JP2019529610A - 多段階ポリマー生成の生成を効果的に制御するための装置及び方法 - Google Patents

多段階ポリマー生成の生成を効果的に制御するための装置及び方法 Download PDF

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JP2019529610A
JP2019529610A JP2019511938A JP2019511938A JP2019529610A JP 2019529610 A JP2019529610 A JP 2019529610A JP 2019511938 A JP2019511938 A JP 2019511938A JP 2019511938 A JP2019511938 A JP 2019511938A JP 2019529610 A JP2019529610 A JP 2019529610A
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reaction
introduction
polymer
monitored
characteristic
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JP2019529610A5 (https=
Inventor
ウェイン フレデリック リード，
ウェイン フレデリック リード，
マイケル フェリックス ドレンスキ，
マイケル フェリックス ドレンスキ，
ナタリー レオナルディ，
ナタリー レオナルディ，
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Yokogawa Fluence Analytics Inc
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Advanced Polymer Monitoring Technologies Inc
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Publication of JP2019529610A5 publication Critical patent/JP2019529610A5/ja
Priority to JP2024088483A priority Critical patent/JP2024113002A/ja
Priority to JP2025157552A priority patent/JP2026001067A/ja
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/001—Multistage polymerisation processes characterised by a change in reactor conditions without deactivating the intermediate polymer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0033—Optimalisation processes, i.e. processes with adaptive control systems
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
    • C08F20/52—Amides or imides
    • C08F20/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
    • C08F20/56—Acrylamide; Methacrylamide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G85/00—General processes for preparing compounds provided for in this subclass
    • G—PHYSICS
    • G05—CONTROLLING; REGULATING
    • G05B—CONTROL OR REGULATING SYSTEMS IN GENERAL; FUNCTIONAL ELEMENTS OF SUCH SYSTEMS; MONITORING OR TESTING ARRANGEMENTS FOR SUCH SYSTEMS OR ELEMENTS
    • G05B13/00—Adaptive control systems, i.e. systems automatically adjusting themselves to have a performance which is optimum according to some preassigned criterion
    • G05B13/02—Adaptive control systems, i.e. systems automatically adjusting themselves to have a performance which is optimum according to some preassigned criterion electric
    • G05B13/04—Adaptive control systems, i.e. systems automatically adjusting themselves to have a performance which is optimum according to some preassigned criterion electric involving the use of models or simulators
    • G—PHYSICS
    • G06—COMPUTING OR CALCULATING; COUNTING
    • G06F—ELECTRIC DIGITAL DATA PROCESSING
    • G06F17/00—Digital computing or data processing equipment or methods, specially adapted for specific functions
    • G06F17/10—Complex mathematical operations
    • G06F17/11—Complex mathematical operations for solving equations, e.g. nonlinear equations, general mathematical optimization problems
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2400/00—Characteristics for processes of polymerization
    • C08F2400/02—Control or adjustment of polymerization parameters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2500/00—Characteristics or properties of obtained polyolefins; Use thereof
    • C08F2500/05—Bimodal or multimodal molecular weight distribution
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/02—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material
    • G01N11/04—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/65—Raman scattering

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Mathematical Physics (AREA)
  • Theoretical Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Software Systems (AREA)
  • Computational Mathematics (AREA)
  • Data Mining & Analysis (AREA)
  • Mathematical Analysis (AREA)
  • Mathematical Optimization (AREA)
  • Pure & Applied Mathematics (AREA)
  • Algebra (AREA)
  • Medical Informatics (AREA)
  • Evolutionary Computation (AREA)
  • Computer Vision & Pattern Recognition (AREA)
  • Operations Research (AREA)
  • Artificial Intelligence (AREA)
  • Databases & Information Systems (AREA)
  • General Engineering & Computer Science (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Polymerisation Methods In General (AREA)
JP2019511938A 2016-08-31 2017-08-31 多段階ポリマー生成の生成を効果的に制御するための装置及び方法 Pending JP2019529610A (ja)

Priority Applications (2)

Application Number Priority Date Filing Date Title
JP2024088483A JP2024113002A (ja) 2016-08-31 2024-05-31 多段階ポリマー生成の生成を効果的に制御するための装置及び方法
JP2025157552A JP2026001067A (ja) 2016-08-31 2025-09-22 多段階ポリマー生成の生成を効果的に制御するための装置及び方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201662382062P 2016-08-31 2016-08-31
US62/382,062 2016-08-31
PCT/US2017/049732 WO2018045231A1 (en) 2016-08-31 2017-08-31 Device and methods to actively control the production of multi-stage polymer production

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JP2024088483A Division JP2024113002A (ja) 2016-08-31 2024-05-31 多段階ポリマー生成の生成を効果的に制御するための装置及び方法

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JP2019529610A true JP2019529610A (ja) 2019-10-17
JP2019529610A5 JP2019529610A5 (https=) 2020-10-08

