JP2019521235A - 完全に配合された潤滑組成物のための脂肪族四面体ボレート化合物 - Google Patents
完全に配合された潤滑組成物のための脂肪族四面体ボレート化合物 Download PDFInfo
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- JP2019521235A JP2019521235A JP2019502677A JP2019502677A JP2019521235A JP 2019521235 A JP2019521235 A JP 2019521235A JP 2019502677 A JP2019502677 A JP 2019502677A JP 2019502677 A JP2019502677 A JP 2019502677A JP 2019521235 A JP2019521235 A JP 2019521235A
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- 125000004076 pyridyl group Chemical group 0.000 description 1
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- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
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- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229940116351 sebacate Drugs 0.000 description 1
- CXMXRPHRNRROMY-UHFFFAOYSA-L sebacate(2-) Chemical compound [O-]C(=O)CCCCCCCCC([O-])=O CXMXRPHRNRROMY-UHFFFAOYSA-L 0.000 description 1
- BHRZNVHARXXAHW-UHFFFAOYSA-N sec-butylamine Chemical compound CCC(C)N BHRZNVHARXXAHW-UHFFFAOYSA-N 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical group [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 description 1
- 239000011684 sodium molybdate Substances 0.000 description 1
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- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 description 1
- NESLWCLHZZISNB-UHFFFAOYSA-M sodium phenolate Chemical compound [Na+].[O-]C1=CC=CC=C1 NESLWCLHZZISNB-UHFFFAOYSA-M 0.000 description 1
- 229960004025 sodium salicylate Drugs 0.000 description 1
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- 235000007586 terpenes Nutrition 0.000 description 1
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 1
- YBRBMKDOPFTVDT-UHFFFAOYSA-N tert-butylamine Chemical compound CC(C)(C)N YBRBMKDOPFTVDT-UHFFFAOYSA-N 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- DZLFLBLQUQXARW-UHFFFAOYSA-N tetrabutylammonium Chemical compound CCCC[N+](CCCC)(CCCC)CCCC DZLFLBLQUQXARW-UHFFFAOYSA-N 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- 125000001544 thienyl group Chemical group 0.000 description 1
- 125000003396 thiol group Chemical class [H]S* 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 description 1
- 125000005425 toluyl group Chemical group 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 125000005270 trialkylamine group Chemical group 0.000 description 1
- ABVVEAHYODGCLZ-UHFFFAOYSA-N tridecan-1-amine Chemical compound CCCCCCCCCCCCCN ABVVEAHYODGCLZ-UHFFFAOYSA-N 0.000 description 1
- IOYXJNDDBALLFR-UHFFFAOYSA-N tridecane-1,2-diol Chemical compound CCCCCCCCCCCC(O)CO IOYXJNDDBALLFR-UHFFFAOYSA-N 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- QAUCEEIOCLCCFG-UHFFFAOYSA-N trihydroxy borate Chemical compound OOB(OO)OO QAUCEEIOCLCCFG-UHFFFAOYSA-N 0.000 description 1
