JP2020512256A - スルホアルミン酸カルシウムベースの無機発泡体 - Google Patents
スルホアルミン酸カルシウムベースの無機発泡体 Download PDFInfo
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- JP2020512256A JP2020512256A JP2019548392A JP2019548392A JP2020512256A JP 2020512256 A JP2020512256 A JP 2020512256A JP 2019548392 A JP2019548392 A JP 2019548392A JP 2019548392 A JP2019548392 A JP 2019548392A JP 2020512256 A JP2020512256 A JP 2020512256A
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- Prior art keywords
- inorganic
- group
- foam
- mixture
- particles
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- 239000006260 foam Substances 0.000 title claims abstract description 165
- 239000011575 calcium Substances 0.000 title claims abstract description 42
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 41
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 239000000203 mixture Substances 0.000 claims abstract description 123
- 238000002360 preparation method Methods 0.000 claims abstract description 32
- 239000000463 material Substances 0.000 claims abstract description 29
- 230000001413 cellular effect Effects 0.000 claims abstract description 20
- 238000001035 drying Methods 0.000 claims abstract description 9
- 239000011230 binding agent Substances 0.000 claims description 106
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 44
- 239000010954 inorganic particle Substances 0.000 claims description 43
- 239000002245 particle Substances 0.000 claims description 40
- 238000000034 method Methods 0.000 claims description 36
- 150000001875 compounds Chemical class 0.000 claims description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 32
- 238000005187 foaming Methods 0.000 claims description 31
- 239000004568 cement Substances 0.000 claims description 29
- 239000010881 fly ash Substances 0.000 claims description 26
- 235000019353 potassium silicate Nutrition 0.000 claims description 21
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 20
- 239000002893 slag Substances 0.000 claims description 20
- 239000000654 additive Substances 0.000 claims description 18
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 18
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 17
- 239000003054 catalyst Substances 0.000 claims description 17
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 15
- 230000000996 additive effect Effects 0.000 claims description 15
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 13
- 239000000835 fiber Substances 0.000 claims description 13
- 239000000126 substance Substances 0.000 claims description 11
- 239000004094 surface-active agent Substances 0.000 claims description 11
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 10
- 229910019142 PO4 Inorganic materials 0.000 claims description 9
- 239000000945 filler Substances 0.000 claims description 9
- 235000021317 phosphate Nutrition 0.000 claims description 9
- 150000001412 amines Chemical class 0.000 claims description 8
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 8
- 235000010216 calcium carbonate Nutrition 0.000 claims description 8
- 229910021487 silica fume Inorganic materials 0.000 claims description 8
- 125000004432 carbon atom Chemical group C* 0.000 claims description 7
- RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 claims description 6
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 5
