JP2018504394A5 - - Google Patents
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- Publication number
- JP2018504394A5 JP2018504394A5 JP2017534608A JP2017534608A JP2018504394A5 JP 2018504394 A5 JP2018504394 A5 JP 2018504394A5 JP 2017534608 A JP2017534608 A JP 2017534608A JP 2017534608 A JP2017534608 A JP 2017534608A JP 2018504394 A5 JP2018504394 A5 JP 2018504394A5
- Authority
- JP
- Japan
- Prior art keywords
- aqueous phase
- organic solvent
- chloride
- carried out
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000008346 aqueous phase Substances 0.000 claims 18
- 238000000034 method Methods 0.000 claims 17
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims 16
- 239000003960 organic solvent Substances 0.000 claims 14
- -1 halide salt Chemical class 0.000 claims 11
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 8
- 239000000203 mixture Substances 0.000 claims 8
- 238000005406 washing Methods 0.000 claims 8
- INTLMJZQCBRQAT-UHFFFAOYSA-K trichloro(octyl)stannane Chemical compound CCCCCCCC[Sn](Cl)(Cl)Cl INTLMJZQCBRQAT-UHFFFAOYSA-K 0.000 claims 4
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 claims 3
- HGQSXVKHVMGQRG-UHFFFAOYSA-N dioctyltin Chemical class CCCCCCCC[Sn]CCCCCCCC HGQSXVKHVMGQRG-UHFFFAOYSA-N 0.000 claims 2
- 239000012074 organic phase Substances 0.000 claims 2
- XMHKTINRBAKEDS-UHFFFAOYSA-N trioctyltin Chemical class CCCCCCCC[Sn](CCCCCCCC)CCCCCCCC XMHKTINRBAKEDS-UHFFFAOYSA-N 0.000 claims 2
- 239000006227 byproduct Substances 0.000 claims 1
- SBOSGIJGEHWBKV-UHFFFAOYSA-L dioctyltin(2+);dichloride Chemical compound CCCCCCCC[Sn](Cl)(Cl)CCCCCCCC SBOSGIJGEHWBKV-UHFFFAOYSA-L 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000012071 phase Substances 0.000 claims 1
- RIECPYZYOLVSJK-UHFFFAOYSA-N tert-butyl 2-dimethylsilyl-5-methylindole-1-carboxylate Chemical compound C[SiH](C)c1cc2cc(C)ccc2n1C(=O)OC(C)(C)C RIECPYZYOLVSJK-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14200184.1 | 2014-12-23 | ||
| EP14200184.1A EP3037425B1 (en) | 2014-12-23 | 2014-12-23 | A process for purifying monooctyltin trichloride |
| PCT/IB2015/001866 WO2016103011A1 (en) | 2014-12-23 | 2015-10-13 | A process for purifying monooctylin trichloride |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2018504394A JP2018504394A (ja) | 2018-02-15 |
| JP2018504394A5 true JP2018504394A5 (enExample) | 2020-04-16 |
| JP6839083B2 JP6839083B2 (ja) | 2021-03-03 |
Family
ID=52338906
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017534608A Active JP6839083B2 (ja) | 2014-12-23 | 2015-10-13 | 三塩化モノオクチルスズを精製する方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10174060B2 (enExample) |
| EP (2) | EP3037425B1 (enExample) |
| JP (1) | JP6839083B2 (enExample) |
| KR (1) | KR102509687B1 (enExample) |
| CN (2) | CN116199710A (enExample) |
| CA (1) | CA2970024A1 (enExample) |
| TW (1) | TWI582102B (enExample) |
| WO (1) | WO2016103011A1 (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11673903B2 (en) | 2018-04-11 | 2023-06-13 | Inpria Corporation | Monoalkyl tin compounds with low polyalkyl contamination, their compositions and methods |
| US10787466B2 (en) | 2018-04-11 | 2020-09-29 | Inpria Corporation | Monoalkyl tin compounds with low polyalkyl contamination, their compositions and methods |
