JP2013006206A - Method for measuring melt layer thickness of mold powder for continuous casting - Google Patents

Method for measuring melt layer thickness of mold powder for continuous casting Download PDF

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JP2013006206A
JP2013006206A JP2011142016A JP2011142016A JP2013006206A JP 2013006206 A JP2013006206 A JP 2013006206A JP 2011142016 A JP2011142016 A JP 2011142016A JP 2011142016 A JP2011142016 A JP 2011142016A JP 2013006206 A JP2013006206 A JP 2013006206A
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powder
molten
thickness
layer thickness
microwave
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JP5690230B2 (en
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Toshihiko Murakami
敏彦 村上
Yoichi Inoue
陽一 井上
Hayae Kayano
早衛 萱野
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Nippon Steel Corp
Wadeco Co Ltd
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Nippon Steel and Sumitomo Metal Corp
Wadeco Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D2/00Arrangement of indicating or measuring devices, e.g. for temperature or viscosity of the fused mass
    • B22D2/003Arrangement of indicating or measuring devices, e.g. for temperature or viscosity of the fused mass for the level of the molten metal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D11/00Continuous casting of metals, i.e. casting in indefinite lengths
    • B22D11/16Controlling or regulating processes or operations
    • B22D11/18Controlling or regulating processes or operations for pouring
    • B22D11/181Controlling or regulating processes or operations for pouring responsive to molten metal level or slag level
    • B22D11/186Controlling or regulating processes or operations for pouring responsive to molten metal level or slag level by using electric, magnetic, sonic or ultrasonic means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/26Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring variations of capacity or inductance of capacitors or inductors arising from the presence of liquid or fluent solid material in the electric or electromagnetic fields
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/28Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring the variations of parameters of electromagnetic or acoustic waves applied directly to the liquid or fluent solid material
    • G01F23/284Electromagnetic waves

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  • Engineering & Computer Science (AREA)
  • Electromagnetism (AREA)
  • Thermal Sciences (AREA)
  • Fluid Mechanics (AREA)
  • General Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Power Engineering (AREA)
  • Length-Measuring Devices Using Wave Or Particle Radiation (AREA)
  • Continuous Casting (AREA)
  • Measurement Of Levels Of Liquids Or Fluent Solid Materials (AREA)

Abstract

PROBLEM TO BE SOLVED: To enable continuous measuring of a melt layer thickness of a powder when continuous casting.SOLUTION: A method for measuring a melt layer thickness of a mold powder when continuous casting is performed when the reflection of microwaves at an interface between a powder part and a melt layer of a mold powder cannot clearly be obtained. The correlation for a melt layer thickness of the mold powder between a molten steel bath level measurement value L1 obtained according to the reflection of microwaves, which are affected by the average permittivity of the powder part and the melt layer of the mold powder, and the difference between the molten steel bath level measurement value L obtained according to an eddy current sensor, which is unaffected by the average permittivity, ΔL1 (=L1-L), is determined in advance, and the mold powder melt layer thickness is determined on the basis of the correlation that was determined in advance. The melt layer thickness of the powder used for continuous casting can be measured continuously and in favorable accuracy, thereby there is effectiveness for the development of a powder and the operation control/quality control.

Description

本発明は、連続鋳造時、鋳型内に注入された溶鋼の湯面上に投入するモールドパウダー(以下、単にパウダーという。)の溶融層の厚みを、製品品質に影響を及ぼすことなく、精度良く連続的に測定することを可能とする方法に関するものである。   In the present invention, the thickness of the molten layer of mold powder (hereinafter simply referred to as “powder”) to be poured on the molten steel surface poured into the mold during continuous casting can be accurately measured without affecting the product quality. The present invention relates to a method that enables continuous measurement.

鋼の連続鋳造では、溶鋼を鋳型内に注入して鋳型と接触させることで冷却して凝固シェルを生成させ、生成させた凝固シェルを鋳型下方に連続的に引く抜くことで鋳片を製造している。   In continuous casting of steel, molten steel is poured into a mold and brought into contact with the mold to cool it to produce a solidified shell, and the produced solidified shell is drawn continuously below the mold to produce a slab. ing.

この連続鋳造において、鋳型と凝固シェル間の摩擦力低減、ならびに鋳型からの抜熱を制御する目的で鋳型内溶鋼の湯面上に投入されるモールドパウダーが、溶融状態となって鋳型と凝固シェル間の隙間に流入するようにしている。   In this continuous casting, the mold powder put on the molten steel surface in the mold is melted for the purpose of reducing the frictional force between the mold and the solidified shell and controlling the heat removal from the mold. It flows into the gap between them.

すなわち、鋳型内溶鋼の湯面上に投入されたパウダーは、溶鋼湯面上で溶融して厚さ数mm〜十数mmの溶融層を形成する。溶融したパウダーは、鋳型と凝固シェルの間に流入してパウダーフィルムを形成する。このパウダーフィルムのうち、鋳型側の部分は冷やされて凝固し、結晶を晶出もしくは析出しつつ、鋳造の進行に伴って鋳型下方へ移動し、やがて下端から排出される。この排出されるパウダーフィルムの量をパウダー消費量という。   That is, the powder charged on the molten steel surface in the mold is melted on the molten steel surface to form a molten layer having a thickness of several mm to several tens of mm. The molten powder flows between the mold and the solidified shell to form a powder film. The part on the mold side of the powder film is cooled and solidified, crystallizes or precipitates, moves to the lower part of the mold as the casting progresses, and is eventually discharged from the lower end. This amount of discharged powder film is called powder consumption.

従って、連続鋳造に際しては、前記パウダー消費量分のパウダーを新たに追加投入する必要がある。   Therefore, in continuous casting, it is necessary to newly add powder corresponding to the powder consumption.

ところで、近年、多種多様な鋳造鋼種に対応すべく、パウダーの開発がなされているが、鋳型内溶鋼からの浮上酸化物ならびに鋳造鋼種成分により溶融パウダーの物性が変化する場合がある。   By the way, in recent years, powders have been developed to cope with a wide variety of cast steel types. However, the physical properties of the molten powder may change depending on the floating oxide from the molten steel in the mold and the cast steel type components.

この溶融パウダー物性の変化は、前記パウダー溶融層の厚み(以下、パウダー溶融層厚みという。)やパウダー消費量に影響するため、パウダー溶融層厚みを連続的に計測し調整することは、連続鋳造操業の安定に繋がる。そこで、パウダー溶融層厚みを計測する方法が各種提案されている。   This change in physical properties of the molten powder affects the thickness of the powder molten layer (hereinafter referred to as the powder molten layer thickness) and the amount of powder consumed. This leads to stable operation. Therefore, various methods for measuring the powder melt layer thickness have been proposed.

このパウダー溶融層厚みを測定する方法として、浸漬した検尺棒の溶損量から測定するバッチ測定(非連続測定)や、この検尺棒による測定を連続的に行えるよう様にした方法(例えば特許文献1)がある。また、複数の各周波数における位相と絶対値の双方を用いてパウダー溶融層厚みを計測する多周波渦流式の方法(例えば特許文献2,3)も提案されている。   As a method for measuring the powder melt layer thickness, batch measurement (non-continuous measurement) for measuring from the amount of erosion of the immersed measuring bar, or a method that enables continuous measurement with this measuring bar (for example, There exists patent document 1). In addition, a multi-frequency eddy current method (for example, Patent Documents 2 and 3) that measures the powder melt layer thickness using both the phase and the absolute value at each of a plurality of frequencies has been proposed.

しかしながら、検尺棒を用いた測定は、パウダー融点で溶融しない鉄棒又は鉄部と、溶融する例えばアルミニウム棒又はアルミニウム部の溶融差をパウダー溶融層厚みとするため、低融点のパウダーの場合は測定が難しい。さらに、検尺棒を用いた測定を連続的に実施する場合、溶融したアルミニウムが溶鋼中に溶解していくので、不純物を製品に添加することになって実用に際しては問題がある。   However, the measurement using a measuring bar is measured in the case of a low melting point powder because the melting difference between the iron bar or iron part that does not melt at the powder melting point and the melting point, for example, the aluminum bar or aluminum part, is the powder melt layer thickness. Is difficult. Further, when the measurement using the measuring bar is continuously performed, the molten aluminum is dissolved in the molten steel, so that there is a problem in practical use because impurities are added to the product.

