JP2015530365A5 - - Google Patents
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- Publication number
- JP2015530365A5 JP2015530365A5 JP2015523457A JP2015523457A JP2015530365A5 JP 2015530365 A5 JP2015530365 A5 JP 2015530365A5 JP 2015523457 A JP2015523457 A JP 2015523457A JP 2015523457 A JP2015523457 A JP 2015523457A JP 2015530365 A5 JP2015530365 A5 JP 2015530365A5
- Authority
- JP
- Japan
- Prior art keywords
- silane
- reaction tube
- gas
- gas supply
- reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000006243 chemical reaction Methods 0.000 claims description 48
- -1 alkenyl halide Chemical class 0.000 claims description 27
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 25
- 229910000077 silane Inorganic materials 0.000 claims description 25
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 claims description 18
- 238000004519 manufacturing process Methods 0.000 claims description 11
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 claims description 10
- 239000005052 trichlorosilane Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- 239000000047 product Substances 0.000 claims description 8
- 239000011541 reaction mixture Substances 0.000 claims description 7
- 125000003342 alkenyl group Chemical group 0.000 claims description 5
- 229920002554 vinyl polymer Polymers 0.000 claims description 5
- 229910052736 halogen Inorganic materials 0.000 claims description 4
- 150000002367 halogens Chemical class 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000012043 crude product Substances 0.000 claims description 3
- 150000004756 silanes Chemical class 0.000 claims description 2
- OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical compound ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 claims 2
- SXZSFWHOSHAKMN-UHFFFAOYSA-N 2,3,4,4',5-Pentachlorobiphenyl Chemical compound C1=CC(Cl)=CC=C1C1=CC(Cl)=C(Cl)C(Cl)=C1Cl SXZSFWHOSHAKMN-UHFFFAOYSA-N 0.000 claims 1
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 claims 1
- BHELZAPQIKSEDF-UHFFFAOYSA-N allyl bromide Chemical compound BrCC=C BHELZAPQIKSEDF-UHFFFAOYSA-N 0.000 claims 1
- INLLPKCGLOXCIV-UHFFFAOYSA-N bromoethene Chemical compound BrC=C INLLPKCGLOXCIV-UHFFFAOYSA-N 0.000 claims 1
- VJIYRPVGAZXYBD-UHFFFAOYSA-N dibromosilane Chemical compound Br[SiH2]Br VJIYRPVGAZXYBD-UHFFFAOYSA-N 0.000 claims 1
- MROCJMGDEKINLD-UHFFFAOYSA-N dichlorosilane Chemical compound Cl[SiH2]Cl MROCJMGDEKINLD-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- IBOKZQNMFSHYNQ-UHFFFAOYSA-N tribromosilane Chemical compound Br[SiH](Br)Br IBOKZQNMFSHYNQ-UHFFFAOYSA-N 0.000 claims 1
- 239000007789 gas Substances 0.000 description 22
- GQIUQDDJKHLHTB-UHFFFAOYSA-N trichloro(ethenyl)silane Chemical compound Cl[Si](Cl)(Cl)C=C GQIUQDDJKHLHTB-UHFFFAOYSA-N 0.000 description 8
- 239000005050 vinyl trichlorosilane Substances 0.000 description 8
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000000376 reactant Substances 0.000 description 5
- 239000005049 silicon tetrachloride Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- 239000012495 reaction gas Substances 0.000 description 2
- 238000007086 side reaction Methods 0.000 description 2
- 239000004071 soot Substances 0.000 description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 239000004971 Cross linker Substances 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 239000013462 industrial intermediate Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000001282 organosilanes Chemical class 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- WDVUXWDZTPZIIE-UHFFFAOYSA-N trichloro(2-trichlorosilylethyl)silane Chemical compound Cl[Si](Cl)(Cl)CC[Si](Cl)(Cl)Cl WDVUXWDZTPZIIE-UHFFFAOYSA-N 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102012212915.4A DE102012212915A1 (de) | 2012-07-24 | 2012-07-24 | Verfahren zur Herstellung von Alkenylhalogensilanen und dafür geeigneter Reaktor |