- RKBCYCFRFCNLTO-UHFFFAOYSA-N triisopropylamine Chemical compound CC(C)N(C(C)C)C(C)C RKBCYCFRFCNLTO-UHFFFAOYSA-N 0.000 description 1
- DXRFOGXSSDRZFP-UHFFFAOYSA-N tripentyl 2-hydroxypropane-1,2,3-tricarboxylate Chemical compound CCCCCOC(=O)CC(O)(C(=O)OCCCCC)CC(=O)OCCCCC DXRFOGXSSDRZFP-UHFFFAOYSA-N 0.000 description 1
- HVLLSGMXQDNUAL-UHFFFAOYSA-N triphenyl phosphite Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)OC1=CC=CC=C1 HVLLSGMXQDNUAL-UHFFFAOYSA-N 0.000 description 1
- YFTHZRPMJXBUME-UHFFFAOYSA-N tripropylamine Chemical compound CCCN(CCC)CCC YFTHZRPMJXBUME-UHFFFAOYSA-N 0.000 description 1
- QQBLOZGVRHAYGT-UHFFFAOYSA-N tris-decyl phosphite Chemical compound CCCCCCCCCCOP(OCCCCCCCCCC)OCCCCCCCCCC QQBLOZGVRHAYGT-UHFFFAOYSA-N 0.000 description 1
- 125000002221 trityl group Chemical group [H]C1=C([H])C([H])=C([H])C([H])=C1C([*])(C1=C(C(=C(C(=C1[H])[H])[H])[H])[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 description 1
- CMPGARWFYBADJI-UHFFFAOYSA-L tungstic acid Chemical compound O[W](O)(=O)=O CMPGARWFYBADJI-UHFFFAOYSA-L 0.000 description 1
- 229940036248 turpentine Drugs 0.000 description 1
- BUMVVNKGNPPUME-UHFFFAOYSA-N undecane-1,2-diol Chemical compound CCCCCCCCCC(O)CO BUMVVNKGNPPUME-UHFFFAOYSA-N 0.000 description 1
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000003981 vehicle Substances 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000010698 whale oil Substances 0.000 description 1
- 125000005023 xylyl group Chemical group 0.000 description 1
Classifications
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- C10M139/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing atoms of elements not provided for in groups C10M127/00 - C10M137/00
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- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/02—Boron compounds
- C07F5/022—Boron compounds without C-boron linkages
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- C10M101/00—Lubricating compositions characterised by the base-material being a mineral or fatty oil
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- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/04—Hydroxy compounds
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- C10M135/10—Sulfonic acids or derivatives thereof
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- C10M135/32—Heterocyclic sulfur, selenium or tellurium compounds
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- C10M137/04—Phosphate esters
- C10M137/10—Thio derivatives
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- C10M149/10—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a nitrogen-containing hetero ring