一方、多周波渦流式は、パウダー層の種類、溶鋼の湯面温度によって計測誤差が大きくなったり、製造する鋳片の厚みが狭くなると計測精度が悪くなる。また、オシレーションの振動パターンによっては計測データがばらつく場合がある。   On the other hand, in the multi-frequency eddy current method, the measurement accuracy becomes worse when the measurement error becomes large or the thickness of the slab to be manufactured becomes narrow depending on the kind of the powder layer and the molten steel surface temperature. In addition, measurement data may vary depending on the vibration pattern of oscillation.

そこで、多周波渦流式の問題点を改良した方法が特許文献4で提案されている。この特許文献4で提案された方法は、パウダー溶融層の温度変化による導電率変化を校正してパウダー溶融層厚み測定値の高精度化を図るべく、以下の4つの工程を備えることを特徴としている。   Therefore, Patent Document 4 proposes a method for improving the problems of the multi-frequency eddy current method. The method proposed in Patent Document 4 includes the following four steps in order to calibrate the change in conductivity due to the temperature change of the powder melt layer and to increase the accuracy of the measured value of the powder melt layer thickness. Yes.

・計測前に校正データの収集を行う校正データ収集工程
・位相情報と絶対値情報を得る計測データ収集工程
・計測データ収集工程で収集した計測データを補正する補正工程
・補正工程にて補正したデータに基づきパウダー溶融層厚みを演算する演算工程
-Calibration data collection process for collecting calibration data before measurement-Measurement data collection process for obtaining phase information and absolute value information-Correction process for correcting measurement data collected in the measurement data collection process-Data corrected in the correction process Calculation process to calculate powder melt layer thickness based on

しかしながら、特許文献4で提案された方法も、大型のために小断面鋳型への適用が難しい多周波渦流式センサーを使用することに変わりはなく、さらに多周波渦流式センサーは装置本体が高価であることなどから、実用に際しては課題がある。また、多周波渦流式は、溶融金属とパウダー溶融層面を測定(分離)する方法で、パウダー層 全体の厚みを計測することが出来ないため、パウダー全体の層厚みの把握が出来ないという欠点もある。   However, the method proposed in Patent Document 4 still uses a multi-frequency eddy current sensor that is difficult to apply to a small-section mold due to its large size, and the multi-frequency eddy current sensor is expensive in its main body. There is a problem in practical use because of the facts. In addition, the multi-frequency eddy current method is a method of measuring (separating) the molten metal and the powder molten layer surface, and the thickness of the entire powder layer cannot be measured. is there.

特開平9−79805号公報Japanese Patent Laid-Open No. 9-79805 特開2005−221282号公報JP 2005-221282 A 特開2006−205227号公報JP 2006-205227 A 特開2007−21529号公報JP 2007-21529 A

本発明が解決しようとする問題点は、鋼の連続鋳造時に、製品品質に影響を及ぼすことなく、パウダー溶融層厚みを精度良く、連続的に測定する方法は、現時点では確立されていないという点である。   The problem to be solved by the present invention is that, at the time of continuous casting of steel, the method for continuously measuring the powder melt layer thickness accurately without affecting the product quality has not been established. It is.

本発明の連続鋳造用パウダーの溶融層厚測定方法は、
連続鋳造時におけるパウダー溶融層厚みの測定を連続的に可能とするために、
例えばパウダーの粉体部分と溶融層の界面でのマイクロ波の反射が明瞭に得られない場合における、連続鋳造時のパウダー溶融層厚み測定方法であって、
前記パウダーの粉体部分と溶融層の各々の平均誘電率の影響を受けるマイクロ波の反射による溶鋼の湯面レベル測定値L1と、前記平均誘電率の影響を受けない渦流センサーによる溶鋼の湯面レベル測定値Lの差ΔL1(=L1−L)と、パウダーの溶融層厚みの相関を予め求めておき、
この予め求めておいた相関に基づいて、パウダー溶融層厚みを得ることを最も主要な特徴としている。
The method for measuring the molten layer thickness of the continuous casting powder of the present invention is as follows.
To enable continuous measurement of powder melt layer thickness during continuous casting,
For example, a method for measuring the thickness of a molten powder layer during continuous casting when the reflection of microwaves at the interface between the powder portion and the molten layer cannot be clearly obtained,
Molten steel surface level measurement value L1 due to microwave reflection affected by the average dielectric constant of the powder part and molten layer of the powder, and the molten steel surface level by the eddy current sensor not affected by the average dielectric constant The correlation between the difference ΔL1 (= L1−L) in the level measurement value L and the molten layer thickness of the powder is obtained in advance,
Based on the correlation obtained in advance, the most important feature is to obtain the powder melt layer thickness.

上記の本発明では、予め求めておいた、マイクロ波の反射による溶鋼の湯面レベル測定値L1と、渦流センサーによる溶鋼の湯面レベル測定値Lの差ΔL1と、パウダーの溶融層厚みの相関に基づき、パウダー溶融層厚みを得ることで、パウダーの溶融層の厚みを連続的に精度良く測定できる。   In the present invention described above, the correlation between the molten metal level measurement value L1 of the molten steel by microwave reflection, the difference ΔL1 of the molten steel level level L measured by the eddy current sensor, and the molten layer thickness of the powder obtained in advance. Based on the above, by obtaining the thickness of the powder melt layer, the thickness of the powder melt layer can be continuously and accurately measured.

本発明は、連続鋳造に用いるパウダーの溶融層の厚みを連続的に精度良く測定することが出来るので、パウダー開発ならびに操業管理・品質管理に効果があり、連続鋳造技術開発に対し、技術的に価値の高い発明である。   Since the present invention can continuously and accurately measure the thickness of the powder melt layer used for continuous casting, it is effective for powder development, operation management and quality control. It is a highly valuable invention.

パウダー厚み測定試験装置の概念図である。It is a conceptual diagram of a powder thickness measurement test apparatus. 中心周波数が20GHzで、変調振幅が4GHzのマイクロ波を用いて、パウダー厚みを測定した結果の一例を示した図である。It is the figure which showed an example of the result of having measured the powder thickness using the microwave whose center frequency is 20 GHz and whose modulation amplitude is 4 GHz. 中心周波数が32GHzで、変調振幅が8GHzのマイクロ波を用いて、厚み40mmのパウダーを測定した結果の一例を示した図である。It is the figure which showed an example of the result of having measured the powder of thickness 40mm using the microwave whose center frequency is 32GHz and whose modulation amplitude is 8GHz. 中心周波数が32GHzで、変調振幅が8GHzのマイクロ波を用いたパウダー厚み測定結果の一例を示した図である。It is the figure which showed an example of the powder thickness measurement result using the microwave whose center frequency is 32 GHz and whose modulation amplitude is 8 GHz. 請求項1に係る発明のパウダー溶融層厚みの測定原理を説明した図である。It is a figure explaining the measurement principle of the powder fusion layer thickness of the invention which concerns on Claim 1. マイクロ波を用いたパウダー層厚の校正結果を示した図である。It is the figure which showed the calibration result of the powder layer thickness using a microwave. 請求項2に係る発明のパウダー溶融層厚みの測定原理を説明した図である。It is a figure explaining the measurement principle of the powder fusion layer thickness of the invention concerning Claim 2. パウダー溶融層厚みとマイクロ波指示値の関係を示した図である。It is the figure which showed the relationship between powder molten layer thickness and a microwave instruction | indication value. 粉体のパウダーとパウダー溶融層の誘電率差が大きい場合の、マイクロ波を用いた測定データ例である。It is an example of measurement data using microwaves when the dielectric constant difference between the powder of powder and the powder melt layer is large.

本発明では、連続鋳造時におけるパウダー溶融層厚みの測定を連続的に可能とするという目的を、例えば、予め求めておいた、マイクロ波の反射による溶鋼の湯面レベル測定値L1と、渦流センサーによる溶鋼の湯面レベル測定値Lの差ΔL1と、パウダーの溶融層厚みの相関に基づき、パウダー溶融層厚みを得ることで実現した。   In the present invention, for the purpose of continuously enabling measurement of the thickness of the powder melt layer during continuous casting, for example, a molten steel surface level measurement value L1 obtained by microwave reflection obtained in advance and an eddy current sensor are obtained. This was realized by obtaining the powder melt layer thickness based on the correlation between the difference ΔL1 of the molten steel surface level measured value L and the melt layer thickness of the powder.

以下、本発明を実施するための形態について、添付図面を用いて説明する。
先ず、本発明の新しい着想から課題解決に至るまでの経過について説明する。
Hereinafter, embodiments for carrying out the present invention will be described with reference to the accompanying drawings.
First, the process from the new idea of the present invention to the solution of the problem will be described.

