減効率を著しく低下させてしまうので不適である。
Next, the dried egg yolk is extruded and granulated by using a binder of fresh water, and then dried to obtain granules having a water content of 7% or less. In conventional granulation, it is common knowledge to use a binder to which starch, protein powder or the like is added. However, in the present invention, when such a binder is used, a film of starch or protein covers the surface of granules obtained by granulation. As a result, carbon dioxide in a supercritical state does not penetrate into the granules in the low cholesterol treatment, and the cholesterol reduction efficiency is significantly lowered, which is not suitable.

【0008】清水のバインダーを用いるに当って、乾燥
卵黄に対する加水量は18〜25%が望ましい。加水量
が多いと多孔性の顆粒が出来にくくなり、一方、少なす
ぎると顆粒自体を形成することが出来ないとともに、た
とえ顆粒に仕上げても乾燥時に顆粒が崩れ、微粉へ戻っ
てしまうからである。この加水は、乾燥卵黄を攪拌しつ
つ、清水を噴霧状に添加するとダマが発生することなく
能率よく行うことができる。
When using the binder of fresh water, the amount of water added to the dried egg yolk is preferably 18 to 25%. If the amount of water added is large, it becomes difficult to form porous granules. On the other hand, if the amount is too small, the granules themselves cannot be formed, and even if the granules are finished, the granules collapse during drying and return to fine powder. . This water addition can be efficiently performed without adding lumps by adding fresh water in a spray state while stirring the dried egg yolk.

【0009】また、上記清水のバインダーを加えた乾燥
卵黄の造粒は、バケット式ブレード型押出し造粒機等を
用い、常法により行えばよい。この造粒によって顆粒が
得られるが、造粒機の押出しスクリーンの径は1.5〜
3.0mmが望ましい。1.5mm未満では圧力により
多孔性が失われ超臨界二酸化炭素の顆粒内への侵入が抑
制される。また、3.0mmを超えると卵黄粒子同士の
結着力が弱いため、顆粒を形成しずらく、顆粒中に乾燥
卵黄の微粉末が混入して、超臨界二酸化炭素処理するに
当って偏流が生じ、脱コレステロール効率が悪いからで
ある。スクリーン径1.5〜3.0mmの造粒機で押出
し造粒をすれば後の試験例にも示すように著しい脱コレ
ステロール効率を示す。
The dry egg yolk added with the fresh water binder may be granulated by a conventional method using a bucket type blade type granulator. Granules are obtained by this granulation, and the diameter of the extrusion screen of the granulator is 1.5 to
3.0 mm is desirable. If it is less than 1.5 mm, the porosity is lost due to the pressure, and the penetration of supercritical carbon dioxide into the granules is suppressed. Further, when the diameter exceeds 3.0 mm, the binding force between the egg yolk particles is weak, so that it is difficult to form granules, and fine powder of dry egg yolk is mixed in the granules, which causes a drift in supercritical carbon dioxide treatment. , Because the cholesterol removal efficiency is poor. When extrusion granulation is performed with a granulator having a screen diameter of 1.5 to 3.0 mm, remarkable cholesterol removal efficiency is exhibited as shown in the following test examples.

【0010】最後に、上記顆粒を常法により超臨界二酸
化炭素により脱コレステロール処理すれば、目的の加工
乾燥卵黄を得ることができる。ここで脱コレステロール
とは、乾燥卵黄中のコレステロールを完全に除くことの
ほか、コレステロール含量をほぼ0.5%以下に低減さ
せることを含むものである。なお、超臨界処理された顆
粒乾燥卵黄は結着性のあるバインダーを使用せずに造粒
しているため、容易にもとのスプレードライした乾燥卵
黄の粒径分布の範囲である粒径10〜100μmの微粉
末に戻る。ここで粒径分布の範囲が10〜100μmで
あるとは、微粉末のほとんど(95%以上)が10〜1
00μm粒径であることをいう。この微粉末は表面積が
大きいため、低濃度食塩水でも溶解することができる。
Finally, the above-mentioned granules are subjected to decholesterolization treatment with supercritical carbon dioxide by a conventional method to obtain the desired processed dried egg yolk. Here, decholesterolization includes not only complete removal of cholesterol in dried egg yolk but also reduction of cholesterol content to approximately 0.5% or less. In addition, since the supercritically treated dried egg yolk is granulated without using a binder having a binding property, it is easy to spray the dried egg yolk with a particle size of 10 which is within the range of the particle size distribution of the dried egg yolk. Return to ~ 100 μm fine powder. Here, the range of the particle size distribution being 10 to 100 μm means that most of fine powder (95% or more) is 10 to 1
It means that the particle size is 00 μm. Since this fine powder has a large surface area, it can be dissolved even in a low-concentration saline solution.

