JP2019108316A - Sour orange derived functional material - Google Patents

Sour orange derived functional material Download PDF

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JP2019108316A
JP2019108316A JP2017255346A JP2017255346A JP2019108316A JP 2019108316 A JP2019108316 A JP 2019108316A JP 2017255346 A JP2017255346 A JP 2017255346A JP 2017255346 A JP2017255346 A JP 2017255346A JP 2019108316 A JP2019108316 A JP 2019108316A
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citrus
saccharomyces
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citrus aurantium
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敦子 森田
Atsuko Morita
敦子 森田
孝男 中村
Takao Nakamura
孝男 中村
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Okada Maki
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Okada Maki
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Abstract

To solve problems in which, conventionally, cosmetics or materials for food product derived from combinations of a fruit, branch and leaf of Citrus aurantium classified to the genus Citrus of Rutaceae have been only, steam distillation, organic solvent and extract immersed in water.SOLUTION: The invention is configured to ferment any one of a fruit, branch and leaf of Citrus aurantium classified into the genus Citrus of Rutaceae or combination thereof by yeast, then distill the same by an ethanol aqueous solution, for obtaining a novel material with high functionality.SELECTED DRAWING: None

Description

本発明は、洗顔料、メイク落とし、化粧水、乳液、クリーム、美容液、美容オイル、化粧石けん等の化粧品類、薬用化粧品類、加工食品用、清涼飲料水用、健康補助用食品用、健康補助用飲料に使用されるミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉のうち一つか、またその組み合わせを酵母で発酵させた後、エタノール水溶液で蒸留することにより得られる化粧品用、薬用化粧品用、加工食品用、清涼飲料水用、健康補助用食品用、健康補助用飲料用素材に関する。  The present invention relates to a cleanser, makeup remover, lotion, milk, cream, essence, cosmetic oil, cosmetic such as cosmetic soap, cosmeceutical, processed food, soft drink, health supplement food, health Cosmetics obtained by fermenting with Citrus aurantium fruit, branches, leaves, or a combination thereof, which is classified into the genus Rutaceae, which is used for supplementary beverages, with yeast and then distilling with an aqueous ethanol solution The present invention relates to materials for medicinal cosmetics, processed foods, soft drinks, foods for health supplements, and beverages for health supplements.

技術背景Technology background

従来から、ミカン科ミカン属に分類されるCitrus aurantiumの果実はビターオレンジという表記にて化粧品やアロマで使用する精油として、多く活用されてきた。  Conventionally, the fruit of Citrus aurantium, which is classified as a citrus family Ricaceae, has been widely used as an essential oil used in cosmetics and aromas in the notation of bitter orange.

また、Citrus aurantiumであるビターオレンジは、柑橘系に特徴的な機能性成分を数多く含んでおり、美容や健康にも機能性を発揮する素材として認知が高いものである。  Bitter orange, which is Citrus aurantium, contains many functional ingredients characteristic of citrus fruits, and is highly recognized as a material that exhibits functionality for beauty and health.

前述のような機能性を目的として、柑橘系を素材とした加工食品、清涼飲料水、健康補助用食品、健康補助用飲料も数多く存在し、その中でもCitrus aurantiumであるビターオレンジは汎用性が高い。  There are many processed foods made from citrus fruits, soft drinks, foods for health supplements, beverages for health supplements for the purpose of functionality as mentioned above, among which Bitter Orange, Citrus aurantium, is highly versatile .

しかしながら、Citrus aurantiumであるビターオレンジを素材とした原材料の中でも、発酵と蒸留を組み合わせたものは未だ存在せず、その機能性も未知のものである。  However, among the raw materials based on bitter orange which is Citrus aurantium, there is still no combination of fermentation and distillation, and its functionality is also unknown.

本発明は、ミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の一つか、またその組み合わせを酵母で発酵させた後、エタノール水溶液で蒸留することにより得られる、未だ存在しなかった化粧品類、薬用化粧品類、加工食品、清涼飲料水、健康補助用食品用、健康補助用飲料用の素材を提供することを目的としている。  The present invention has not yet been obtained by fermenting one of Citrus aurantium fruits, branches and leaves, or a combination thereof classified in the genus Rutaceae, with yeast and then distilling with an aqueous ethanol solution. It is intended to provide materials for cosmetics, cosmeceuticals, processed foods, soft drinks, foods for health supplements, and beverages for health supplements.

本発明では、ミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の一つか、またその組み合わせを使用する。  In the present invention, one of Citrus aurantium fruits, branches and leaves, or a combination thereof, which is classified as an Ritaceae is used.