鋼の連続鋳造時におけるパウダー溶融層厚み、及び投入したパウダー全体の層厚み(以下、パウダー投入厚みという。)の管理は、従来から操業管理の重要な因子である。特にパウダー溶融層厚みの定量的な把握は、近年、多種多様な鋳造鋼種対応において、パウダー開発の重要な管理ファクターであった。   Management of the thickness of the molten powder layer during continuous casting of steel and the thickness of the entire charged powder (hereinafter referred to as “powder charged thickness”) has been an important factor in operation management. In particular, quantitative determination of the thickness of the powder melt layer has recently been an important management factor for powder development in dealing with a wide variety of cast steel types.

しかしながら、従来は、連続鋳造中に安定してパウダー溶融層厚みを測定する方法がなく、検尺棒を用いて非連続的に測定する方法が用いられていた。多周波渦流式によるパウダー溶融層厚みの測定方法も提案されているが、先に説明した問題点を有するために、現状では実用化されていない。   However, conventionally, there is no method for measuring the thickness of the powder melt layer stably during continuous casting, and a method for measuring discontinuously using a measuring bar has been used. A method for measuring the thickness of the powder melt layer by a multi-frequency eddy current method has also been proposed, but it has not been put into practical use at present because of the problems described above.

そこで、発明者らは、粉体及び固体の界面を測定する方法として実用化されているマイクロ波は、空気中での温度変化に影響されず、さらに金属は透過せずに非金属物体を透過する特性があるため、粉体のパウダー表面(以下、パウダー投入界面という。)と、溶鋼湯面(以下、溶鋼界面という。)で反射して二つの界面の分離が可能であると考えた。なお、転炉内スラグのレベル測定などに実用化されていてスラグ表面を測定する目的で従来から用いられている汎用マイクロ波は、中心周波数は10GHz近傍、変調振幅は2GHz程度のものが一般的である。   Therefore, the inventors have put microwaves in practical use as a method for measuring the interface between powders and solids, and are not affected by temperature changes in the air. Therefore, it was considered that the two interfaces could be separated by reflecting on the powder surface of the powder (hereinafter referred to as the powder input interface) and the molten steel surface (hereinafter referred to as the molten steel interface). In general, general-purpose microwaves that have been put to practical use for measuring the level of slag in converters and that have been used for the purpose of measuring the slag surface generally have a center frequency of around 10 GHz and a modulation amplitude of about 2 GHz. It is.

また、連続鋳造時におけるパウダー溶融層厚みは、通常、十数mmである。従って、発明者らは、本発明の目的とする、パウダー溶融層厚み及びパウダー投入厚みを測定するために必要な、パウダー溶融層厚みが十数mmの場合に、パウダー投入界面と溶鋼界面の、二つの界面の測定(分離)が可能かどうかを確認するためのラボ試験を実施した。   Further, the thickness of the powder melt layer during continuous casting is usually a few tens of millimeters. Therefore, the inventors of the present invention, for the purpose of the present invention, required to measure the powder melt layer thickness and the powder input thickness, when the powder melt layer thickness is more than a dozen mm, between the powder input interface and the molten steel interface, A laboratory test was conducted to confirm whether the measurement (separation) of the two interfaces was possible.

先ず、中心周波数が20GHz、変調振幅が4GHzのマイクロ波を用いて、鋳型内溶鋼湯面上へのパウダー(粉体)投入後の厚みを変化させ、パウダー投入量と投入底面の測定指示値の変化を調査した。その結果、パウダー投入量と投入底面指示値に相関があり、パウダーの誘電率の影響を受けて投入パウダー全体層厚みと線形な関係にあることを見出した。   First, using a microwave with a center frequency of 20 GHz and a modulation amplitude of 4 GHz, the thickness after the powder (powder) is placed on the molten steel surface in the mold is changed, and the amount of powder input and the measurement indication value of the bottom of the input are determined. The change was investigated. As a result, it was found that there is a correlation between the amount of powder input and the indicated value at the bottom of the input, and there is a linear relationship with the total thickness of the input powder under the influence of the dielectric constant of the powder.

ここで、投入底面指示値とは、測定器から溶鋼界面(=溶鋼湯面)までの距離をいう。また、変調振幅とは、マイクロ波の中心周波数からの変動周波数幅を意味する。   Here, the input bottom surface instruction value refers to the distance from the measuring instrument to the molten steel interface (= molten steel surface). The modulation amplitude means a fluctuation frequency width from the center frequency of the microwave.

パウダーの投入量によって投入底面指示値が変化するのは、マイクロ波がパウダーを透過するときにパウダーの誘電率に影響されるためである。   The reason why the input bottom surface indication value changes depending on the amount of powder input is that the microwave is affected by the dielectric constant of the powder when it passes through the powder.

そこで、発明者らは、パウダー投入厚みによる投入底面指示値の変化を事前に測定しておけば、検量データを用いて補正することで、連続的にパウダー溶融層厚みの変化を測定できると考えた。   Therefore, the inventors believe that if the change in the input bottom surface indication value due to the powder input thickness is measured in advance, the change in the powder melt layer thickness can be continuously measured by correcting using the calibration data. It was.

しかしながら、前記マイクロ波は波長が十数mmと長く距離測定精度が悪いために、本発明で目的とするパウダー溶融層厚みやパウダー投入界面などの十数cmの範囲内での測定の場合、測定精度ならびにパウダー投入界面での反射波を安定して得ることが難しかった。   However, since the microwave has a wavelength as long as several tens of millimeters and the distance measurement accuracy is poor, the measurement is performed in the case of measurement within a range of tens of centimeters such as the thickness of the powder melt layer and the powder injection interface intended in the present invention It was difficult to obtain accurate and stable reflected waves at the powder injection interface.

そこで、発明者らは、パウダー投入界面と溶鋼界面の二つの界面の測定(分離)のさらなる精度向上を図るには、マイクロ波の波長を前記マイクロ波よりも短い数mmにすること、さらに変調振幅を大きくすることが有効であると考えた。   In order to further improve the accuracy of measurement (separation) of the two interfaces of the powder injection interface and the molten steel interface, the inventors set the wavelength of the microwave to a few millimeters shorter than the microwave, and further modulated it. We thought that increasing the amplitude would be effective.

マイクロ波を用いて距離を正確に測定するのは、一般的にFMCW(Frequency Modulation Continuous Wave)方式が有効とされていて、今回のマイクロ波も本方式を採用している。   The FMCW (Frequency Modulation Continuous Wave) method is generally effective for accurately measuring the distance using the microwave, and this microwave also adopts this method.

FMCW方式は、マイクロ波に周波数変調を連続的に行う方式で、変調振幅と中心周波数が重要である。中心周波数の増加によるメリットは、マイクロ波波長を短くする方向に作用することにあり、また、変調振幅を大きくすると、マイクロ波反射の遅れを分離しやすく、距離の測定精度向上に繋がることが知られている。   The FMCW method is a method in which frequency modulation is continuously performed on a microwave, and modulation amplitude and center frequency are important. The advantage of increasing the center frequency is that it works in the direction of shortening the microwave wavelength, and increasing the modulation amplitude makes it easier to separate the delay in microwave reflection, leading to improved distance measurement accuracy. It has been.

発明者らは、さらなる距離測定精度の向上を図るべく、中心周波数を、20GHzの前記マイクロ波よりも増加した32GHzのマイクロ波を用い、変調振幅を変化させて、中心周波数が20GHzの前記マイクロ波を用いた場合と同様の試験を実施した。   In order to further improve the distance measurement accuracy, the inventors use a 32 GHz microwave whose center frequency is increased from the 20 GHz microwave, and changes the modulation amplitude to change the microwave having the center frequency of 20 GHz. The same test as in the case of using was performed.

その結果、変調振幅を、4GHzの前記マイクロ波よりも大きい8GHzとすることで、目標とするパウダー投入界面と溶鋼界面の二つの界面の分離測定を、パウダー投入厚みが15mmから可能であることを見出した。   As a result, by setting the modulation amplitude to 8 GHz, which is larger than the microwave of 4 GHz, it is possible to measure the separation between the target powder input interface and the molten steel interface from a powder input thickness of 15 mm. I found it.

本発明は上記の知見に基づいて成されたものである。
以下、請求項1に係る発明の連続鋳造用パウダーの溶融層厚み測定方法について説明する。
発明者らは、図1に示す試験装置を使用してパウダー投入厚みとマイクロ波出力値変化の関係を調査した。なお、マイクロ波出力値とは、パウダーの表面や図1の試験装置を構成する箱の底面で反射した反射波の形状、強度、及び帰還時間を言う。
The present invention has been made based on the above findings.
Hereinafter, the method for measuring the melt layer thickness of the powder for continuous casting according to the first aspect of the present invention will be described.
The inventors investigated the relationship between the powder input thickness and the change in microwave output value using the test apparatus shown in FIG. The microwave output value refers to the shape, intensity, and feedback time of the reflected wave reflected from the powder surface and the bottom surface of the box constituting the test apparatus of FIG.