- XFWJKVMFIVXPKK-UHFFFAOYSA-N calcium;oxido(oxo)alumane Chemical compound [Ca+2].[O-][Al]=O.[O-][Al]=O XFWJKVMFIVXPKK-UHFFFAOYSA-N 0.000 claims description 5
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 4
- 125000001931 aliphatic group Chemical group 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 4
- 239000006185 dispersion Substances 0.000 claims description 4
- 239000010440 gypsum Substances 0.000 claims description 4
- 229910052602 gypsum Inorganic materials 0.000 claims description 4
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 4
- 150000004760 silicates Chemical class 0.000 claims description 4
- 125000001424 substituent group Chemical group 0.000 claims description 4
- 125000003118 aryl group Chemical group 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 3
- 125000004122 cyclic group Chemical group 0.000 claims description 3
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 claims description 3
- 150000004679 hydroxides Chemical class 0.000 claims description 3
- 239000011810 insulating material Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 150000004767 nitrides Chemical class 0.000 claims description 3
- 239000010452 phosphate Substances 0.000 claims description 3
- 239000006254 rheological additive Substances 0.000 claims description 3
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 3
- 239000011358 absorbing material Substances 0.000 claims description 2
- 150000001408 amides Chemical class 0.000 claims description 2
- 229910052925 anhydrite Inorganic materials 0.000 claims description 2
- 239000004566 building material Substances 0.000 claims description 2
- 150000001735 carboxylic acids Chemical class 0.000 claims description 2
- 150000001247 metal acetylides Chemical class 0.000 claims description 2
- 239000003002 pH adjusting agent Substances 0.000 claims description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 2
- UEZVMMHDMIWARA-UHFFFAOYSA-M phosphonate Chemical compound [O-]P(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-M 0.000 claims description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 2
- 239000008030 superplasticizer Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 12
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 33
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 28
- 229920000876 geopolymer Polymers 0.000 description 26
- -1 CaCO 3 Chemical class 0.000 description 22
- 210000004027 cell Anatomy 0.000 description 19
- 239000000843 powder Substances 0.000 description 17
- 239000000292 calcium oxide Substances 0.000 description 15
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 12
- 239000000377 silicon dioxide Substances 0.000 description 12
- 239000007789 gas Substances 0.000 description 11
- 238000009826 distribution Methods 0.000 description 10
- 239000012071 phase Substances 0.000 description 10
- 239000002994 raw material Substances 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 238000002296 dynamic light scattering Methods 0.000 description 9
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 9
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- 239000011398 Portland cement Substances 0.000 description 7
- 239000012190 activator Substances 0.000 description 7
- 239000003513 alkali Substances 0.000 description 7
- 239000000395 magnesium oxide Substances 0.000 description 7
- 235000012239 silicon dioxide Nutrition 0.000 description 7