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- C10M161/00—Lubricating compositions characterised by the additive being a mixture of a macromolecular compound and a non-macromolecular compound, each of these compounds being essential
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- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
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- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
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- C10M2203/102—Aliphatic fractions
- C10M2203/1025—Aliphatic fractions used as base material
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- C10M2205/028—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers containing aliphatic monomers having more than four carbon atoms
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Abstract
Description
本発明の例示的な実施形態は、潤滑組成物において有用な、特に潤滑剤において改善された溶解度および摩擦性能を有する摩擦調整剤として有用な、潤滑剤添加剤および特にイオン性ボレート化合物に関する。
例示的な実施形態の一態様によると、完全に配合された潤滑組成物は、潤滑粘度油と、イオン性四面体ボレート化合物であって、両方とも直鎖C18−タルトリミドである2つの二座ジオキソ配位子を有するホウ素原子を有する四面体ホウ酸アニオン、ポリイソブテニル数平均分子量750〜2,500を有する従来のアンモニウム置換ポリイソブテニルスクシンイミド化合物を含む第1の分散剤、ならびにN:CO比1.8およびポリブチレニル数平均分子量750〜2,500を有するアンモニウム置換ポリイソブテニルスクシンイミド(succinimde)化合物を含む第2の分散剤を含み、第1の分散剤および第2の分散剤のうちの1種または複数種がカチオン形態である、イオン性四面体ボレート化合物とを含む。完全に配合された潤滑組成物は、清浄剤、酸化防止剤、分散剤、摩耗防止剤、粘度調整剤、極圧剤、消泡剤、腐食防止剤、流動点降下剤、摩擦調整剤、抗乳化剤、およびシール膨張剤のうちの1種または複数種から選択される性能添加剤をさらに含む。
例示的な実施形態の態様は、潤滑組成物、潤滑方法、および潤滑組成物の使用に関する。
A.イオン性ボレート化合物
R3およびR4は、独立して、水素(R3とR4の両方が通常水素でないことを条件とする)もしくは1〜48個の炭素原子の脂肪族ヒドロカルビル基であるか、または一緒になって、複素環式環(1〜32個の炭素原子の1つもしくは複数のヒドロカルビル基で置換されていてよい)であってよい置換もしくは非置換の5もしくは6員の脂肪族環を形成し、
mは、0または1であり、
Xは、水素、1〜24個の炭素原子のヒドロカルビル基、−OR5、−NHR5、=O、およびこれらの混合物から選択され、
R5は、1〜24個の炭素原子のヒドロカルビル基であり、
Mは、カチオンを表し、
nは、整数、すなわち、少なくとも1であり、最大7、または最大4であることができる)
で示される一般的構造で表すことができる。
(i)炭化水素置換基、すなわち、脂肪族(例えば、アルキルまたはアルケニル)、脂環式(例えば、シクロアルキル、シクロアルケニル)置換基、および芳香族置換されている脂肪族または脂環式置換基、ならびに環が分子の別の部分を介して完成する環式置換基(例えば、2つの置換基が一緒になって環を形成する);
(ii)置換されている炭化水素置換基、すなわち、本発明との関連で非炭化水素基を含有する置換基は、置換基の主に炭化水素の性質を変化させない(例えば、ハロ(特にクロロおよびフルオロ)、ヒドロキシ、アルコキシ、メルカプト、アルキルメルカプト、ニトロ、ニトロソ、およびスルホキシ);
(iii)ヘテロ置換基、すなわち、主に炭化水素の性状を有する一方で、その他は炭素原子で構成される環または鎖内に炭素以外を含有し得る置換基。
X’およびm’は、Xおよびmに対してそれぞれ記載されている通りであってよい)
で示される構造で表すことができる。
[B]− n−pqMn+([A]q−)p
(式中、[A]−は、第2のアニオンを表し、q≧1、p≧1、かつn−pq≧1である)
のものであってよい。
組成物を形成する方法
で表すことができる。
として示されている。
C.他の性能添加剤
清浄剤
酸化防止剤
分散剤
摩耗防止剤
油溶性チタン化合物
極圧(EP)剤
消泡剤
粘度調整剤
腐食防止剤および金属不活性化剤
流動点降下剤
摩擦調整剤
抗乳化剤
シール膨張剤
潤滑組成物の使用
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/ポリイソブチレンスクシンイミドベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物を含む混合物を、N−オレイルタルトリミド(44.6g)、トリス(2−エチルヘキシル)ボレート32.6g)、および100 TBNの直接アルキル化ポリイソブチレンスクシンイミド(PIBSA)分散剤(14%希釈油を含有する)(22.8g)をブレンドして、タルトリミド:ボレート:PIBSAのモル比2:1:1を得ることにより形成する。PIBSA分散剤は、1000Mnの高ビニリデンポリイソブチレンおよびN:CO(m)比1.79およびTBN 100を有するコハク酸無水物から作製する。大気圧下、反応は80℃で2時間行う。生成物はさらに精製せずに単離する。