図1中の1は、箱4に装入した粉体のパウダー5に向けてマイクロ波を照射し、パウダー5を透過して箱4の底面で反射したマイクロ波を受信する照射・受信器で、受信用のアンテナ1aを有している。このアンテナ1aで受信されたマイクロ波は、照射・受信器1から信号増幅用のアンプ2を介してデータ収集用PC3に送られる。   Reference numeral 1 in FIG. 1 denotes an irradiation / receiver that irradiates the microwave toward the powder 5 of the powder charged in the box 4 and receives the microwave transmitted through the powder 5 and reflected from the bottom surface of the box 4. The receiving antenna 1a is provided. The microwave received by the antenna 1a is sent from the irradiation / receiver 1 to the data collection PC 3 through the signal amplification amplifier 2.

なお、照射・受信器1から照射されたマイクロ波の一部は、パウダー5の表面(パウダー投入界面)で反射される。   A part of the microwave irradiated from the irradiation / receiver 1 is reflected on the surface of the powder 5 (powder input interface).

前記図1の試験装置を使用した試験においては、パウダー5とパウダー溶融層の界面は箱4の底面と近接しているが、実操業における溶鋼界面に相当する箱4の底面での反射波が最も大きい。   In the test using the test apparatus of FIG. 1, the interface between the powder 5 and the powder molten layer is close to the bottom surface of the box 4, but the reflected wave at the bottom surface of the box 4 corresponding to the molten steel interface in actual operation is generated. The biggest.

従って、この箱4の底面での反射波が、パウダーの有無によって明確な差が生じ、パウダーの厚み変化に対して線形に変化していれば、オフラインでパウダー溶融状態のマイクロ波出力値の変化を測定して校正することで、連続してパウダー溶融層をモニターできることになる。   Therefore, if the reflected wave at the bottom surface of the box 4 has a clear difference depending on the presence or absence of powder and changes linearly with respect to the change in the thickness of the powder, the change in the microwave output value in the powder melting state offline. By measuring and calibrating, the powder melt layer can be monitored continuously.

そこで、発明者らは、第1段階の試験として、図1の装置を使用した試験において、箱4に装入するパウダー5の厚みだけを変化させ、マイクロ波出力値が粉体のパウダーの誘電率の影響を受けてどのように変化するかについて調査した。その結果、両者は線形に変化する知見を得た。   Therefore, as a first stage test, the inventors changed only the thickness of the powder 5 charged in the box 4 in the test using the apparatus of FIG. We investigated how it changed under the influence of the rate. As a result, both obtained the knowledge which changes linearly.

次に、第2段階の試験として、粉体より密度が高い溶融状態のパウダーを模擬するために、パウダーを一旦溶解して凝固させた試料を粉体のパウダーとの間に挟み、パウダー溶融層を模擬した多層(粉体+固体)状態で、同様の試験を実施した。   Next, as a second stage test, in order to simulate a molten powder having a higher density than the powder, the powder once melted and solidified is sandwiched between the powder and the powder melt layer. The same test was performed in a multilayer (powder + solid) state simulating

その結果、溶融凝固後のパウダーの誘電率は、粉体状態のパウダーの誘電率よりも大きいので、マイクロ波出力値に大きな差を生じることを確認し、今回の原理で測定が可能であることが判明した。   As a result, the dielectric constant of the powder after melting and solidification is larger than the dielectric constant of the powder in the powder state. Therefore, it was confirmed that a large difference in the microwave output value was produced, and measurement was possible using this principle. There was found.

しかしながら、実操業においては、パウダー溶融層の表面でのマイクロ波の反射は、溶鋼界面と近似していて、溶鋼界面の反射に吸収される懸念があり、明瞭に区別できないことが予想される。   However, in actual operation, the reflection of microwaves on the surface of the powder molten layer is close to the molten steel interface, and there is a concern that the reflection is reflected by the reflection of the molten steel interface, so that it is expected that it cannot be clearly distinguished.

そこで、これに対する対策として、発明者らは、溶鋼界面は、金属面での反射なので、粉体のパウダーとパウダー溶融層を通過したマイクロ波は、安定した反射(マイクロ波出力)が得られることを利用してパウダー溶融層厚みを換算する、以下の本発明の原理を思いつくに至った。   Therefore, as countermeasures against this, since the molten steel interface is a reflection on the metal surface, the inventors are able to obtain a stable reflection (microwave output) for the microwave passing through the powder powder and the molten powder layer. The following principle of the present invention has been conceived in which the powder melt layer thickness is converted by using.

つまり、本発明の原理では、パウダーとパウダー溶融層を通過したマイクロ波は、空気中を透過したマイクロ波ではないため、粉体のパウダーとパウダー溶融層の平均誘電率の影響を受けて、マイクロ波出力値が大きくなる。すなわち、マイクロ波としては反射が遅れて見掛け上距離が大きくなる出力となる。従って、この大きな距離となったマイクロ波出力値と例えば従来の検尺棒を用いて測定した実際のパウダー溶融層厚みの関係の校正値をデータとして持っておくことで、パウダー溶融層厚みを換算できることになる。   In other words, in the principle of the present invention, the microwave that has passed through the powder and the powder melt layer is not the microwave that has passed through the air, and therefore the microwave is affected by the average dielectric constant of the powder powder and the powder melt layer. Wave output value increases. That is, the output of the microwave is delayed and reflected to increase the apparent distance. Therefore, the powder melted layer thickness can be converted by holding the calibration value of the relationship between the microwave output value that has become this large distance and the actual powder melted layer thickness measured using, for example, a conventional measuring rod. It will be possible.

実操業における溶鋼界面からの反射波は、パウダーの誘電率の影響を受けた反射波になるので、この溶鋼界面とパウダー投入界面との測定(分離)が出来れば、パウダー溶融層表面でのマイクロ波の反射がなくても精度良くパウダー溶融層厚みを推定することができる。   The reflected wave from the molten steel interface in actual operation becomes a reflected wave affected by the dielectric constant of the powder, so if measurement (separation) between the molten steel interface and the powder injection interface is possible, the micro wave on the surface of the powder molten layer Even if there is no wave reflection, the powder melt layer thickness can be accurately estimated.

なお、金属面の反射は、溶鋼と固体でも変化しないため、鋳型内のメニスカス(溶鋼界面)として、確認した。   In addition, since the reflection of a metal surface does not change with molten steel and solid, it confirmed as the meniscus (molten steel interface) in a casting_mold | template.

従って、先ず、熱間試験、例えばタンマン炉(小型の試験炉)を用いてパウダーを溶融させ、実際のパウダー粉体厚みとパウダー溶融層厚みを従来の検尺棒で測定し、予め溶鋼界面、パウダー投入界面などの多点を測定した際のマイクロ波出力値との校正を行う。   Therefore, first, the powder is melted using a hot test, for example, a Tamman furnace (small test furnace), the actual powder powder thickness and the powder melt layer thickness are measured with a conventional measuring rod, and the molten steel interface, Calibration with the microwave output value when measuring multiple points such as the powder injection interface.

そして、マイクロ波を用いて測定した溶鋼界面からパウダー投入界面を減算して求めたパウダー投入厚み(紛体のパウダーとパウダー溶融層の誘電率の影響を受けて生じた差を含んでいる)を、例えば従来の検尺棒等で測定した実際のパウダー溶融層厚みによって校正し、検量線を求めておく。   And the powder input thickness obtained by subtracting the powder input interface from the molten steel interface measured using microwave (including the difference caused by the dielectric constant of the powder powder and the powder melt layer), For example, a calibration curve is obtained by calibrating with the actual powder melt layer thickness measured with a conventional measuring rod or the like.

実機の連続鋳造では、鋳型内の溶鋼界面(鋳型内溶鋼湯面、メニスカスとも言う。)の真の値は、通常の操業の流動制御に使われている渦流センサーで常時監視している。従って、渦流センサーで測定した溶鋼界面の真の値と、マイクロ波を用いて測定した溶鋼界面の測定値との差(ズレ)が、粉体のパウダーとパウダー溶融層の誘電率の影響を受けて生じた差(ズレ)であるので、事前に調査した前記検量線から、パウダー溶融層厚みを推算するのである。   In actual continuous casting, the true value of the molten steel interface in the mold (also referred to as molten steel surface in the mold, also called meniscus) is constantly monitored by eddy current sensors used for flow control in normal operations. Therefore, the difference between the true value of the molten steel interface measured by the eddy current sensor and the measured value of the molten steel interface measured using microwaves is affected by the dielectric constant of the powder powder and the powder molten layer. Therefore, the powder melt layer thickness is estimated from the calibration curve examined in advance.