- 239000002002 slurry Substances 0.000 description 7
- 239000000725 suspension Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000011572 manganese Substances 0.000 description 6
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 239000005995 Aluminium silicate Substances 0.000 description 5
- 239000004604 Blowing Agent Substances 0.000 description 5
- 235000012211 aluminium silicate Nutrition 0.000 description 5
- 239000004088 foaming agent Substances 0.000 description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 description 5
- 239000011707 mineral Substances 0.000 description 5
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 5
- 229920002239 polyacrylonitrile Polymers 0.000 description 5
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Chemical compound [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 5
- 239000002202 Polyethylene glycol Substances 0.000 description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 239000012298 atmosphere Substances 0.000 description 4
- 150000007942 carboxylates Chemical group 0.000 description 4
- 239000002734 clay mineral Substances 0.000 description 4
- 229910021485 fumed silica Inorganic materials 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 4
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 4
- 229920001223 polyethylene glycol Polymers 0.000 description 4
- 239000000473 propyl gallate Substances 0.000 description 4
- 229940075579 propyl gallate Drugs 0.000 description 4
- 235000010388 propyl gallate Nutrition 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 150000003335 secondary amines Chemical class 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 238000003723 Smelting Methods 0.000 description 3
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 3
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- 125000000129 anionic group Chemical group 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 125000002843 carboxylic acid group Chemical group 0.000 description 3
- 239000003093 cationic surfactant Substances 0.000 description 3
- 239000001913 cellulose Substances 0.000 description 3
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- 235000010980 cellulose Nutrition 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical class O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 3
- 229910010272 inorganic material Inorganic materials 0.000 description 3
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- 239000001301 oxygen Substances 0.000 description 3
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 3
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- 229910021653 sulphate ion Inorganic materials 0.000 description 3
- YFSUTJLHUFNCNZ-UHFFFAOYSA-M 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonate Chemical compound [O-]S(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F YFSUTJLHUFNCNZ-UHFFFAOYSA-M 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 2
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 description 2
- ICGLPKIVTVWCFT-UHFFFAOYSA-N 4-methylbenzenesulfonohydrazide Chemical compound CC1=CC=C(S(=O)(=O)NN)C=C1 ICGLPKIVTVWCFT-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 2
- 230000005653 Brownian motion process Effects 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
- 102000016938 Catalase Human genes 0.000 description 2
- 108010053835 Catalase Proteins 0.000 description 2