【0011】[0011]

【作用】本発明においては、スプレードライして得られ
た乾燥卵黄を清水のバインダーを用いて押出し造粒をす
るので、これによって得られる顆粒は物理的な圧力によ
り点で卵黄微粒子が結合している状態であるため多孔性
を有する。その結果、微粒子に由来する表面積の大きさ
と、顆粒による多孔性の両面を備えており、超臨界状態
の二酸化炭素の浸透性が高く、しかも偏流や目詰まりが
生じないためコレステロールを効率的に抽出することが
できる。また、卵黄に過剰な加熱がされておらず、しか
も超臨界処理後には物理的圧力による顆粒が容易に崩
れ、造粒前の粒径の分布10〜100μmの微粉末に戻
るため、この粉末は表面積が大きく多孔性であるから低
濃度食塩水への溶解力も向上することになる。
In the present invention, the dried egg yolk obtained by spray-drying is extruded and granulated by using a binder of fresh water. Since it is in a state where it has porosity. As a result, it has both surface area derived from fine particles and porosity due to granules, high permeability of carbon dioxide in the supercritical state, and efficient extraction of cholesterol because drift and clogging do not occur. can do. Further, the egg yolk is not excessively heated, and further, after the supercritical treatment, the granules due to physical pressure are easily collapsed to return to a fine powder having a particle size distribution of 10 to 100 μm before granulation. Since it has a large surface area and is porous, the ability to dissolve in low-concentration saline is also improved.

【0012】以下、実施例と試験例を述べる。Examples and test examples will be described below.

【実施例】実施例1 鶏卵を割卵して得た卵黄をスプレードライして乾燥卵黄
(水分3.5%:粒径の分布10〜100μm)を製造
した。この乾燥卵黄をホバートミキサーに入れ、攪拌し
ながらバインダーとして清水を噴霧状に添加してその水
分が18%になるまで加水した。その後、これを押出し
造粒装置(畑鉄工社製、バケット式:スクリーン径2.
0mm)を用いて造粒した後、流動層乾燥機にて水分
2.5%に乾燥して、顆粒卵黄を得た。この顆粒卵黄3
00gをテストプラントにて40℃、25MPaの条件
下で超臨界二酸化炭素30Kgと接触させたところ、粒径
の分布10〜100μmの微粉末からなる加工乾燥卵黄
174gが得られた。この加工乾燥卵黄は、コレステロ
ール含量0.2%であった。
[Examples] Example 1 Egg yolk obtained by breaking chicken eggs was spray-dried to produce dried egg yolk (water content 3.5%: particle size distribution 10 to 100 µm). This dried egg yolk was put in a Hobart mixer, and while stirring, fresh water was added in a spray form as a binder to add water until the water content became 18%. Then, this was extruded and granulated (manufactured by Hata Tekko KK, bucket type: screen diameter 2.
(0 mm) and then dried in a fluidized bed dryer to a water content of 2.5% to obtain granular egg yolk. This granule yolk 3
When 00 g was brought into contact with 30 kg of supercritical carbon dioxide at 40 ° C. and 25 MPa in a test plant, 174 g of processed dried egg yolk consisting of fine powder having a particle size distribution of 10 to 100 μm was obtained. This processed dried egg yolk had a cholesterol content of 0.2%.

【0013】[0013]