発明者らは、上記方法に使用するマイクロ波の好適な条件を見出すべく、先ず初めに、中心周波数が20GHz、変調振幅が4GHzのマイクロ波を用いて、下記表1に示す主要成分値のパウダー厚みとマイクロ波出力値の関係を調査した。その結果を図2に示す。   In order to find out suitable conditions for the microwave used in the above method, the inventors first used a microwave having a center frequency of 20 GHz and a modulation amplitude of 4 GHz, and used the powders having the main component values shown in Table 1 below. The relationship between thickness and microwave output value was investigated. The result is shown in FIG.

Figure 2013006206
Figure 2013006206

図2における測定距離は、図1に示したアンテナ1aの根元(アンテナ導波管の細い方)から、パウダー表面及び箱の底面までの測定距離を示したものである。箱の底面は、パウダー投入厚みが増加すると誘電率の影響を多くうけて、見掛けの距離が離れたように出力される。一方、パウダー表面であるパウダー投入界面は、パウダー投入厚みが増えるとアンテナ1aとの距離が近づくので、測定距離が小さくなる。   The measurement distance in FIG. 2 indicates the measurement distance from the base of the antenna 1a shown in FIG. 1 (the narrower side of the antenna waveguide) to the powder surface and the bottom of the box. The bottom surface of the box is output as if the apparent distance is increased due to the greater influence of the dielectric constant when the powder input thickness increases. On the other hand, the powder input interface which is the powder surface becomes closer to the antenna 1a as the powder input thickness increases, so the measurement distance becomes smaller.

また、パウダー投入界面と溶鋼界面となる箱の底面の二つの界面の分離測定が可能であるかどうかを調査した結果、測定対象面までの測定距離はパウダー投入厚みの変化にほぼ線形に変化していた。   In addition, as a result of investigating whether it is possible to separate and measure the two interfaces of the bottom of the box, which is the powder input interface and the molten steel interface, the measurement distance to the measurement target surface changes almost linearly with the change of the powder input thickness. It was.

このように、中心周波数が20GHz、変調振幅が4GHzのマイクロ波を使用した測定では、パウダー投入厚みと箱の底面の指示値(図2の▲印)に相関があることが判明した。   As described above, in the measurement using the microwave having the center frequency of 20 GHz and the modulation amplitude of 4 GHz, it has been found that there is a correlation between the powder input thickness and the indicated value on the bottom surface of the box (marked with ▲ in FIG. 2).

一方、パウダー表面(図2の■印)については、パウダー投入厚みが50mmの場合は反射波が不明瞭で、100mmの場合は反射波がなく、150mmの場合のみ明確な反射波が確認された。   On the other hand, with respect to the powder surface (marked with ■ in FIG. 2), the reflected wave was unclear when the powder thrown thickness was 50 mm, there was no reflected wave when 100 mm, and a clear reflected wave was confirmed only when the thickness was 150 mm. .

本発明で目標とするマイクロ波によるパウダーの上記の二つの界面の測定(分離)を行うためには、パウダー投入厚みが100mm以下での精度が必要である。   In order to measure (separate) the above-mentioned two interfaces of the powder by microwaves, which is a target in the present invention, it is necessary to have an accuracy when the powder input thickness is 100 mm or less.

さらに精度の良い測定を行うためには、パウダー投入界面(パウダー表面)に加えて、溶鋼界面(箱の底面)の二つの測定値を得ることが重要なので、さらなる、精度向上試験として中心周波数が32GHz、変調振幅が8GHzのマイクロ波を用いて、同様の試験を実施した。その結果を図4に示す。   In order to perform measurements with higher accuracy, it is important to obtain two measured values for the molten steel interface (bottom of the box) in addition to the powder input interface (powder surface). A similar test was performed using a microwave of 32 GHz and a modulation amplitude of 8 GHz. The result is shown in FIG.

図3は、パウダー厚みが40mmの場合における、箱の底面とパウダー表面の二つの界面からの反射波を示すデータの一例で、縦軸がマイクロ波反射波のスペクトルを示し、パウダー表面と箱の底面に相当する距離換算スペクトルにピーク値が出力されていることが読み取れる。   FIG. 3 is an example of data showing the reflected waves from the two interfaces between the bottom surface of the box and the powder surface when the powder thickness is 40 mm, and the vertical axis shows the spectrum of the microwave reflected wave, It can be seen that the peak value is output in the distance conversion spectrum corresponding to the bottom surface.

また、前述の中心周波数が20GHz、変調振幅が4GHzのマイクロ波を用いた試験では、図2に示したように、パウダー投入厚みは100mm以下の場合の測定ができずに、パウダー投入界面と溶鋼界面の二つの界面の測定(分離)ができなかった。   Further, in the test using the microwave having the center frequency of 20 GHz and the modulation amplitude of 4 GHz as described above, as shown in FIG. It was not possible to measure (separate) two interfaces.

しかしながら、中心周波数が32GHz、変調振幅が8GHzのマイクロ波を使用した場合は、図4に示すように、パウダー投入厚みが15mmから、パウダー表面、箱の底面共に線形に変化し、パウダー投入界面と溶鋼界面の二つの界面の分離測定が可能であった。   However, when a microwave having a center frequency of 32 GHz and a modulation amplitude of 8 GHz is used, as shown in FIG. 4, the powder input thickness changes from 15 mm to both the powder surface and the bottom of the box, and the powder input interface The separation measurement of the two interfaces of the molten steel interface was possible.

実操業を考えた場合、パウダー投入厚みが15mm以下ということはほとんど無いため、今回の発明範囲は連続鋳造操業の中で、十分適用可能な範囲と考えられる。従って、発明者らは、パウダー溶融層厚み測定への応用展開について考えた。   Considering the actual operation, since the powder input thickness is hardly 15 mm or less, the scope of the present invention is considered to be a sufficiently applicable range in the continuous casting operation. Therefore, the inventors considered the application development to the powder melt layer thickness measurement.

パウダー溶融層の厚み変化は、パウダーの誘電率変化として現れるため、事前に、パウダー溶融状態の誘電率変化とパウダー投入界面と溶鋼界面の二つの界面の分離出力値を計測しておけば、計測データによりパウダーの溶融層厚みを連続的に推算できることになる。   Since the change in the thickness of the powder melt layer appears as a change in the dielectric constant of the powder, it is possible to measure by measuring the change in the dielectric constant of the powder melt state and the separation output value of the two interfaces, the powder input interface and the molten steel interface, in advance. Based on the data, the powder melt layer thickness can be estimated continuously.

ところで、パウダーの誘電率とマイクロ波の中心周波数、変調振幅は、パウダー投入界面と溶鋼界面の二つの界面の測定精度などに影響を及ぼす。すなわち、パウダーの誘電率は、個々のパウダー物性により多少は変化するものの、粉体か溶融状態かによって大きく影響を受ける。つまり、パウダーの誘電率の変化は、溶融層の厚みに置き換えることが出来るので、マイクロ波の反射がパウダーの誘電率の影響を受けて測定値に変化が現れることは、パウダー溶融層の厚み変化がパウダー誘電率の変化として現れたことを意味している。   By the way, the dielectric constant of the powder, the center frequency of the microwave, and the modulation amplitude affect the measurement accuracy of the two interfaces of the powder injection interface and the molten steel interface. In other words, the dielectric constant of the powder is somewhat affected by the powder properties, although it varies somewhat depending on the individual powder properties. In other words, the change in the dielectric constant of the powder can be replaced by the thickness of the molten layer, and the change in the measured value due to the influence of the dielectric constant of the powder reflects the change in the thickness of the powder molten layer. Is expressed as a change in powder dielectric constant.

従って、実用化されている成分範囲の一般的なパウダーには、基本パターンとなるパウダーの投入厚みとパウダー溶融層厚みの検量線を求めておけば、多くのパウダー溶融層厚みの測定に対応することが可能になる。勿論、個々のパウダーの誘電率を測定することも無意味ではない。   Therefore, it is possible to measure a large number of powder melt layer thicknesses by obtaining a calibration curve for the input thickness of the powder and the powder melt layer thickness, which are the basic patterns, for general powders in the range of components in practical use. It becomes possible. Of course, measuring the dielectric constant of each individual powder is not meaningless.