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- WJYIASZWHGOTOU-UHFFFAOYSA-N Heptylamine Chemical compound CCCCCCCN WJYIASZWHGOTOU-UHFFFAOYSA-N 0.000 description 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
- 239000005909 Kieselgur Substances 0.000 description 2
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- 235000019738 Limestone Nutrition 0.000 description 2
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- 229910000831 Steel Inorganic materials 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 150000001340 alkali metals Chemical group 0.000 description 2
- 150000005215 alkyl ethers Chemical class 0.000 description 2
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 2
- 229910021486 amorphous silicon dioxide Inorganic materials 0.000 description 2
- 239000003945 anionic surfactant Substances 0.000 description 2
- RHZUVFJBSILHOK-UHFFFAOYSA-N anthracen-1-ylmethanolate Chemical compound C1=CC=C2C=C3C(C[O-])=CC=CC3=CC2=C1 RHZUVFJBSILHOK-UHFFFAOYSA-N 0.000 description 2
- 239000003830 anthracite Substances 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 239000002585 base Substances 0.000 description 2
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- 229960000686 benzalkonium chloride Drugs 0.000 description 2
- 229960001950 benzethonium chloride Drugs 0.000 description 2
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 description 2
- CADWTSSKOVRVJC-UHFFFAOYSA-N benzyl(dimethyl)azanium;chloride Chemical compound [Cl-].C[NH+](C)CC1=CC=CC=C1 CADWTSSKOVRVJC-UHFFFAOYSA-N 0.000 description 2
- KQNZLOUWXSAZGD-UHFFFAOYSA-N benzylperoxymethylbenzene Chemical compound C=1C=CC=CC=1COOCC1=CC=CC=C1 KQNZLOUWXSAZGD-UHFFFAOYSA-N 0.000 description 2
- 238000005537 brownian motion Methods 0.000 description 2
- XOPOEBVTQYAOSV-UHFFFAOYSA-N butyl 3,4,5-trihydroxybenzoate Chemical group CCCCOC(=O)C1=CC(O)=C(O)C(O)=C1 XOPOEBVTQYAOSV-UHFFFAOYSA-N 0.000 description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 2
- 239000001506 calcium phosphate Substances 0.000 description 2
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- 125000002091 cationic group Chemical group 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 229960000541 cetyl alcohol Drugs 0.000 description 2
- 229960001927 cetylpyridinium chloride Drugs 0.000 description 2
- NFCRBQADEGXVDL-UHFFFAOYSA-M cetylpyridinium chloride monohydrate Chemical compound O.[Cl-].CCCCCCCCCCCCCCCC[N+]1=CC=CC=C1 NFCRBQADEGXVDL-UHFFFAOYSA-M 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 239000002666 chemical blowing agent Substances 0.000 description 2
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- 230000000052 comparative effect Effects 0.000 description 2
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- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N coumarin Chemical compound C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 description 2
- PSLWZOIUBRXAQW-UHFFFAOYSA-M dimethyl(dioctadecyl)azanium;bromide Chemical compound [Br-].CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC PSLWZOIUBRXAQW-UHFFFAOYSA-M 0.000 description 2
- 150000002170 ethers Chemical class 0.000 description 2
- 239000003063 flame retardant Substances 0.000 description 2
- 239000005338 frosted glass Substances 0.000 description 2
- 229930182478 glucoside Natural products 0.000 description 2