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/ポリイソブチレンスクシンイミドベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物含有混合物を実施例1の通りであるが、N−オレイルタルトリミド(21.9g)は、60%OTおよび40%鉱油の混合物として供給し、PIBSA分散剤を2000Mnの高ビニリデンポリイソブチレンならびにN:CO(m)比1.79およびTBN 13を有するコハク酸無水物から作製して、形成する。
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/過塩基性カルシウムスルホネート清浄剤ベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物を含む混合物を、60%OTと40%鉱油との混合物として供給されるN−オレイルタルトリミド(70.8g)、トリス(2−エチルヘキシル)ボレート(21.7g)、および400 TBNのカルシウムスルホネート清浄剤(7.5g)をブレンドして、タルトリミド:ボレート:清浄剤のモル比2:1:1を得ることによって形成する。反応は80℃で2時間行う。生成物はさらに精製せずに単離する。
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/過塩基性カルシウムスルホネート清浄剤ベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物を含む混合物を、反応を100℃で2時間行うこと、および生じた混合物を減圧下に配置して、アルコール(2−エチルヘキサノール)を共沸蒸留することを除いて、実施例2の通り形成する。生成物はさらに精製せずに単離する。
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/中性のカルシウムスルホネート清浄剤ベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物を含む混合物を、85 TBNのカルシウムスルホネート清浄剤(28.0g)を使用することを除いて、実施例2の通り形成する。
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/フェノール系酸化防止剤ベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物を含む混合物を、2,6−ジ−(secブチル),4−(2−エチルヘキシルアミノメチルフェノール(21.6g)を塩基として使用することを除いて、実施例2の通り形成する。
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/過塩基性カルシウムスルホネート清浄剤ベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物を含む混合物を、(11.6g)の400 TBNのカルシウムスルホネート清浄剤を用いて、タルトリミド:ボレート:清浄剤のモル比1:1:1を得ることを除いて、実施例2に記載されている通り形成する。
N−オレイルタルトリミド/トリス(2−エチルヘキシル)ボレート/過塩基性カルシウムスルホネート清浄剤ベースのイオン性四面体ボレート化合物:イオン性四面体ボレート化合物を含む混合物を、(11.6g)の400のTBNのカルシウムスルホネート清浄剤を用いて、タルトリミド:ボレート:清浄剤のモル比1:1:1を得ることを除いて、実施例3に記載されている通り形成する。
溶媒プロセス手順1による四面体ホウ素化N−オレイルタルトリミド(四面体の複合体を形成するための、ホウ酸の存在下でのin situでのタルトリミドの形成):187.6gの酒石酸(1.25mol、2.0当量)および19.3gのホウ酸(0.31mol、0.5当量)を110gのペンタノール中で撹拌し、還流加熱する。334.4gのオレイルアミン(1.25mol、2.0当量)を添加漏斗を介して添加する。生じた反応物を140℃で5時間保持する。次いで、溶媒を、真空蒸留を介して除去して、さらに精製せずに最終生成物を得る。11B NMR (160 MHz, CDCl3) ppm: 9.60 (br).元素分析:0.6%B、3.2%N。
溶媒プロセス手順1による四面体ホウ素化N−オレイルタルトリミド:250gの酒石酸(0.93mol、2.0当量)および28.9gのホウ酸(0.47mol、1.0当量)を153gのブタノール中で撹拌し、加熱還流する。140.3gのオレイルアミン(0.93mol、2.0当量)を添加漏斗を介して添加する。一部の溶媒を除去しながら、生じた反応物を140〜145℃に加熱し、5時間保持する。次いで、溶媒を、真空蒸留を介して除去して、さらに精製せずに最終生成物を得る。11B NMR (160 MHz, CDCl3) ppm: 9.48 (br).元素分析:1.3%B、3.2%N。
溶媒プロセス手順2による四面体ホウ素化N−オレイルタルトリミド(四面体の複合体を形成するための、ホウ酸を後で添加する、in situでのタルトリミドの形成):1201gの酒石酸(8.0mol、2.0当量)を850gのペンタノール中で撹拌し、加熱還流する。2140gのオレイルアミン(8.0mol、2.0当量)を1時間にわたり添加する。反応物を140℃で5時間保持し、次いで110℃に冷却する。123.6gのホウ酸(2.0mol、0.5当量)を一度に添加する。次いで、反応混合物を140℃に加熱し、2時間保持する。次いで、溶媒を、真空蒸留を介して除去して、さらに精製せずに最終生成物を得る。11B NMR (160 MHz, CDCl3) ppm: 10.39 (br), 7.32 (br), 6.21 (br).元素分析:0.6%B、3.3%N。
グリセロールモノオレエート(GMO)、ホウ酸およびアミンから調製される四面体ボレート:254gのGMO(0.5mol、2.0当量)および15.5gのホウ酸(0.25mol、1.0当量)を撹拌しながら165℃に加熱する。反応物をこの温度で3時間保持する。次いで、46.4gのトリ−n−ブチルアミン(0.25mol、1.0当量)を一度に添加する。生じた反応混合物を165℃でさらに3時間保持して、さらに精製せずに所望の生成物を得る。11B NMR (160 MHz, CDCl3) ppm: 11.39 (br).