つまり、パウダー投入界面及び溶鋼界面の二つの界面が安定して測定できれば、本発明で目的とするパウダー溶融層厚みの連続測定は十分に可能となる。   That is, if the two interfaces of the powder input interface and the molten steel interface can be measured stably, the continuous measurement of the powder melt layer thickness intended in the present invention is sufficiently possible.

鋼の連続鋳造では、図5に示すように、一般的に鋳型内溶鋼13の湯面レベルを測定する目的で、渦流センサー11が設置されている。浸漬ノズル12から供給された溶鋼13は鋳型14内に注入され、鋳型14からの冷却により凝固シェル15を形成し、鋳型下方に引き抜かれる。鋳型内は、注入された溶鋼13を保温・被覆さらに凝固シェル15と鋳型14の潤滑を目的として、パウダー16が投入され、溶鋼13との接触面にパウダー溶融層17が存在している。   In the continuous casting of steel, as shown in FIG. 5, the eddy current sensor 11 is generally installed for the purpose of measuring the surface level of the molten steel 13 in the mold. Molten steel 13 supplied from the immersion nozzle 12 is poured into the mold 14, forms a solidified shell 15 by cooling from the mold 14, and is drawn out below the mold. In the mold, powder 16 is introduced for the purpose of keeping and covering the injected molten steel 13 and lubricating the solidified shell 15 and the mold 14, and a powder molten layer 17 exists on the contact surface with the molten steel 13.

本発明の目的であるパウダー溶融層厚みの測定原理は、既設の渦流センサー11による溶鋼13の湯面レベル測定値L(真の値)と、マイクロ波を用いた前述のパウダー投入界面と溶鋼界面の二つの界面の測定分離値を対比比較することで、パウダー溶融層厚みを得るものである。   The measurement principle of the thickness of the powder melt layer, which is the object of the present invention, is the measured level L (true value) of the molten steel 13 by the existing eddy current sensor 11 and the above-described powder input interface and molten steel interface using microwaves. By comparing and comparing the measured separation values of the two interfaces, the powder melt layer thickness is obtained.

すなわち、照射・受信器1より照射したマイクロ波をアンテナ1aで受信し、パウダー投入界面の測定値L2と、溶鋼13の湯面レベルの測定値L1を得る。このうち、パウダー投入界面の測定値L2は、空気中の測定であるために真の値であるが、湯面レベルの測定値L1は、パウダー16を透過しているので、パウダー誘電率の影響を受けて誤差を有している。   That is, the microwave irradiated from the irradiation / receiver 1 is received by the antenna 1a, and the measured value L2 of the powder injection interface and the measured value L1 of the molten steel level of the molten steel 13 are obtained. Of these, the measured value L2 at the powder input interface is a true value because it is measured in the air, but the measured value L1 at the hot water level is transmitted through the powder 16 and is therefore influenced by the powder dielectric constant. Have an error.

そして、前記既設の渦流センサー11を用いて測定した溶鋼13の湯面レベルの測定値L(真の値)と、マイクロ波を照射して測定した溶鋼13の湯面レベルの測定値L1の差と、パウダー投入界面の測定値L2から、以下に説明するようにパウダー溶融層厚み変化(誘電率変化)の校正を行い、パウダー溶融層厚みを算出する。   Then, the difference between the measured value L (true value) of the molten steel level measured using the existing eddy current sensor 11 and the measured value L1 of the molten metal level measured by irradiating microwaves. From the measured value L2 of the powder input interface, the powder melt layer thickness change (dielectric constant change) is calibrated as described below, and the powder melt layer thickness is calculated.

(パウダー溶融層厚みの換算方法)
図2をベースにパウダー溶融層厚み変化の試算原理を説明する。
(Conversion method of powder melt layer thickness)
The calculation principle of the powder melt layer thickness change will be described with reference to FIG.

図2に示したように、マイクロ波を用いて測定したパウダー表面及び箱の底面までの距離と、パウダー投入厚みには相関があり、連続鋳造時のメニスカスに対応する箱の底面位置の測定距離が、パウダー誘電率の影響を受けてパウダー投入厚み増加と比例して大きくなる傾向がある。   As shown in FIG. 2, there is a correlation between the distance to the powder surface and the bottom surface of the box measured using microwaves and the thickness of the powder, and the measurement distance of the bottom position of the box corresponding to the meniscus during continuous casting However, it tends to increase in proportion to the increase in the thickness of the charged powder due to the influence of the dielectric constant of the powder.

マイクロ波を用いて測定した溶鋼界面の距離L1と、渦流センサー11を用いて測定した溶鋼界面の距離Lとの差ΔL1(=L1−L)と、実際のパウダー投入厚みとの関係の一例を示した図を図6に示す。   An example of the relationship between the difference ΔL1 (= L1−L) between the distance L1 of the molten steel interface measured using the microwave and the distance L of the molten steel interface measured using the eddy current sensor 11 and the actual powder input thickness The figure shown is shown in FIG.

図5を用いて説明したように、溶鋼13の湯面(メニスカス)の真の値は、渦流センサー11により連続的に計測されている。   As described with reference to FIG. 5, the true value of the molten metal surface (meniscus) of the molten steel 13 is continuously measured by the eddy current sensor 11.

よって、マイクロ波による測定値を、渦流センサー11による測定値を基に事前に校正しておけば、マイクロ波を用いて測定した溶鋼界面までの距離L1と渦流センサー11を用いて連続的に計測されている溶鋼界面までの真の距離Lの差ΔL1(=L1−L)を求めれば、図6からパウダー投入厚みを推算することができる。例えば前記差ΔLが30mmの場合は、図6に示すパウダー粉体単層時の校正線より、パウダー投入厚みは約70mmであると推算できる。   Therefore, if the measured value by the microwave is calibrated in advance based on the measured value by the eddy current sensor 11, the distance L1 to the molten steel interface measured by using the microwave and the eddy current sensor 11 are continuously measured. If the difference ΔL1 (= L1−L) of the true distance L to the molten steel interface is obtained, the powder input thickness can be estimated from FIG. For example, when the difference ΔL is 30 mm, it can be estimated from the calibration line for the powder powder single layer shown in FIG.

同様に、パウダー投入厚み(粉体のパウダー+パウダー溶融層)とパウダー溶融層厚みの関係を事前に校正してデータを用意しておけば、パウダー溶融層厚みを連続的に推算することができる。   Similarly, if the data is prepared by calibrating the relationship between the powder input thickness (powder powder + powder melt layer) and the powder melt layer thickness in advance, the powder melt layer thickness can be estimated continuously. .

すなわち、渦流センサー11を用いた溶鋼13の湯面レベルの測定値Lと、マイクロ波を用いた溶鋼13の湯面レベルの測定値L1を、予め冷間で校正して同一指示値としておく。   That is, the measured value L of the molten metal level of the molten steel 13 using the eddy current sensor 11 and the measured value L1 of the molten metal level of the molten steel 13 using microwaves are calibrated cold in advance and set to the same indicated value.

溶鋼13の湯面上にパウダー16が投入されると、渦流センサー11による湯面レベルの測定値Lは変化しないが、マイクロ波による湯面レベルの測定値L1は、パウダー平均誘電率の影響を受けて変化する。   When the powder 16 is put on the molten metal surface of the molten steel 13, the measured value L of the molten metal surface level by the eddy current sensor 11 does not change, but the measured value L1 of the molten metal surface level by the microwave is influenced by the average powder dielectric constant. Change in response.

そして、これら両測定値の差ΔL1(=L1−L)は、パウダー投入厚み(粉体+パウダー溶融層)の変化に比例するため、予め求めておいた、前記差ΔLとパウダー投入厚み(粉体+パウダー溶融層)、パウダー投入厚み(粉体+パウダー溶融層)とパウダー溶融層厚みの校正データより、パウダー溶融層厚みを推算することができる。これが請求項1に係る発明である。   Since the difference ΔL1 (= L1−L) between these two measured values is proportional to the change in the powder input thickness (powder + powder melt layer), the previously obtained difference ΔL and the powder input thickness (powder) Body + powder melt layer), powder input thickness (powder + powder melt layer) and powder melt layer thickness calibration data, the powder melt layer thickness can be estimated. This is the invention according to claim 1.