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JP2019511938A Pending JP2019529610A (ja) 2016-08-31 2017-08-31 多段階ポリマー生成の生成を効果的に制御するための装置及び方法
JP2024088483A Pending JP2024113002A (ja) 2016-08-31 2024-05-31 多段階ポリマー生成の生成を効果的に制御するための装置及び方法
JP2025157552A Pending JP2026001067A (ja) 2016-08-31 2025-09-22 多段階ポリマー生成の生成を効果的に制御するための装置及び方法

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JP2025157552A Pending JP2026001067A (ja) 2016-08-31 2025-09-22 多段階ポリマー生成の生成を効果的に制御するための装置及び方法

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US (2) US12012471B2 (https=)
EP (1) EP3491471A4 (https=)
JP (3) JP2019529610A (https=)
WO (1) WO2018045231A1 (https=)

Cited By (1)

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Publication number Priority date Publication date Assignee Title
JP2025507697A (ja) * 2022-02-26 2025-03-21 ヨコガワ フルエンス アナリティクス， インコーポレイテッド 重合反応の酸素ベースの制御

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3491471A4 (en) 2016-08-31 2020-01-15 Advanced Polymer Monitoring Technologies Inc. DEVICE AND METHOD FOR ACTIVE CONTROL OF A MULTI-STAGE POLYMER PRODUCTION
CN117270483B (zh) * 2023-11-22 2024-04-12 中控技术股份有限公司 化工生产装置全流程动态优化控制方法、装置、电子设备
CN120949722A (zh) * 2025-08-15 2025-11-14 青岛仁成海绵制品有限公司 多变量协同的聚氨酯连续生产智能控制方法及系统
CN121338666B (zh) * 2025-12-19 2026-03-20 西安凯翔光电科技有限公司 基于光谱分析的聚合反应智能监测调控方法、装置

Citations (1)

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Publication number Priority date Publication date Assignee Title
WO2016054138A1 (en) * 2014-10-01 2016-04-07 Advanced Polymer Monitoring Technologies, Inc. Systems and methods for control of polymer reactions and processing using automatic continuous online monitoring

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3972804A (en) * 1974-10-02 1976-08-03 Universal Oil Products Company Control of hydrogen/hydrocarbon mole ratio in hydrogen-consuming process
US3974064A (en) * 1974-10-02 1976-08-10 Universal Oil Products Company Control of hydrogen/hydrocarbon mole ratio and the control system therefor
JPS55142008A (en) * 1979-04-23 1980-11-06 Mitsui Petrochem Ind Ltd Preparation of polyolefin
US6042790A (en) * 1993-02-08 2000-03-28 Phillips Petroleum Company Apparatus for maintaining unreacted monomer concentration in a polymerization reactor
US7838605B2 (en) 2003-10-17 2010-11-23 Univation Technologies, Llc Polymerization monitoring and control using improved leading indicators
US6988022B2 (en) * 2004-04-13 2006-01-17 Univation Technologies, Llc Method for online estimation of reactor split for multimodal polyolefins
US7179882B2 (en) * 2004-08-02 2007-02-20 Bayer Materialscience Llc Low viscosity polymer polyols
US7786203B2 (en) 2005-09-16 2010-08-31 Milliken & Company Polymer compositions comprising nucleating or clarifying agents and articles made using such compositions
US8071699B2 (en) * 2006-09-21 2011-12-06 Union Carbide Chemicals & Plastics Technology Llc Methods of controlling properties in multimodal systems
JP5296694B2 (ja) * 2006-09-29 2013-09-25 ジ アドミニストレイターズ オブ ザ チューレン エデュケイショナル ファンド 懸濁液内の微粒子の特性及び反応中の可溶性成分の特性を同時にモニタリングする方法及び装置
JP5244574B2 (ja) 2008-12-16 2013-07-24 日本ポリプロ株式会社 ポリオレフィンの製造方法及びその装置
JP5726721B2 (ja) * 2011-12-27 2015-06-03 日本ポリプロ株式会社 ポリオレフィンの製造方法およびその装置
EP3230712A4 (en) 2015-01-22 2018-05-16 Advanced Polymer Monitoring Technologies Inc. Systems and methods for predicting and controlling the properties of a chemical species during a time-dependent process
EP3491471A4 (en) 2016-08-31 2020-01-15 Advanced Polymer Monitoring Technologies Inc. DEVICE AND METHOD FOR ACTIVE CONTROL OF A MULTI-STAGE POLYMER PRODUCTION

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016054138A1 (en) * 2014-10-01 2016-04-07 Advanced Polymer Monitoring Technologies, Inc. Systems and methods for control of polymer reactions and processing using automatic continuous online monitoring

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2025507697A (ja) * 2022-02-26 2025-03-21 ヨコガワ フルエンス アナリティクス， インコーポレイテッド 重合反応の酸素ベースの制御

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Publication number Publication date
US12522674B2 (en) 2026-01-13
WO2018045231A1 (en) 2018-03-08
JP2026001067A (ja) 2026-01-06
US20240309121A1 (en) 2024-09-19
US12012471B2 (en) 2024-06-18
EP3491471A4 (en) 2020-01-15
JP2024113002A (ja) 2024-08-21
US20190194360A1 (en) 2019-06-27
EP3491471A1 (en) 2019-06-05

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