【試験例】試験例1 次の4種のサンプルを用意した。 対照区1(特表平7−507930の製法によるもの) 鶏卵を割卵して得た卵黄をドラムドライして乾燥卵黄
(水分3.5%)を製し、この乾燥卵黄を実施例1と同
じ条件で超臨界二酸化炭素処理して得られた加工乾燥卵
黄 対照区2(特公昭62−51092の製法によるもの) 鶏卵を割卵して得た卵黄をスプレードライして乾燥卵黄
(水分3.5%)を製し、この乾燥卵黄を実施例1と同
じ条件で超臨界ニ酸化炭素処理して得られた加工乾燥卵
黄 対照区3 乾燥卵黄にバインダーとして1%澱粉溶液を噴霧状に添
加した他は、すべて実施例1と同じ条件で処理して得ら
れた加工乾燥卵黄 テスト区 実施例1によって得られた加工乾燥卵黄 上記各サンプルについてコレステロール含量と微粉末の
粒径の分布を測定すると共に、食塩水に対する溶解性を
観察したところ表1の結果が得られた。
[Test Example] Test Example 1 The following four types of samples were prepared. Control area 1 (by the production method of Tokuhyo Hyodai 7-507930) The egg yolk obtained by splitting chicken eggs was drum-dried to produce dried egg yolk (water content 3.5%), and this dried egg yolk was used as Example 1. Controlled dried egg yolk control group 2 obtained by supercritical carbon dioxide treatment under the same conditions (by the method of Japanese Patent Publication No. 62-51092) Egg yolk obtained by splitting chicken eggs was spray-dried to dry egg yolk (water content 3. 5%) was prepared, and the dried egg yolk was treated with supercritical carbon dioxide under the same conditions as in Example 1 to obtain a processed dried egg yolk control group 3. A 1% starch solution was added as a binder to the dried egg yolk in a spray form. Other than that, processed dried egg yolk test section obtained by treating under the same conditions as in Example 1 processed dried egg yolk obtained in Example 1 The cholesterol content and the particle size distribution of fine powder were measured for each sample. , Soluble in saline The results in Table 1 was observed sex were obtained.

【0014】[0014]

【表1】 [Table 1]

【0015】表1より、本発明によれば、コレステロー
ル含量が低く、しかも低濃度の食塩水に溶解性のよい加
工乾燥卵黄が得られることが理解できる。
From Table 1, it can be understood that according to the present invention, a processed dried egg yolk having a low cholesterol content and good solubility in a saline solution having a low concentration can be obtained.

【0016】試験例2 鶏卵を割卵して得た卵黄をスプレードライして乾燥卵黄
(水分3.2%)を製した。この乾燥卵黄をホバートミ
キサーに入れ、攪拌しながらバインダーとして清水を注
加してその水分が18%となるまで加水した。次に、こ
の加水した乾燥卵黄を押出し造粒装置(実施例1で用い
たものと同じ)にて造粒するに当り、表2に示すように
スクリーン径をかえて他の操作は実施例と同様にして、
5種類の顆粒卵黄(サンプル)を製した。次に、各サン
プルについてそれぞれ300gをテストプラントにて4
0℃、25MPaの条件下で超臨界ニ酸化炭素30Kgと
接触させて、5種類の加工乾燥卵黄を得た。得られた各
乾燥卵黄についてコレステロール含量を測定したとこ
ろ、表2の結果が得られた。
Test Example 2 Egg yolk obtained by splitting chicken eggs was spray-dried to produce dried egg yolk (water content 3.2%). The dried egg yolk was placed in a Hobart mixer, and while stirring, fresh water was added as a binder to add water until the water content became 18%. Next, when granulating the hydrated dried egg yolk with an extrusion granulator (the same as that used in Example 1), the screen diameter was changed as shown in Table 2 and other operations were the same as those in Example. Similarly,
Five types of granular egg yolks (samples) were produced. Next, for each sample, 300 g of
It was brought into contact with 30 kg of supercritical carbon dioxide under the conditions of 0 ° C. and 25 MPa to obtain 5 types of processed dried egg yolk. When the cholesterol content of each of the obtained dried egg yolks was measured, the results shown in Table 2 were obtained.

【0017】[0017]

【表2】 [Table 2]

【0018】表2より、押出し造粒に当って1.5〜
3.0mmのスクリーンを用いて造粒し、これを超臨界
二酸化炭素処理すれば、コレステロール含量が低い加工
乾燥卵黄が得られることが理解できる。
From Table 2, it can be seen that the extrusion granulation is 1.5 to
It can be understood that a granulated processed egg yolk with a low cholesterol content can be obtained by granulating using a 3.0 mm screen and subjecting it to supercritical carbon dioxide treatment.

【0019】[0019]

【発明の効果】以上述べたように、本発明によれば、脱
コレステロール率が高く、低濃度の食塩水にも溶解する
加工卵黄を製造することができ、この加工卵黄は健康食
品や加工食品等の原料として好適である。
As described above, according to the present invention, it is possible to produce a processed egg yolk which has a high decholesterolization rate and can be dissolved in a salt solution having a low concentration. The processed egg yolk is a health food or a processed food. It is suitable as a raw material.