グリセロールモノオレエート(GMO)、ホウ酸および400 TBNのCa清浄剤から調製される四面体ボレート:257gのGMO(0.5mol、2.0当量)および15.7gのホウ酸(0.25mol、1.0当量)を撹拌しながら165℃に加熱する。反応物をこの温度で4時間保持する。35.5gの400 TBNのCa清浄剤を添加して、反応を165℃でさらに3時間保持する。粗生成物を濾過して、所望の生成物を得る。11B NMR (160 MHz, CDCl3) ppm: 9.98 (br), 6.75 (br).
グリセロールモノオレエート(GMO)、ホウ酸および100 TBNのポリイソブチレンスクシンイミド(PIBSA)分散剤から調製される四面体ボレート:508gのGMO(1.0mol、2.0当量)、241.3gの三面体ホウ酸エステル(0.5mol、1.0当量)、および280.5gの100 TBNのポリイソブチレンスクシンイミド(PIBSA)分散剤(0.5mol、1.0当量)を80℃で2時間混合して、さらに精製せずに所望の生成物を得る。11B NMR (160 MHz, CDCl3) ppm: 22.73 (br), 17.58 (br), 10.08 (br).
1,2−オクタンジオール、ホウ酸およびアミンから調製される四面体ボレート:146gの1,2−オクタンジオール(1.0mol、2.0当量)および30.9gのホウ酸(0.5mol、1.0当量)を撹拌しながら165℃に加熱する。反応物をこの温度で2時間保持し、次いで140℃に冷却する。64.6gの2−エチルヘキシルアミン(0.5mol、1.0当量)を添加漏斗を介して添加する。生じた混合物を140℃で3時間撹拌して、さらに精製せずに所望の生成物を得る。11B NMR (160 MHz) ppm: 11.71 (br)
比較用潤滑剤実施例CLE4:全Caスルホネート過塩基性清浄剤を含む乗用車エンジンオイル中のOTを含む潤滑組成物。
Claims (41)
- 潤滑粘度油と、
イオン性四面体ボレート化合物であって、
両方とも直鎖C18−タルトリミドである2つの二座ジオキソ配位子を有するホウ素原子を有する四面体ホウ酸アニオン、
ポリイソブテニル数平均分子量750〜2,500を有する従来のアンモニウム置換ポリイソブテニルスクシンイミド化合物を含む第1の分散剤、
N:CO比1.8およびポリブチレニル数平均分子量750〜2,500を有するアンモニウム置換ポリイソブテニルスクシンイミド化合物を含む第2の分散剤を含み、
前記第1の分散剤および前記第2の分散剤のうちの1種または複数種がカチオン形態である、イオン性四面体ボレート化合物と
清浄剤、酸化防止剤、分散剤、摩耗防止剤、粘度調整剤、極圧剤、消泡剤、腐食防止剤、流動点降下剤、摩擦調整剤、抗乳化剤、およびシール膨張剤からなる群から選択される性能添加剤と、
を含む、完全に配合された潤滑組成物。 - 前記潤滑粘度油が、グループI基油、グループII基油、グループII基油、グループIII基油、グループIV基油、およびグループV基油からなる群から選択される基油を含む、請求項1または2に記載の組成物。
- 前記清浄剤が、アルカリ土類金属スルホネート、フェネートおよびサリチレートからなる群から選択される過塩基性金属含有清浄剤を含む、請求項1から3に記載の組成物。
- 前記清浄剤が、0.01重量%〜1.1重量%の範囲の量で前記組成物中に存在する、請求項1から4に記載の組成物。
- 前記分散剤が、ポリイソブテニルスクシンイミドを含む、請求項1から5に記載の組成物。
- 前記分散剤が、0.01重量%〜20重量%の範囲の量で前記組成物中に存在する、請求項1から6に記載の組成物。
- 前記酸化防止剤が、無灰酸化防止剤を含む、請求項1から7に記載の組成物。