| DE102012212915.4 | 2012-07-24 | ||
| PCT/EP2013/060910 WO2014016014A1 (de) | 2012-07-24 | 2013-05-28 | Verfahren zur herstellung von alkenylhalogensilanen und dafür geeigneter reaktor |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015530365A JP2015530365A (ja) | 2015-10-15 |
| JP2015530365A5 true JP2015530365A5 (enExample) | 2016-07-07 |
| JP6042540B2 JP6042540B2 (ja) | 2016-12-14 |
Family
ID=48534389
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015523457A Expired - Fee Related JP6042540B2 (ja) | 2012-07-24 | 2013-05-28 | アルケニルハロゲンシランの製造方法、及び当該製造方法に適した反応器 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9272258B2 (enExample) |
| EP (1) | EP2877475B1 (enExample) |
| JP (1) | JP6042540B2 (enExample) |
| KR (1) | KR101792923B1 (enExample) |
| BR (1) | BR112015001368A2 (enExample) |
| DE (1) | DE102012212915A1 (enExample) |
| RU (1) | RU2605553C2 (enExample) |
| WO (1) | WO2014016014A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102012212913A1 (de) | 2012-07-24 | 2014-05-15 | Evonik Industries Ag | Verfahren zur Herstellung von Alkenylhalogensilanen und dafür geeigneter Reaktor |
| CN112041324B (zh) * | 2018-05-01 | 2024-03-15 | 美利肯公司 | 生产卤代硅烷化合物的方法 |
| US12479867B2 (en) | 2019-12-13 | 2025-11-25 | Dow Silicones Corporation | Processes for synthesizing unsymmetrical disiloxanes |
| USD959424S1 (en) | 2020-02-26 | 2022-08-02 | Samsung Electronics Co., Ltd. | Mobile telephone |
| CN114797739B (zh) * | 2022-05-27 | 2023-10-13 | 浙江海蓝化工集团有限公司 | 一种管道反应器及其合成物料的方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE530407A (enExample) * | 1953-07-17 | |||
| SU123959A1 (ru) * | 1959-04-02 | 1959-11-30 | Г.В. Одабашян | Способ получени винил- и фенилдихлорсиланов |
| FR2608455B1 (fr) * | 1986-12-23 | 1989-04-28 | Inst Francais Du Petrole | Dispositif d'introduction de gaz comprenant des tubes comportant des zones retreintes |
| DE4001820A1 (de) | 1990-01-23 | 1991-07-25 | Huels Chemische Werke Ag | Reaktor zur herstellung von vinylchlorsilanen durch umsetzung von vinylchlorid mit chlorsilanen bei erhoehter temperatur |
| DE4016021A1 (de) | 1990-05-18 | 1991-11-21 | Huels Chemische Werke Ag | Verfahren zur herstellung von vinyltrichlorsilan |
| DE19727576A1 (de) * | 1996-11-06 | 1998-05-07 | Huels Chemische Werke Ag | Verfahren zur Herstellung von Vinyltrichlorsilan |
| EP0841342B1 (de) * | 1996-11-06 | 2001-11-28 | Degussa AG | Verfahren zur Herstellung von Vinyltrichlorsilan |
| DE19918114C2 (de) | 1999-04-22 | 2002-01-03 | Degussa | Verfahren und Vorrichtung zur Herstellung von Vinylchlorsilanen |
| DE19918115C2 (de) | 1999-04-22 | 2002-01-03 | Degussa | Verfahren zur Herstellung von Vinylchlorsilanen |
| EP1180521B1 (de) * | 2000-08-18 | 2006-07-19 | Degussa AG | Verfahren zur Herstellung von Allyltrichlorsilan |
| JP2002303495A (ja) * | 2001-03-30 | 2002-10-18 | Sumika Plastech Co Ltd | 蓄熱装置 |
| US7741515B2 (en) * | 2004-09-02 | 2010-06-22 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| DE102012212913A1 (de) | 2012-07-24 | 2014-05-15 | Evonik Industries Ag | Verfahren zur Herstellung von Alkenylhalogensilanen und dafür geeigneter Reaktor |
-
2012
- 2012-07-24 DE DE102012212915.4A patent/DE102012212915A1/de not_active Withdrawn
-
2013
- 2013-05-28 JP JP2015523457A patent/JP6042540B2/ja not_active Expired - Fee Related
- 2013-05-28 KR KR1020157003947A patent/KR101792923B1/ko not_active Expired - Fee Related
- 2013-05-28 BR BR112015001368A patent/BR112015001368A2/pt not_active IP Right Cessation
- 2013-05-28 EP EP13725367.0A patent/EP2877475B1/de not_active Not-in-force
- 2013-05-28 WO PCT/EP2013/060910 patent/WO2014016014A1/de not_active Ceased
- 2013-05-28 RU RU2015105915/04A patent/RU2605553C2/ru not_active IP Right Cessation
- 2013-05-28 US US14/416,989 patent/US9272258B2/en not_active Expired - Fee Related
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