Claims (2)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 スプレードライして得られる乾燥卵黄を
清水のバインダーを用いて押出し造粒して多孔性の顆粒
とした後、これを超臨界二酸化炭素で脱コレステロール
処理し、粒径の分布10〜100μmの微粒子にするこ
とを特徴とする加工乾燥卵黄の製法。
1. Porous granules obtained by extrusion-drying dried egg yolk obtained by spray drying with a binder of fresh water.
And then decholesterolizing it with supercritical carbon dioxide to obtain fine particles having a particle size distribution of 10 to 100 μm.
【請求項2】 スクリーン径が1.5〜3.0mmの造
粒機で押出し造粒することを特徴とする請求項1記載の
加工乾燥卵黄の製法。
2. The method for producing a processed dried egg yolk according to claim 1, which comprises extruding and granulating with a granulator having a screen diameter of 1.5 to 3.0 mm.
JP2000163465A 2000-05-31 2000-05-31 Processed dried egg yolk Expired - Lifetime JP3459617B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2000163465A JP3459617B2 (en) 2000-05-31 2000-05-31 Processed dried egg yolk

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2000163465A JP3459617B2 (en) 2000-05-31 2000-05-31 Processed dried egg yolk

Publications (2)

Publication Number Publication Date
JP2001340064A JP2001340064A (en) 2001-12-11
JP3459617B2 true JP3459617B2 (en) 2003-10-20

Family

ID=18667213

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000163465A Expired - Lifetime JP3459617B2 (en) 2000-05-31 2000-05-31 Processed dried egg yolk

Country Status (1)

Country Link
JP (1) JP3459617B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009131218A (en) * 2007-11-30 2009-06-18 Q P Corp Processed dried yolk and method for producing the same

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100532678B1 (en) * 2003-06-30 2005-11-30 그린텍이십일 주식회사 IgY titre improved egg yolk powder and process for preparation thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009131218A (en) * 2007-11-30 2009-06-18 Q P Corp Processed dried yolk and method for producing the same

Also Published As

Publication number Publication date
JP2001340064A (en) 2001-12-11

Similar Documents

Publication Publication Date Title
JP3188657B2 (en) Tablet or granular product
CA1311961C (en) Agglomerates of potato granules
JPS5886046A (en) Premix for animal feed
JP3459617B2 (en) Processed dried egg yolk
FI59527B (en) FOERFARANDE FOER FRAMSTAELLNING AV EN TORR AGGLOMERERAD HOMOGENT BLANDAD PRODUKT ANVAENDBAR I EN SNABBMATPRODUKT
JP3378383B2 (en) Production methods for brewing raw materials
JPH1056969A (en) Soybean protein/cocoa granule and its production
JP2003047442A (en) Reprocessing of nemacystus decipiens dried by freeze-dry method through product after grinding and granulation or drying into food and health food and nemacystus decipiens of original alga by reconstitution with water
KR101861151B1 (en) Producing method of egg-bean curd having rich amino acid content and egg-bean curd produced thereby
JP2999220B2 (en) Production method of powdered sake lees
JPH0195739A (en) Production of readily soluble granular stevia sweetener
JPS60184378A (en) Production of granular food
JPS5951568B2 (en) Method for producing easily water-soluble polyacrylic acid metal salt granules
JPS5959173A (en) Preparation of granule or cube of sweetener
JP3110697B2 (en) Recycled powder of coffee extract cake and its use as an auxiliary ingredient for processed foods and as a raw material for activated carbon
JPH0783683B2 (en) Meat-like protein food with improved taste
JP3231276B2 (en) Chitosan composition and method for producing the same
US2192326A (en) Pharmaceutical
JPS5853891B2 (en) How to make knots
JP4739311B2 (en) Processed dried egg yolk and method for producing the same
JPS6219808B2 (en)
JPH0597687A (en) Method for producing dried yeast granule
JP2004105066A (en) Powdered soy sauce
JP2972356B2 (en) Production method of film feed
JPS6167465A (en) Production of pill of sea tangle

Legal Events

Date Code Title Description
TRDD Decision of grant or rejection written
R150 Certificate of patent or registration of utility model

Ref document number: 3459617

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090808

Year of fee payment: 6

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20120808

Year of fee payment: 9

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20180808

Year of fee payment: 15

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term