すなわち、請求項1に係る発明では、パウダー投入厚みの変化を、パウダー表面(パウダー投入界面)で反射するマイクロ波で測定した測定値L2で検出し、パウダー投入量(パウダー投入厚み)と、校正データを用いたパウダー溶融層厚みの補正を行なうことと、鋳型内溶鋼の湯面レベル変化に対しては、渦流センサーによる湯面レベル測定値Lとマイクロ波による湯面レベル測定値L1をモニターすることで、パウダー投入厚み変化・鋳型内湯面レベル変化を補正し、パウダー溶融層厚みの測定精度向上を図っている。   In other words, in the invention according to claim 1, the change in the powder input thickness is detected by the measured value L2 measured by the microwave reflected on the powder surface (powder input interface), and the amount of powder input (powder input thickness) and the calibration are detected. For the correction of the powder melt layer thickness using the data and the change in the molten metal level of the molten steel in the mold, the molten metal level measured value L by the eddy current sensor and the molten metal level measured value L1 by the microwave are monitored. Therefore, the measurement accuracy of the powder melt layer thickness is improved by correcting the change in the powder thickness and the change in the level of the molten metal in the mold.

次に、請求項3に係る発明のパウダー溶融層厚みの測定原理と実施例について説明する。   Next, the measurement principle and examples of the powder melt layer thickness of the invention according to claim 3 will be described.

粉体のパウダー部分とパウダー溶融層で大きく誘電率が異なる場合は、図7に示すように、粉体のパウダー表面と、パウダー溶融層の上面、および溶鋼湯面(パウダー溶融層の下面)の距離換算スペクトルが検知されることになる。   When the dielectric constant is greatly different between the powder portion of the powder and the powder melt layer, as shown in FIG. 7, the powder surface of the powder, the upper surface of the powder melt layer, and the molten steel surface (the lower surface of the powder melt layer) A distance-converted spectrum is detected.

よって、パウダー溶融層厚みは、マイクロ波による溶鋼の湯面レベル測定値L1からパウダー溶融層の上面レベル測定値L3の差ΔL2(=L1−L3)によっても求めることが可能となる。   Therefore, the powder melt layer thickness can also be obtained by the difference ΔL2 (= L1−L3) between the molten steel level measurement value L1 of the molten steel and the upper surface level measurement value L3 of the powder melt layer.

図8にパウダー溶融層厚みとマイクロ波指示値の関係の一例を示す。
マイクロ波によるパウダー溶融層厚み測定中に、検尺棒を用いて実際のパウダー溶融層厚みを測定し、図8に示したような、マイクロ波指示値と実際のパウダー溶融層厚みの相関を取ることで、連続的にパウダー溶融層厚みを推定することが可能となる。
FIG. 8 shows an example of the relationship between the powder melt layer thickness and the microwave instruction value.
During the measurement of the powder melt layer thickness by microwave, the actual powder melt layer thickness is measured using a measuring rod, and the correlation between the microwave indication value and the actual powder melt layer thickness as shown in FIG. 8 is obtained. Thus, it becomes possible to continuously estimate the powder melt layer thickness.

発明者らは、粉体のパウダー部分とパウダー溶融層で大きく誘電率が異なる場合の測定を行った。そのデータの一例を図9に示す。図7に示すような、溶鋼の湯面レベル測定値L1、パウダー溶融層の上面レベル測定値L3、パウダー投入界面測定値L2に相当するマイクロ波反射波が測定できていることが分かる。   The inventors measured when the dielectric constants of the powder portion and the powder melt layer differed greatly. An example of the data is shown in FIG. It can be seen that the microwave reflected wave corresponding to the molten steel surface level measured value L1, the powder molten layer upper surface level measured value L3, and the powder input interface measured value L2 as shown in FIG. 7 can be measured.

すなわち、粉体のパウダーとパウダー溶融層の誘電率が大きく異なる場合は、溶鋼の湯面レベルの測定値L1、パウダー投入界面の測定値L2、パウダー溶融層の上面レベルの測定値L3を測定することでパウダー溶融層厚みの推定が可能である。   That is, when the dielectric constants of the powder powder and the powder molten layer are greatly different, the measured value L1 of the molten steel surface level, the measured value L2 of the powder input interface, and the measured value L3 of the upper surface level of the powder molten layer are measured. Thus, the powder melt layer thickness can be estimated.

また、誘電率の差が小さい場合でも、先に説明したように、溶鋼の湯面レベルの測定値L1とパウダー投入界面の測定値L2を検出することにより、パウダー溶融層厚みの推定が可能であり、本発明の有効性が確認できた。   Further, even when the difference in dielectric constant is small, as described above, it is possible to estimate the thickness of the molten powder layer by detecting the measured value L1 of the molten steel surface level and the measured value L2 of the powder input interface. The effectiveness of the present invention was confirmed.

なお、本発明では、マイクロ波の反射位相変化を考慮して測定精度を向上させている。すなわち、距離の変化量とマイクロ波の反射位相の変化は比例関係にあり、距離の変化は位相の変化にλ/(4π)を乗じることで求められる。従って、波長λが数mm〜数cmと短ければ、マイクロ波の反射位相の変化から、距離の変化量を精度よく求めることができる。   In the present invention, the measurement accuracy is improved in consideration of the change in the reflection phase of the microwave. That is, the amount of change in distance and the change in reflection phase of the microwave are in a proportional relationship, and the change in distance can be obtained by multiplying the change in phase by λ / (4π). Therefore, if the wavelength λ is as short as several millimeters to several centimeters, the distance variation can be accurately obtained from the change in the microwave reflection phase.

本発明は上記の例に限らず、各請求項に記載された技術的思想の範疇であれば、適宜実施の形態を変更しても良いことは言うまでもない。   The present invention is not limited to the above example, and it goes without saying that the embodiments may be changed as appropriate within the scope of the technical idea described in each claim.

例えば、パウダーの粉体部分と溶融層の界面でのマイクロ波の反射が明瞭に得られる場合には、次のようにして、パウダーの溶融層厚みを測定しても良い。   For example, when the reflection of the microwave at the interface between the powder portion of the powder and the molten layer is clearly obtained, the thickness of the molten layer of the powder may be measured as follows.

パウダーの粉体部分と溶融層の界面である溶融層の上面からのマイクロ波反射による上面レベル測定値L3と、レーザーやマイクロ波反射などの任意のセンサーによるパウダー表面レベルの測定値L2の差ΔL3(=L3−L2)を粉体状態のパウダー誘電率で補正してパウダー粉体層の厚みを求める。   The difference ΔL3 between the measured value L3 of the upper surface level by microwave reflection from the upper surface of the molten layer, which is the interface between the powder part of the powder and the molten layer, and the measured value L2 of the powder surface level by an arbitrary sensor such as laser or microwave reflection The thickness of the powder powder layer is determined by correcting (= L3−L2) with the powder dielectric constant in the powder state.

前記求めたパウダー粉体層の厚みと、前記パウダー表面レベルの測定値L2を渦流センサーによって求められた溶鋼の湯面レベル測定値Lから減算する。これにより、モールドパウダー溶融層の厚みを得ることができる。これが請求項2に係る発明である。   The obtained thickness of the powder powder layer and the measured value L2 of the powder surface level are subtracted from the measured value L of the molten steel surface level obtained by the eddy current sensor. Thereby, the thickness of the mold powder melt layer can be obtained. This is the invention according to claim 2.

また、上記の例では、渦流センサーを用いて鋳型内溶鋼界面の真の値を測定したものについて説明しているが、真の値を測定できるものであれば、任意の湯面レベルセンサーにより測定した値を使用しても良い。   In the above example, the true value of the molten steel interface in the mold is measured using an eddy current sensor. However, if the true value can be measured, it is measured by an arbitrary hot water level sensor. You may use the value that you did.

さらに、上記の例では、中心周波数の増加とパウダー投入界面と溶鋼界面の二つの界面の分離測定を可能として、精度良く測定するために、中心周波数が32GHz、変調振幅が8GHzと大きくしたマイクロ波を使用しているが、本発明のモールドパウダー溶融層厚み測定を可能とするためには、少なくとも中心周波数が20GHz〜32GHzの範囲内にあり、かつ変調振幅が8GHz以内であればよい。   Furthermore, in the above example, a microwave with a large center frequency of 32 GHz and a modulation amplitude of 8 GHz is provided to enable accurate measurement by increasing the center frequency and enabling separation measurement of the two interfaces of the powder injection interface and the molten steel interface. However, in order to enable measurement of the mold powder melt layer thickness of the present invention, it is sufficient that at least the center frequency is in the range of 20 GHz to 32 GHz and the modulation amplitude is within 8 GHz.

その理由は、図2に示した結果を得たラボ試験でも、パウダー投入表面の測定は難しいものの、投入底面の測定は可能であるからである。   The reason is that, even in the laboratory test that obtained the results shown in FIG. 2, it is difficult to measure the powder input surface, but it is possible to measure the input bottom surface.