- 前記酸化防止剤が、0.1重量%〜3重量%の範囲の量で前記組成物中に存在する、請求項1から8に記載の組成物。
- 前記摩耗防止剤が、ジアルキルジチオリン酸亜鉛を含む、請求項1から9に記載の組成物。
- 前記摩耗防止剤が、0.01重量%〜3重量%の範囲の量で前記組成物中に存在する、請求項1から10に記載の組成物。
- 前記粘度調整剤が、0.01重量%〜10重量%の範囲の量で前記組成物中に存在する、請求項1から11に記載の組成物。
- 前記極圧剤が、0.01重量%〜3重量%の範囲の量で前記組成物中に存在する、請求項1から12に記載の組成物。
- 前記消泡剤が、ポリシロキサン、アクリル酸エチルと2−エチルヘキシルアクリレートのコポリマー、フッ化ポリシロキサン、トリアルキルホスフェート、ポリエチレングリコール、ポリエチレンオキシド、ポリプロピレンオキシドおよび(エチレンオキシド−プロピレンオキシド)ポリマーからなる群から選択される、請求項1から13に記載の組成物。
- 前記腐食防止剤が、脂肪アミン、オクタン酸オクチルアミン、ドデセニルコハク酸または無水物の縮合物、脂肪酸、ベンゾトリアゾールの誘導体、1,2,4−トリアゾール、ベンゾイミダゾール、2−アルキルジチオベンゾイミダゾールおよび2−アルキルジチオベンゾチアゾールからなる群から選択される、請求項1から14に記載の組成物。
- 前記流動点降下剤が、ポリアルファオレフィン、無水マレイン酸−スチレンコポリマーのエステル、ポリメタクリレート、ポリアクリレート、およびポリアクリルアミドからなる群から選択される、請求項1から16に記載の組成物。
- 前記摩擦調整剤が、0.005〜2重量%の範囲の量で前記組成物中に存在する窒素含有モリブデン化合物を含む、請求項1から16に記載の組成物。
- 前記抗乳化剤が、トリアルキルホスフェート、ならびにエチレングリコール、エチレンオキシド、プロピレンオキシドのポリマーおよびコポリマーからなる群から選択される、請求項1から17に記載の組成物。
- 前記シール膨張剤が、スルホレン誘導体を含む、請求項1から18に記載の組成物。
- 油溶性チタン化合物をさらに含む、請求項1から19に記載の組成物。
- 潤滑粘度油と、
イオン性四面体ボレート化合物であって、
両方とも直鎖C18−タルトリミドである2つの二座ジオキソ配位子を有するホウ素原子を有する四面体ホウ酸アニオン、
ポリイソブテニル数平均分子量750〜2,500を有する従来のアンモニウム置換ポリイソブテニルスクシンイミド化合物を含む第1の分散剤、ならびに
N:CO比1.8およびポリブチレニル数平均分子量750〜2,500を有するアンモニウム置換ポリイソブテニルスクシンイミド化合物を含む第2の分散剤を含み、
前記第1の分散剤および前記第2の分散剤のうちの1種または複数種がカチオン形態である、イオン性四面体ボレート化合物と、
第3のポリイソブテニルスクシンイミド分散剤と、
アルカリ土類金属スルホネート、フェネートおよびサリチレートからなる群から選択される、過塩基性金属含有清浄剤と、
ジアルキルジチオリン酸亜鉛と、
無灰酸化防止剤と、
粘度調整剤、極圧剤、消泡剤、腐食防止剤、流動点降下剤、摩擦調整剤、抗乳化剤、およびシール膨張剤からなる群から選択される性能添加剤と
を含む、完全に配合された潤滑組成物。 - 内燃エンジンを潤滑させる方法であって、
完全に配合された潤滑組成物を前記エンジンの潤滑システムに供給することを含み、前記完全に配合された潤滑組成物が、
潤滑粘度油と、
イオン性四面体ボレート化合物であって、
両方とも直鎖C18−タルトリミドである2つの二座ジオキソ配位子を有するホウ素原子を有する四面体ホウ酸アニオン、
ポリイソブテニル数平均分子量750〜2,500を有する従来のアンモニウム置換ポリイソブテニルスクシンイミド化合物を含む第1の分散剤、