前項で使用するミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の一つか、またその組み合わせを、24乃至48時間、遮光条件で自然乾燥させる。  One of Citrus aurantium fruits, branches and leaves, or a combination thereof, which is classified in the Rutaceae family belonging to the Rutaceae family used in the preceding paragraph, is naturally dried in a light-shielded condition for 24 to 48 hours.

自然乾燥させたミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の一つか、またその組み合わせを、20乃至50度、遮光条件下で酵母により48時間以上発酵させる。  One of Citrus aurantium fruits, branches and leaves, or a combination thereof, which is classified into a naturally dried Citrus group of the family Ricaceae, is fermented by yeast at 20 to 50 ° C. for at least 48 hours under light blocking conditions.

前項で使用する酵母は、Saccharomyces属のSaccharomyces cerecisiae、Saccharomyces bayanus、Saccharomyces boulardii、Saccharomyces bulderi、Saccharomyces carioanus、Saccharomyces cariocus、Saccharomyces chevalieri、Saccharomyces dairenensis、Saccharomyces ellipsoideus、Saccharomyces florentinus、Saccharomyces kluyveri、Saccharomyces martiniae、Saccharomyces norbensis、Saccharomyces paradoxus、Saccharomyces pastorianus、Saccharomyces spencerorum、Saccharomyces turicensis、Saccharomyces unisporus、Saccharomycesuvarum、Saccharomyces zonatus、Saccharomycopsis属、Candida属のCandida kefyr、Candida bombicola、Candida utilis、Candida saitoana、Zygosaccharomyces属のZygosaccharomyces rouxii、Zygosaccharomyces microellipsoides、Kluyveromyces属、Schizosaccharomyces属のSchizosaccharomyces pombe、Torulaspora属のTorulaspora delbrueckii、Pichia属のPichia anomala、Pichia caribbica、Pseudoxyma属のPseudoxyma tsukubaensis、Endomyces属のうち一つか、また二つ以上の組合せを使用する。  Yeast used in the previous section, Saccharomyces genus Saccharomyces cerecisiae, Saccharomyces bayanus, Saccharomyces boulardii, Saccharomyces bulderi, Saccharomyces carioanus, Saccharomyces cariocus, Saccharomyces chevalieri, Saccharomyces dairenensis, Saccharomyces ellipsoideus, Saccharomyces florentinus, Saccharomyces kluyveri, Saccharomyces martiniae, Saccharomyces norben is, Saccharomyces paradoxus, Saccharomyces pastorianus, Saccharomyces spencerorum, Saccharomyces turicensis, Saccharomyces unisporus, Saccharomycesuvarum, Saccharomyces zonatus, Saccharomycopsis genus, Candida genus Candida kefyr, Candida bombicola, Candida utilis, Candida saitoana, Zygosaccharomyces the genus Zygosaccharomyces rouxii, Zygosaccharomyces microellipsoid Es, Kluyveromyces sp., Schizosaccharomyces sp. Schizosaccharomyces pombe, Torulaspora sp. Torulaspora delbrueckii, Pichia sp. Pichia anomala, Pichia caribbica, Pseudoxyma sp. Pseudoxyma tsukubaensis

「0009」で発酵させたミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の一つか、またその組み合わせを、エタノール水溶液で蒸留する。  One of Citrus aurantium fruits, branches and leaves, or a combination thereof, which is classified as a citrus family belonging to the genus Rutaceae, which has been fermented by "0009", is distilled with an aqueous ethanol solution.

前項で使用するエタノール水溶液は、水10乃至20%に対してエタノール80乃至90%の割合が好ましい。  The ethanol aqueous solution used in the preceding paragraph preferably has a ratio of 80 to 90% of ethanol to 10 to 20% of water.

「0011」で行う蒸留は、蒸留層に仕込んだエタノール水溶液が、仕込み量の80乃至90%蒸留された時点で終了する。  The distillation performed in “0011” is finished when the aqueous ethanol solution charged in the distillation layer is distilled at 80 to 90% of the preparation amount.

前項の蒸留で残った10乃至20%のエタノール水溶液を、蒸留された蒸留液と混合することで完成とする。  The 10 to 20% aqueous ethanol solution remaining after the distillation of the preceding paragraph is completed by mixing with the distilled distillate.

ミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の一つか、またその組み合わせを、Saccharomyces属のSaccharomyces cerecisiae、Saccharomyces bayanus、Saccharomyces boulardii、Saccharomyces bulderi、Saccharomyces carioanus、Saccharomyces cariocus、Saccharomyces chevalieri、Saccharomyces dairenensis、Saccharomyces ellipsoideus、Saccharomyces florentinus、Saccharomyces kluyveri、Saccharomyces martiniae、Saccharomyces norbensis、Saccharomyces paradoxus、Saccharomyces pastorianus、Saccharomyces spencerorum、Saccharomyces turicensis、Saccharomyces unisporus、Saccharomycesuvarum、Saccharomyces zonatus、Saccharomycopsis属、Candida属のCandida kefyr、Candida bombicola、Candida utilis、Candida saitoana、Zygosaccharomyces属のZygosaccharomyces rouxii、Zygosaccharomyces microellipsoides、Kluyveromyces属、Schizosaccharomyces属のSchizosaccharomyces pombe、Torulaspora属のTorulaspora delbrueckii、Pichia属のPichia anomala、Pichia caribbica、Pseudoxyma属のPseudoxyma tsukubaensis、Endomyces属のうち一つか、また二つ以上の組合せの酵母で発酵させた後、エタノール水溶液で蒸留することで、化粧品、薬用化粧品、加工食品、清涼飲料水、健康補助用食品、健康補助用飲料に安定な状態で配合することのできる素材を得ることができる。  The fruit, branch, leaf, or a combination of Citrus aurantium that is classified as a citrus family Citrus genus Citrus, against the genus Saccharomyces, Saccharomyces cericiaceae, Saccharomyces bayanus, Saccharomyces boulardii, Saccharomyces bulderi, Saccharomyces carigatecich dairenensis, Saccharomyces ellipsoideus, Saccharomyces florentinus, Saccharomyces kluyveri, Sa charomyces martiniae, Saccharomyces norbensis, Saccharomyces paradoxus, Saccharomyces pastorianus, Saccharomyces spencerorum, Saccharomyces turicensis, Saccharomyces unisporus, Saccharomycesuvarum, Saccharomyces zonatus, Saccharomycopsis genus, Candida genus Candida kefyr, Candida bombicola, Candida utilis, Candida saitoana, Zygosaccharomy of Zygosaccharomyces spp. es rouxii, Zygosaccharomyces microellipsoides, Kluyveromyces genus, Schizosaccharomyces pombe of the Schizosaccharomyces genus, Torulaspora delbrueckii of the genus Torulaspora, Pichia nomicala of the Pichia genus, Pichia carib After fermenting with yeast, by distilling with an aqueous ethanol solution, it is possible to obtain a material that can be formulated in a stable state in cosmetics, cosmeceuticals, processed foods, soft drinks, foods for health supplements, and beverages for health supplements. It can be.

ミカン科ミカン属に分類されるCitrus aurantiumなどの柑橘系果実には、ポリメトキシフラボノイドであるノビレチンが含まれている。ノビレチンは、抗アレルギー作用、アポトーシス制御作用、微小循環改善作用、抗酸化作用、認知症予防など、機能性に富んだ成分であり、Citrus aurantiumの果実を使用した素材は化粧品や健康補助用食品に配合することで、多くの機能性が期待できる。  Citrus fruits such as Citrus aurantium, which are classified in the family Rutaceae, include the polymethoxyflavonoid nobiletin. Nobiletin is a highly functional ingredient such as anti-allergic action, apoptosis control action, microcirculation improvement action, antioxidant action, prevention of dementia, etc. The material using Citrus aurantium fruit is for cosmetics and health supplement food By blending, many functionality can be expected.

またミカン科ミカン属に分類されるCitrus aurantiumなどの柑橘系果実には、近年、発見され話題となっているポリメトキシフラボノイドであるスダチチンが含まれている。この成分は、ノビレチンが有する機能性のほか、体重増加抑制作用が確認されており、ミカン科ミカン属に分類されるCitrus aurantiumの果実を使用した素材を清涼飲料水、加工食品、健康補助用食品、健康補助用飲料などに配合することで、更に多くの機能性が期待できる。  Citrus fruits such as Citrus aurantium, which are classified as a citrus family of the genus Citrus, contain sudatitin, which is a polymethoxyflavonoid that has recently been discovered and discussed. This ingredient has confirmed its weight gain suppressive action in addition to the functionality possessed by nobiletin, and it uses the fruit of Citrus aurantium that is classified as a citrus family that belongs to the genus Citrus, which is a soft drink, processed food, food for health supplement By blending it with a health-supporting beverage, more functionality can be expected.

ミカン科ミカン属に分類されるCitrus aurantiumの枝、葉から得られる精油はプチグレンと呼ばれており、リナロール、リモネン、β−ピネン、オシメン、酢酸リナリルなどのモノタエルペンアルコール類が含まれている。  The essential oil obtained from the branches and leaves of Citrus aurantium, which is classified as a citrus family, is called petitegren and includes monotael pen alcohols such as linalool, limonene, β-pinene, osimene, linalyl acetate and the like There is.