ちなみに、マイクロ波の波長が長い(中心周波数が小さい)とパウダー粉体を含めて透過し易くなるが、パウダー表面の反射波は得られ難くなる。一方、波長を短く(中心周波数を大きく)するとパウダー表面での反射は容易になるが、パウダー内を透過し難くなる。   Incidentally, if the wavelength of the microwave is long (the center frequency is small), it is easy to transmit including the powder powder, but it is difficult to obtain the reflected wave on the powder surface. On the other hand, when the wavelength is shortened (center frequency is increased), reflection on the powder surface is facilitated, but it is difficult to transmit through the powder.

そこで、発明者らは、マイクロ波の中心周波数を20GHz〜32GHzの範囲に増加し、さらに変調振幅を8GHz以内まで広くすることで、測定に十分なパウダー表面の反射波、およびパウダー内の透過波を得て、パウダー投入界面と溶鋼界面の二つの界面の分離測定を可能としている。   Therefore, the inventors increased the center frequency of the microwave to a range of 20 GHz to 32 GHz and further widened the modulation amplitude to within 8 GHz, so that the reflected wave on the powder surface and the transmitted wave in the powder sufficient for measurement were obtained. It is possible to measure the separation of the two interfaces of the powder input interface and the molten steel interface.

1 照射・受信器
1a アンテナ
2 アンプ
3 データ収集用PC
4 箱
5 パウダー
11 渦流センサー
12 浸漬ノズル
13 溶鋼
14 鋳型
15 凝固シェル
16 パウダー
17 パウダー溶融層
1 Irradiation / Receiver 1a Antenna 2 Amplifier 3 Data collection PC
4 boxes 5 powder 11 eddy current sensor 12 immersion nozzle 13 molten steel 14 mold 15 solidified shell 16 powder 17 powder molten layer

Claims (5)

モールドパウダーの粉体部分と溶融層の界面でのマイクロ波の反射が明瞭に得られない場合における、連続鋳造時のモールドパウダー溶融層厚み測定方法であって、
前記モールドパウダーの粉体部分と溶融層の各々の平均誘電率の影響を受けるマイクロ波の反射による溶鋼の湯面レベル測定値L1と、前記平均誘電率の影響を受けない湯面レベルセンサーによる溶鋼の湯面レベル測定値Lの差ΔL1(=L1−L)と、モールドパウダーの溶融層厚みの相関を予め求めておき、
この予め求めておいた相関に基づいて、モールドパウダー溶融層厚みを得ることを特徴とする連続鋳造用モールドパウダーの溶融層厚み測定方法。
A method for measuring the thickness of a molten mold powder layer during continuous casting in the case where microwave reflection at the interface between the powder portion of the mold powder and the molten layer cannot be clearly obtained,
Molten steel level measurement L1 by the reflection of microwaves affected by the average dielectric constant of the powder part and molten layer of the mold powder, and the molten steel by the molten metal level sensor not affected by the average dielectric constant A correlation between the difference ΔL1 (= L1−L) in the measured level L of the molten metal and the molten layer thickness of the mold powder is obtained in advance.
A method for measuring a molten layer thickness of a mold powder for continuous casting, characterized in that a mold powder molten layer thickness is obtained based on the correlation obtained in advance.
モールドパウダーの粉体部分と溶融層の界面でのマイクロ波の反射が明瞭に得られる場合における、連続鋳造時のモールドパウダー溶融層厚み測定方法であって、
モールドパウダーの粉体部分のみの平均誘導率の影響を受けるモールドパウダーの粉体部分と溶融層の界面である溶融層の上面からのマイクロ波反射による上面レベル測定値L3と、任意のセンサーによるパウダー表面レベルの測定値L2の差ΔL3(=L3−L2)を粉体状態のパウダー誘電率で補正してパウダー粉体層の厚みを求め、
この求めたパウダー粉体層の厚みと、前記パウダー表面レベルの測定値L2を湯面レベルセンサーによって求められた溶鋼の湯面レベル測定値Lから減算することにより、モールドパウダー溶融層の厚みを得ることを特徴とする連続鋳造用モールドパウダーの溶融層厚み測定方法。
A method for measuring the thickness of a molten mold powder layer during continuous casting in the case where microwave reflection at the interface between the powder portion of the mold powder and the molten layer is clearly obtained,
Upper surface level measurement value L3 by microwave reflection from the upper surface of the molten layer, which is the interface between the mold powder powder portion and the molten layer affected by the average induction rate of only the powder portion of the mold powder, and powder by an arbitrary sensor The difference ΔL3 (= L3−L2) in the measured value L2 of the surface level is corrected by the powder dielectric constant in the powder state to obtain the thickness of the powder powder layer.
The thickness of the powder powder layer is obtained by subtracting the measured value L2 of the powder powder layer and the measured value L2 of the powder surface level from the measured value L of the molten steel level obtained by the molten metal level sensor. A method for measuring a molten layer thickness of a continuous casting mold powder.
モールドパウダーの粉体部分と溶融層の界面、および溶鋼の湯面でのマイクロ波の反射がそれぞれ明瞭に得られる場合における、連続鋳造時のモールドパウダー溶融層厚み測定方法であって、
前記モールドパウダーの粉体部分と溶融層の各々の平均誘電率の影響を受けるマイクロ波の反射による溶鋼の湯面レベル測定値L1と、モールドパウダーの粉体部分のみの平均誘導率の影響を受けるモールドパウダーの粉体部分と溶融層の界面である溶融層の上面からのマイクロ波反射による上面レベル測定値L3の差ΔL2(=L1−L3)と、モールドパウダーの溶融層厚みの相関を予め求めておき、
この予め求めておいた相関に基づいて、マイクロ波の反射により測定したモールドパウダーの溶融層厚みを較正することを特徴とする連続鋳造用モールドパウダーの溶融層厚み測定方法。
Mold powder melt layer thickness measurement method at the time of continuous casting, in the case where the reflection of the microwave on the interface between the powder part of the mold powder and the molten layer and the molten steel surface is obtained clearly,
Influenced by the average dielectric constant of only the powder part of the mold powder and the measured level L1 of the molten steel due to the reflection of the microwave affected by the average dielectric constant of the powder part and the molten layer of the mold powder. The correlation between the difference ΔL2 (= L1−L3) of the upper surface level measurement value L3 due to the microwave reflection from the upper surface of the molten layer, which is the interface between the powder portion of the mold powder and the molten layer, and the molten layer thickness of the mold powder is obtained in advance. Leave
A method for measuring a molten layer thickness of a mold powder for continuous casting, wherein the molten layer thickness of the mold powder measured by reflection of microwaves is calibrated based on the correlation obtained in advance.
請求項1に記載の連続鋳造用モールドパウダーの溶融層厚み測定方法において、
前記マイクロ波による溶鋼の湯面レベル測定値L1と、前記渦流センサーによる溶鋼の湯面レベル測定値Lの差ΔL1(L1−L)を連続的に測定し、前記予め求めておいた相関に基づいてパウダー溶融層厚みを連続的に得ることを特徴とする連続鋳造用モールドパウダーの溶融層厚み測定方法。
In the molten layer thickness measuring method of the mold powder for continuous casting according to claim 1,
The difference ΔL1 (L1−L) between the measured level L1 of the molten steel by the microwave and the measured level L of the molten steel by the eddy current sensor is continuously measured, and based on the previously obtained correlation. A method for measuring a melt layer thickness of a mold powder for continuous casting, wherein the powder melt layer thickness is continuously obtained.
請求項1〜4の何れかに記載の連続鋳造用モールドパウダーの溶融層厚み測定方法において、
マイクロ波の反射位相変化を用いて、マイクロ波による前記測定値を計測することを特徴とする連続鋳造用モールドパウダーの溶融層厚み測定方法。
In the melt layer thickness measuring method of the mold powder for continuous casting according to any one of claims 1 to 4,
A method for measuring a molten layer thickness of a mold powder for continuous casting, wherein the measurement value by microwave is measured using a change in reflection phase of microwave.
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JP2014153077A (en) * 2013-02-05 2014-08-25 Nippon Steel & Sumitomo Metal Method for measuring thickness of slag floating on molten metal surface
WO2016173901A1 (en) * 2015-04-29 2016-11-03 Primetals Technologies Austria GmbH Slag detection in a distributor of a strand casting system

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Publication number Priority date Publication date Assignee Title
JP2014153077A (en) * 2013-02-05 2014-08-25 Nippon Steel & Sumitomo Metal Method for measuring thickness of slag floating on molten metal surface
WO2016173901A1 (en) * 2015-04-29 2016-11-03 Primetals Technologies Austria GmbH Slag detection in a distributor of a strand casting system

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