- MNWFXJYAOYHMED-UHFFFAOYSA-N heptanoic acid Chemical compound CCCCCCC(O)=O MNWFXJYAOYHMED-UHFFFAOYSA-N 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 150000002432 hydroperoxides Chemical class 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 150000002484 inorganic compounds Chemical class 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 125000003010 ionic group Chemical group 0.000 description 2
- 239000003077 lignite Substances 0.000 description 2
- 239000006028 limestone Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 2
- 229910003455 mixed metal oxide Inorganic materials 0.000 description 2
- 239000003607 modifier Substances 0.000 description 2
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 2
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- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 description 1
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Images
Classifications
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- C—CHEMISTRY; METALLURGY
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- C04B38/02—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by adding chemical blowing agents
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- C04B12/00—Cements not provided for in groups C04B7/00 - C04B11/00
- C04B12/04—Alkali metal or ammonium silicate cements ; Alkyl silicate cements; Silica sol cements; Soluble silicate cements
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- C04B22/068—Peroxides, e.g. hydrogen peroxide
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- C04B22/142—Sulfates
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- C04B28/06—Aluminous cements
- C04B28/065—Calcium aluminosulfate cements, e.g. cements hydrating into ettringite
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Abstract
Description
(1) 以下のもの:
(i) 少なくとも1つの群の無機粒子;
(ii) 少なくとも1種の両親媒性化合物;
(iii) 以下のもの:
(iiia) 少なくとも1種のスルホアルミン酸カルシウム混合物と、任意で
(iiib) 水硬性バインダー、潜在水硬性バインダー、ポゾランバインダーおよびこれらの混合物から成る群より選択される少なくとも1種のさらなる無機バインダーと
を含む少なくとも1種の無機バインダー混合物;
(iv) 水;および任意で
(v) 少なくとも1種の添加剤;
を混合する工程、ならびに
(2) 得られた発泡体調製物を化学的、物理的または機械的な発泡により発泡させる工程
を含む、無機発泡体を製造する方法に関する。
(i) 少なくとも1つの群の無機粒子;
(ii) 少なくとも1種の両親媒性化合物;
(iii) 以下のもの:
(iiia) 少なくとも1種のスルホアルミン酸カルシウム混合物と、任意で
(iiib) 水硬性バインダー、潜在水硬性バインダー、ポゾランバインダーおよびこれらの混合物から成る群より選択される少なくとも1種のさらなる無機バインダーと
を含む少なくとも1種の無機バインダー混合物;
(iv) 水;および任意で
(v) 少なくとも1種の添加剤
を含む無機発泡体に関する。
(i) 少なくとも1つの群の無機粒子;
(ii) 少なくとも1種の両親媒性化合物;
(iii) 以下のもの:
(iiia) 少なくとも1種のスルホアルミン酸カルシウム混合物と、任意で
(iiib) 水硬性バインダー、潜在水硬性バインダー、ポゾランバインダーおよびこれらの混合物から成る群より選択される少なくとも1種のさらなる無機バインダーと
を含む少なくとも1種の無機バインダー混合物
を成分として含み、ここで
成分(i)、(ii)および(iii)が個別に存在するか、または
成分(i)および(ii)が混合物として存在し、成分(iii)が個別に存在するか、または
成分(i)、(ii)および(iii)が混合物として存在する、
無機発泡体調製物を製造するための組成物に関する。
・ 純粋および混合金属酸化物を含む酸化物(特に、酸化アルミニウム、二酸化ケイ素、スピネル、セリウム−ガドリニウム酸化物、酸化ジルコニウム、酸化マグネシウム、酸化スズ、酸化チタンおよび酸化セリウム);
・ 水酸化物(特に、水酸化アルミニウム、水酸化カルシウム、水酸化マグネシウム、非常に具体的には水酸化アルミニウム);
・ 炭化物(特に、炭化ケイ素、炭化ホウ素);
・ 窒化物(特に、窒化ケイ素、窒化ホウ素);
・ リン酸塩(特に、リン酸カルシウム、例えば、リン酸三カルシウム、ヒドロキシアパタイト);
・ 炭酸塩(特に、炭酸ニッケル、炭酸カルシウム(破砕石灰石または沈降炭酸カルシウム)、炭酸マグネシウム);
・ ケイ酸塩(特に、二酸化ケイ素、シリカフューム、フライアッシュ、石英、すりガラス、スラグ、ケイ酸カルシウム、ムライト、コーディエライト、粘土鉱物、例えばカオリンまたはベントナイト、ケイ酸ジルコニウム、ゼオライト、珪藻土、非常に具体的には、シリカフューム、粘土鉱物、ケイ酸ジルコニウム;具体的には、粘土鉱物);
・ 硫酸塩(特に硫酸カルシウム)。
ここで、少なくとも1つの頭部基が、ホスフェート、ホスホネート、スルフェート、スルホネート、アルコール、アミン、アミド、ピロリジン、ガレートおよびカルボン酸から成る群より選択され、
かつここで、少なくとも1つの尾部基が、2〜8個の炭素原子を有する脂肪族基または芳香族基または環式基より選択され、ここで炭素原子が、C1〜C8アルキル、第二級OHおよび第二級NH2より選択される1つ以上の同じまたは異なる置換基で任意に置換されている。
a) イーリマイト(ye’elimite)(4CaO×3Al2O3×SO3)および任意でベライト(belite)(2CaO×SiO2)、ならびに