前項に記載のプチグレンは、殺菌、清浄作用、皮脂バランスの調整作用、皮膚強壮作用などが確認されており、ミカン科ミカン属に分類されるCitrus aurantiumの枝、葉から得られる精油を化粧品や薬用化粧品に配合することで、肌の清浄化が期待できる。    Puchigren described in the preceding paragraph has been confirmed to have bactericidal activity, cleansing activity, sebum balance adjustment activity, skin tonic activity, etc., and is used for cosmetic and medicinal purposes for essential oils obtained from the branches and leaves of Citrus aurantium that are classified as a citrus family. By blending in cosmetics, it can be expected to clean the skin.

ミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉は、前述のような機能性に優れた成分を含んでいることから、化粧品、薬用化粧品、加工食品、清涼飲料水、健康補助用食品、健康補助用飲料に配合する素材として適している。The fruits, branches and leaves of Citrus aurantium, which is classified as an citrus family, belongs to the genus Citrus and includes the above-mentioned components with excellent functionality. Therefore, it is for cosmetics, cosmeceuticals, processed foods, soft drinks, health support It is suitable as a material to be blended into foods and beverages for health support.

以下、本発明の実施を説明する。  Hereinafter, implementation of the present invention will be described.

ミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の組み合わせをSaccharomyces cerecisiaeで、48時間、遮光条件下、24度で発酵させる。  The fruit, branch and leaf combination of Citrus aurantium, which is classified as a citrus family Citrus genus, is fermented with Saccharomyces cerevisiae for 48 hours at 24 degrees in a lightproof condition.

発酵後のミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉の組み合わせを、80%エタノール水溶液で蒸留する。  The combination of fruit, branch and leaf of Citrus aurantium, which is classified as a citrus family of the family Rutaceae, after fermentation is distilled with 80% aqueous ethanol.

蒸留は、2000ミリリットルの80%エタノール水溶液で行い、蒸留液が1600ミリリットルに到達した時点で、蒸留を止める。  The distillation is carried out with 2000 ml of 80% aqueous ethanol and stops the distillation when the distillate reaches 1600 ml.

蒸留で残った400ミリリットルの残液を、1600ミリリットルの蒸留液と混合して完成とする。  The remaining 400 milliliters of residue is mixed with 1600 milliliters of distillate to complete.

本発明は、化粧品、薬用化粧品、加工食品、清涼飲料水、健康補助用食品、健康補助用飲料を製造する産業で利用される。  The present invention is used in the industry producing cosmetics, cosmeceuticals, processed foods, soft drinks, health supplement foods, health supplement beverages.

Claims (2)

ミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉のうち一つか、またその組み合わせを酵母で発酵させた後、エタノール水溶液で蒸留することで得られる化粧品、薬用化粧品、加工食品、清涼飲料水、健康補助用食品、健康補助用飲料に用いる素材。Citrus aurantium that is classified as a citrus family Citrus aurantium is one of a fruit, a branch and a leaf, or a combination thereof is fermented with yeast and then a cosmetic, a cosmeceutical, a processed food, a refreshing drink obtained by distillation with an aqueous ethanol solution Materials used for drinking water, food for health supplements, and beverages for health supplements. ミカン科ミカン属に分類されるCitrus aurantiumの果実、枝、葉のうち一つか、またその組み合わせを酵母で発酵させた後、エタノール水溶液で蒸留することで得られる素材を配合した化粧品、薬用化粧品、加工食品、清涼飲料水、健康補助用食品、健康補助用飲料。Cosmetics, cosmeceuticals, etc. which are compounded with materials obtained by fermenting with Citrus aurantium fruit, branches, leaves, or one of the combinations of Citrus aurantium, which is classified as a citrus family with the genus Citrus, and with a solution obtained by distilling with ethanol aqueous solution Processed foods, soft drinks, health supplements, health supplements.
JP2017255346A 2017-12-19 2017-12-19 Sour orange derived functional material Pending JP2019108316A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2020193198A (en) * 2019-05-28 2020-12-03 シャネル パフュームズ ビューテ Fermented extract of aerial parts of bitter orange

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2020193198A (en) * 2019-05-28 2020-12-03 シャネル パフュームズ ビューテ Fermented extract of aerial parts of bitter orange
JP7174736B2 (en) 2019-05-28 2022-11-17 シャネル パフュームズ ビューテ Fermented extract of the aerial part of bitter orange

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