| KR20240129107A (ko) | 2018-06-21 | 2024-08-27 | 인프리아 코포레이션 | 모노알킬 주석 알콕사이드 및 이들의 가수분해 및 축합 생성물의 안정적인 용액 |
| US11966158B2 (en) | 2019-01-30 | 2024-04-23 | Inpria Corporation | Monoalkyl tin trialkoxides and/or monoalkyl tin triamides with low metal contamination and/or particulate contamination, and corresponding methods |
| US11498934B2 (en) | 2019-01-30 | 2022-11-15 | Inpria Corporation | Monoalkyl tin trialkoxides and/or monoalkyl tin triamides with particulate contamination and corresponding methods |
| CN110423248A (zh) * | 2019-08-09 | 2019-11-08 | 南通名泰化工有限公司 | 一种高纯度玻璃热端喷涂液单丁基三氯化锡的制备方法 |
| US12072626B2 (en) | 2021-02-19 | 2024-08-27 | Inpria Corporation | Organometallic radiation patternable coatings with low defectivity and corresponding methods |
| EP4074717A1 (en) * | 2021-04-13 | 2022-10-19 | BNT Chemicals GmbH | Method for cleaving alkyl tin halides |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2718522A (en) * | 1953-06-10 | 1955-09-20 | Metal & Thermit Corp | Recovery of organotin compounds |
| NL276512A (enExample) | 1961-03-28 | 1900-01-01 | ||
| NL302013A (enExample) * | 1962-12-18 | 1900-01-01 | ||
| JPS5915914B2 (ja) * | 1972-04-14 | 1984-04-12 | エム アンド テイ ケミカルス インコ−ポレイテツド | 非対称型トリオルガノスズ・ハライド類の製造方法 |
| DK284875A (da) | 1974-09-19 | 1976-03-20 | Schering Ag | Fremgangsmade til fremstilling af alkyltintrichlorider |
| US4174346A (en) * | 1976-01-30 | 1979-11-13 | Albright & Wilson Limited | Process for preparing organotin compounds |
| JPS5940837B2 (ja) * | 1976-04-13 | 1984-10-03 | 日東化成株式会社 | トリアルキル錫ハライド及びモノアルキル錫トリハライドの製造法 |
| JPS5921873B2 (ja) * | 1980-12-24 | 1984-05-22 | 北興化学工業株式会社 | モノアルキル錫トリハライドの精製法 |
| JPS5921874B2 (ja) * | 1980-12-24 | 1984-05-22 | 北興化学工業株式会社 | モノアルキル錫トリハライドの精製方法 |
| JPS5921875B2 (ja) * | 1980-12-24 | 1984-05-22 | 北興化学工業株式会社 | ジアルキル錫ジハライドの製造法 |
| EP1225177A1 (en) | 2001-01-19 | 2002-07-24 | Atofina Vlissingen B.V. | Process for the production of monoalkyltin trihalides |
| ATE419255T1 (de) | 2002-08-08 | 2009-01-15 | Chemtura Organometallics Gmbh | Verfahren zur herstellung und verwendung von mono-und dialkylzinnhalogeniden |
| EP1743898A1 (en) | 2005-07-12 | 2007-01-17 | Arkema Vlissingen B.V. | Process for the preparation of monoalkyl tin trihalides and dialkyl tin dihalides |
| CN103313996B (zh) * | 2010-07-01 | 2016-06-29 | Pmc有机金属有限公司 | 制备单烷基锡三卤化物和二烷基锡二卤化物的方法 |
-
2014
- 2014-12-23 EP EP14200184.1A patent/EP3037425B1/en active Active
-
2015
- 2015-09-15 TW TW104130479A patent/TWI582102B/zh active
- 2015-10-13 JP JP2017534608A patent/JP6839083B2/ja active Active
- 2015-10-13 CN CN202211654950.7A patent/CN116199710A/zh active Pending
- 2015-10-13 CN CN201580070548.6A patent/CN107207543A/zh active Pending
- 2015-10-13 CA CA2970024A patent/CA2970024A1/en active Pending
- 2015-10-13 EP EP15798178.8A patent/EP3237428A1/en not_active Withdrawn
- 2015-10-13 US US15/538,228 patent/US10174060B2/en active Active
- 2015-10-13 KR KR1020177020395A patent/KR102509687B1/ko active Active
- 2015-10-13 WO PCT/IB2015/001866 patent/WO2016103011A1/en not_active Ceased
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