b) 硬石膏(CaSO4)および/または硫酸カルシウム半水和物(CaSO4×0.5H2O)および/または石膏(CaSO4×2H2O)、
を、90:10〜60:40、好ましくは80:20〜65:35のa):b)の重量比で含有していてもよい。
5〜35重量%のSO3
30〜60重量%のCaO
0〜30重量%のSiO2
5〜35重量%のAl2O3
好ましくは
10〜30重量%のSO3
30〜50重量%のCaO
0〜20重量%のSiO2
15〜35重量%のAl2O3
より好ましくは
17〜27重量%のSO3
37〜47重量%のCaO
5〜15重量%のSiO2
20〜30重量%のAl2O3
の一般的な分析酸化物組成を有する。
(iiia) 少なくとも1種のスルホアルミン酸カルシウム混合物、ならびに
(iiib) 水硬性バインダー、潜在水硬性バインダー、ポゾランバインダーおよびこれらの混合物から成る群より選択される少なくとも1種のさらなる無機バインダー
を含む場合、成分(iiib)および(iiia)は、0.1〜3.4、好ましくは0.1〜2.0、より好ましくは0.3〜1.5の相対重量比で存在していてもよい。
(1a) 少なくとも1つの群の無機粒子、少なくとも1種の両親媒性化合物、および任意で少なくとも1種の添加剤を水に分散させて、水性分散液を得る工程、ならびに
(1b) 水性分散液を少なくとも1種の無機バインダー混合物と混合する工程
を含む。
比較例1
ジオポリマー発泡体を、以下の組成の原材料から製造した:
20.5重量%のメタカオリン(Argical(商標)M1200S、Imerys)
20.5重量%のフライアッシュ(Microsit(登録商標)M10、BauMineral)
7.8重量%のアルミン酸カルシウムセメント(Ciment Fondu(登録商標)、Kerneos)
1.2重量%の界面活性剤(アルキルポリグルコシド、Glucopon(登録商標)225DK、BASF)
0.2重量%のPAN繊維(6mm、6.7dtex)
19.5重量%の水
27.4重量%の水ガラス(’’Kaliwasserglass K58’’、BASF)
2.9重量%のNaOH。
79.8重量%の炭酸カルシウム(Socal31)、15.1重量%のブチルガレートおよび5.1重量%の酸化マンガン(IV)を含む混合物を「発泡体形成用粉末」として予め混合した。
19.2重量%のメタカオリン(Argical(商標)M1200S、Imerys)
19.2重量%のフライアッシュ(Microsit(登録商標)M10、BauMineral)
7.3重量%のアルミン酸カルシウムセメント(Ciment Fondu(登録商標)、Kerneos)
2.3重量%の発泡体形成用粉末
0.2重量%のPAN繊維(6mm、6.7dtex)
23.4重量%の水
26.3重量%の水ガラス(’’Kaliwasserglass K58’’、BASF)
2.8重量%の過酸化水素(50%溶液)。
88.5重量%の炭酸カルシウム(Schaefer Precarb100)、5.8重量%のエナント酸および5.7重量%の酸化マンガン(IV)を含む混合物を「発泡体形成用粉末」として予め混合した。
39.4重量%のスルホアルミン酸カルシウム(Alipre(登録商標)、Italcementi)
12.2重量%の硫酸カルシウム二水和物
6.5重量%の発泡体形成用粉末
0.3重量%のPAN繊維(6mm、6.7dtex)
38.7重量%の水
2.9重量%の過酸化水素(50%溶液)。
83.7重量%の炭酸カルシウム(Schaefer Precarb100)、5.5重量%のエナント酸および10.8重量%の酸化マンガン(IV)を含む混合物を「発泡体形成用粉末」として予め混合した。
18.7重量%のスルホアルミン酸カルシウム(Alipre(登録商標)、Italcementi)
5.8重量%の硫酸カルシウム二水和物
12.2重量%のメタカオリン(Argical(商標)M1200S、Imerys)
12.2重量%のフライアッシュ(Microsit(登録商標)M10、BauMineral)
3.7重量%の発泡体形成用粉末
0.2重量%のPAN繊維(6mm、6.7dtex)
43.9重量%の水
3.2重量%の過酸化水素(50%溶液)。
Claims (19)
- (1) 以下のもの:
(i) 少なくとも1つの群の無機粒子;
(ii) 少なくとも1種の両親媒性化合物;
(iii) 以下のもの:
(iiia) 少なくとも1種のスルホアルミン酸カルシウム混合物と、任意で
(iiib) 水硬性バインダー、潜在水硬性バインダー、ポゾランバインダーおよびこれらの混合物から成る群より選択される少なくとも1種のさらなる無機バインダーと
を含む少なくとも1種の無機バインダー混合物;
(iv) 水;および任意で
(v) 少なくとも1種の添加剤;
を混合する工程、ならびに
(2) 得られた発泡体調製物を化学的、物理的または機械的な発泡により発泡させる工程
を含む、無機発泡体を製造する方法。 - 前記少なくとも1つの群の無機粒子が、酸化物、水酸化物、炭化物、窒化物、リン酸塩、炭酸塩、ケイ酸塩、硫酸塩およびこれらの混合物から成る群より選択される、請求項1記載の方法。
- 前記少なくとも1つの群の無機粒子が、シリカ粒子、アルミナ粒子、ジルコニア粒子およびCaCO3粒子、ならびにこれらの混合物から成る群より選択される、請求項1または2記載の方法。
- 前記少なくとも1つの群の無機粒子が、30nm〜300μmの範囲にある中央粒径D50を有する、請求項1から3までのいずれか1項記載の方法。
- 前記少なくとも1種の両親媒性化合物が、少なくとも1つの極性頭部基と少なくとも1つの非極性尾部基とを有する両親媒性化合物を含み、
ここで、前記少なくとも1つの頭部基が、ホスフェート、ホスホネート、スルフェート、スルホネート、アルコール、アミン、アミド、ピロリジン、ガレートおよびカルボン酸から成る群より選択され、
かつここで、前記少なくとも1つの尾部基が、2〜8個の炭素原子を有する脂肪族基または芳香族基または環式基より選択され、ここで前記炭素原子が、C1〜C8アルキル、第二級OHおよび第二級NH2より選択される1つ以上の同じまたは異なる置換基で任意に置換されている、
請求項1から4までのいずれか1項記載の方法。 - 前記少なくとも1種の両親媒性化合物が、カルボン酸、ガレートおよびアミンから成る群より選択される少なくとも1つの頭部基と、2〜8個の炭素原子を有する脂肪族基より選択される少なくとも1つの尾部基とを有する両親媒性化合物を含む、請求項1から5までのいずれか1項記載の方法。
- 前記少なくとも1種のスルホアルミン酸カルシウム混合物が、5〜35重量%のSO3、30〜60重量%のCaO、0〜30重量%のSiO2および5〜35重量%のAl2O3の分析酸化物組成を有する、請求項1から6までのいずれか1項記載の方法。
- 前記少なくとも1種のスルホアルミン酸カルシウム混合物が、a)イーリマイト(4CaO×3Al2O3×SO3)および任意でベライト(2CaO×SiO2)、ならびにb)硬石膏(CaSO4)、硫酸カルシウム半水和物(CaSO4×0.5H2O)および/または石膏(CaSO4×2H2O)を、90:10〜60:40のa):b)の重量比で含有する、請求項1から7までのいずれか1項記載の方法。
- 前記少なくとも1種のさらなる無機バインダーが、高炉スラグ、マイクロシリカ、メタカオリン、アルミノシリケート、フライアッシュおよびこれらの混合物から成る群より選択される、請求項1から8までのいずれか1項記載の方法。
- 前記少なくとも1種のさらなる無機バインダーが、メタカオリンとフライアッシュとの混合物である、請求項1から9までのいずれか1項記載の方法。
- 前記少なくとも1種の無機バインダー混合物(iii)が、