N:CO比1.8およびポリブチレニル数平均分子量750〜2,500を有するアンモニウム置換ポリイソブテニルスクシンイミド化合物を含む第2の分散剤を含み、
前記第1の分散剤および前記第2の分散剤のうちの1種または複数種がカチオン形態である、イオン性四面体ボレート化合物と、
清浄剤、酸化防止剤、分散剤、摩耗防止剤、粘度調整剤、極圧剤、消泡剤、腐食防止剤、流動点降下剤、摩擦調整剤、抗乳化剤、およびシール膨張剤からなる群から選択される性能添加剤と
を含む、方法。 - 前記潤滑粘度油が、グループI基油、グループII基油、グループII基油、グループIII基油、グループIV基油、およびグループV基油からなる群から選択される基油を含む、請求項22または23に記載の方法。
- 前記清浄剤が、アルカリ土類金属スルホネート、フェネートおよびサリチレートからなる群から選択される過塩基性金属含有清浄剤を含む、請求項22から24に記載の方法。
- 前記清浄剤が、0.01重量%〜1.1重量%の範囲の量で前記組成物中に存在する、請求項22から25に記載の方法。
- 前記分散剤が、ポリイソブテニルスクシンイミドを含む、請求項22から26に記載の方法。
- 前記分散剤が、0.01重量%〜20重量%の範囲の量で前記組成物中に存在する、請求項22から27に記載の方法。
- 前記酸化防止剤が、無灰酸化防止剤を含む、請求項22から28に記載の方法。
- 前記酸化防止剤が、0.1重量%〜3重量%の範囲の量で前記組成物中に存在する、請求項22から29に記載の方法。
- 前記摩耗防止剤が、ジアルキルジチオリン酸亜鉛を含む、請求項22から30に記載の方法。
- 前記摩耗防止剤が、0.01重量%〜3重量%の範囲の量で前記組成物中に存在する、請求項22 31に記載の方法。
- 前記粘度調整剤が、0.01重量%〜10重量%の範囲の量で前記組成物中に存在する、請求項22から32に記載の方法。
- 前記極圧剤が、0.01重量%〜3重量%の範囲の量で前記組成物中に存在する、請求項22から33に記載の方法。
- 前記消泡剤が、ポリシロキサン、アクリル酸エチルと2−エチルヘキシルアクリレートのコポリマー、フッ化ポリシロキサン、トリアルキルホスフェート、ポリエチレングリコール、ポリエチレンオキシド、ポリプロピレンオキシドおよび(エチレンオキシド−プロピレンオキシド)ポリマーからなる群から選択される、請求項22から34に記載の方法。
- 前記腐食防止剤が、脂肪アミン、オクタン酸オクチルアミン、ドデセニルコハク酸または無水物の縮合物、脂肪酸、ベンゾトリアゾールの誘導体、1,2,4−トリアゾール、ベンゾイミダゾール、2−アルキルジチオベンゾイミダゾールおよび2−アルキルジチオベンゾチアゾールからなる群から選択される、請求項22から35に記載の方法。
- 前記流動点降下剤が、ポリアルファオレフィン、無水マレイン酸−スチレンコポリマーのエステル、ポリメタクリレート、ポリアクリレート、およびポリアクリルアミドからなる群から選択される、請求項22から36に記載の方法。
- 前記摩擦調整剤が、0.005〜2重量%の範囲の量で前記組成物中に存在する窒素含有モリブデン化合物を含む、請求項22から37に記載の方法。
- 前記抗乳化剤が、トリアルキルホスフェート、ならびにエチレングリコール、エチレンオキシド、プロピレンオキシドのポリマーおよびコポリマーからなる群から選択される、請求項22から38に記載の方法。
- 前記シール膨張剤が、スルホレン誘導体を含む、請求項22から39に記載の方法。
- 油溶性チタン化合物をさらに含む、請求項22から40に記載の方法。
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