(iiic) DIN EN197−1(11/2011)に準拠したCEM I、CEM II、CEM III、CEM IV、CEM Vセメント、またはアルミン酸カルシウムセメントより選択される少なくとも1種のセメント、好ましくはCEM Iセメント
を含む、請求項1から10までのいずれか1項記載の方法。 - 前記少なくとも1種の添加剤が、pH改質剤、フィラー、促進剤、遅延剤、レオロジー調整剤、超可塑剤、界面活性剤、繊維、水ガラス、さらなる疎水化剤、触媒およびこれらの混合物から成る群より選択される、請求項1から11までのいずれか1項記載の方法。
- 無機粒子表面に対する両親媒性化合物の量が、0.5〜160μmol/m2であり;かつ/または
前記無機粒子が、前記少なくとも1種の無機バインダー混合物の量に対して0.1〜25重量%の量で用意され;かつ/または
前記無機バインダー混合物に対する水の重量比が0.1〜2.0である、
請求項1から12までのいずれか1項記載の方法。 - 工程(1)が、
(1a) 前記少なくとも1つの群の無機粒子、前記少なくとも1種の両親媒性化合物、および任意で前記少なくとも1種の添加剤を水に分散させて、水性分散液を得る工程、ならびに
(1b) 前記水性分散液を前記少なくとも1種の無機バインダー混合物と混合する工程
を含む、請求項1から13までのいずれか1項記載の方法。 - 請求項1から14までのいずれか1項記載の方法により得られる無機発泡体。
- (i) 少なくとも1つの群の無機粒子;
(ii) 少なくとも1種の両親媒性化合物;
(iii) 以下のもの:
(iiia) 少なくとも1種のスルホアルミン酸カルシウム混合物と、任意で
(iiib) 水硬性バインダー、潜在水硬性バインダー、ポゾランバインダーおよびこれらの混合物から成る群より選択される少なくとも1種のさらなる無機バインダーと
を含む少なくとも1種の無機バインダー混合物;
(iv) 水;および任意で
(v) 少なくとも1種の添加剤
を含む無機発泡体。 - 請求項15または16記載の無機発泡体を硬化および任意で乾燥させることにより得られる気泡材料。
- (i) 少なくとも1つの群の無機粒子;
(ii) 少なくとも1種の両親媒性化合物;
(iii) 以下のもの:
(iiia) 少なくとも1種のスルホアルミン酸カルシウム混合物と、任意で
(iiib) 水硬性バインダー、潜在水硬性バインダー、ポゾランバインダーおよびこれらの混合物から成る群より選択される少なくとも1種のさらなる無機バインダーと
を含む少なくとも1種の無機バインダー混合物
を成分として含み、ここで
前記成分(i)、(ii)および(iii)が個別に存在するか、または
前記成分(i)および(ii)が混合物として存在し、成分(iii)が個別に存在するか、または
前記成分(i)、(ii)および(iii)が混合物として存在する、
無機発泡体調製物を製造するための組成物。 - 断熱材、防音材または吸音材としての、防火のための、および/または低密度の建材としての、請求項15または16記載の無機発泡体、請求項17記載の気泡材料、および/または請求項18記載の組成物の使用。
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EP17159443.5 | 2017-03-06 | ||
EP17159443 | 2017-03-06 | ||
PCT/EP2018/055292 WO2018162381A1 (en) | 2017-03-06 | 2018-03-05 | Inorganic foam based on calcium sulfoaluminate |
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JP7150742B2 JP7150742B2 (ja) | 2022-10-11 |
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JP2019548392A Active JP7150742B2 (ja) | 2017-03-06 | 2018-03-05 | スルホアルミン酸カルシウムベースの無機発泡体 |
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US (1) | US11066337B2 (ja) |
EP (2) | EP3592715B1 (ja) |
JP (1) | JP7150742B2 (ja) |
CN (1) | CN110650934A (ja) |
AU (2) | AU2018232506A1 (ja) |
CA (1) | CA3055003A1 (ja) |
ES (2) | ES2887030T3 (ja) |
PL (2) | PL3907203T3 (ja) |
SA (1) | SA519410064B1 (ja) |
WO (1) | WO2018162381A1 (ja) |
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CN117083255A (zh) * | 2021-03-26 | 2023-11-17 | 圣马-麦格纳1有限公司 | 水泥组合物 |
IT202100013175A1 (it) * | 2021-05-20 | 2022-11-20 | Isoltech S R L | Metodo di preparazione di una schiuma minerale, schiuma minerale e relativo uso. |
CN113998700B (zh) * | 2021-10-12 | 2024-03-08 | 昆明理工大学 | 一种以微硅粉为原料制备Si/SiC@C负极材料的方法 |
CN114804790A (zh) * | 2022-04-08 | 2022-07-29 | 山东大学 | 一种钙矾石基储能泡沫轻质土及其制备方法和应用 |
CN116003140B (zh) * | 2022-12-25 | 2023-09-19 | 江苏极易新材料有限公司 | 一种低堆积密度的复配剂的造粒方法 |
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CA3055003A1 (en) | 2018-09-13 |
PL3907203T3 (pl) | 2022-11-21 |
ES2887030T3 (es) | 2021-12-21 |
EP3907203B1 (en) | 2022-07-20 |
AU2018232506A1 (en) | 2019-09-26 |
ES2925454T3 (es) | 2022-10-18 |
US20200024201A1 (en) | 2020-01-23 |
EP3592715B1 (en) | 2021-07-14 |
RU2019130668A3 (ja) | 2021-07-05 |
WO2018162381A1 (en) | 2018-09-13 |
EP3592715A1 (en) | 2020-01-15 |
SA519410064B1 (ar) | 2023-01-17 |
JP7150742B2 (ja) | 2022-10-11 |
CN110650934A (zh) | 2020-01-03 |
PL3592715T3 (pl) | 2022-02-14 |
US11066337B2 (en) | 2021-07-20 |
EP3907203A1 (en) | 2021-11-10 |
AU2023210634A1 (en) | 2023-08-24 |
RU2019130668A (ru) | 2021-04-07 |
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