JP2012512658A5 - - Google Patents
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- Publication number
- JP2012512658A5 JP2012512658A5 JP2011542416A JP2011542416A JP2012512658A5 JP 2012512658 A5 JP2012512658 A5 JP 2012512658A5 JP 2011542416 A JP2011542416 A JP 2011542416A JP 2011542416 A JP2011542416 A JP 2011542416A JP 2012512658 A5 JP2012512658 A5 JP 2012512658A5
- Authority
- JP
- Japan
- Prior art keywords
- biomass
- lignin
- solvent
- solvent solution
- ammonia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002028 Biomass Substances 0.000 claims description 38
- 238000000034 method Methods 0.000 claims description 32
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 22
- 229920005610 lignin Polymers 0.000 claims description 19
- 239000002904 solvent Substances 0.000 claims description 18
- 150000001720 carbohydrates Chemical class 0.000 claims description 12
- 229910021529 ammonia Inorganic materials 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000003960 organic solvent Substances 0.000 claims description 10
- 235000014633 carbohydrates Nutrition 0.000 claims description 9
- 239000000725 suspension Substances 0.000 claims description 9
- BAVYZALUXZFZLV-UHFFFAOYSA-N mono-methylamine Natural products NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 claims description 8
- 229920002488 Hemicellulose Polymers 0.000 claims description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 150000003973 alkyl amines Chemical class 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000012038 nucleophile Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 4
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 claims description 4
- 150000002009 diols Chemical class 0.000 claims description 4
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims description 4
- 229920001021 polysulfide Polymers 0.000 claims description 4
- 239000005077 polysulfide Substances 0.000 claims description 4
- 150000008117 polysulfides Polymers 0.000 claims description 4
- 150000003568 thioethers Chemical class 0.000 claims description 4
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 2
- 239000003513 alkali Substances 0.000 claims description 2
- 150000001336 alkenes Chemical class 0.000 claims description 2
- 150000001345 alkine derivatives Chemical class 0.000 claims description 2
- 239000000010 aprotic solvent Substances 0.000 claims description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims description 2
- 229920002678 cellulose Polymers 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims description 2
- 125000004122 cyclic group Chemical group 0.000 claims description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 2
- 239000012634 fragment Substances 0.000 claims description 2
- 150000004679 hydroxides Chemical class 0.000 claims description 2
- 239000002029 lignocellulosic biomass Substances 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 230000014759 maintenance of location Effects 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 125000000250 methylamino group Chemical group [H]N(*)C([H])([H])[H] 0.000 claims description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 2
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 239000003774 sulfhydryl reagent Substances 0.000 claims description 2
- 150000003573 thiols Chemical class 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 240000008042 Zea mays Species 0.000 description 4
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 4
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 4
- 235000005822 corn Nutrition 0.000 description 4
- 239000010902 straw Substances 0.000 description 4
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 240000005979 Hordeum vulgare Species 0.000 description 2
- 235000007340 Hordeum vulgare Nutrition 0.000 description 2
- 240000000111 Saccharum officinarum Species 0.000 description 2
- 235000007201 Saccharum officinarum Nutrition 0.000 description 2
- 241000209140 Triticum Species 0.000 description 2
- 235000021307 Triticum Nutrition 0.000 description 2
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 description 1
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 1
- 241000609240 Ambelania acida Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 229920001503 Glucan Polymers 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 241000234435 Lilium Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241001520808 Panicum virgatum Species 0.000 description 1
- 240000006394 Sorghum bicolor Species 0.000 description 1
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 1
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 1
- 239000010905 bagasse Substances 0.000 description 1
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000002361 compost Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000002772 monosaccharides Chemical class 0.000 description 1
- 239000010893 paper waste Substances 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 229920001221 xylan Polymers 0.000 description 1
- 150000004823 xylans Chemical class 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13917908P | 2008-12-19 | 2008-12-19 | |
| US61/139,179 | 2008-12-19 | ||
| PCT/US2009/068373 WO2010080464A1 (en) | 2008-12-19 | 2009-12-17 | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012512658A JP2012512658A (ja) | 2012-06-07 |
| JP2012512658A5 true JP2012512658A5 (https=) | 2013-01-31 |
| JP5634410B2 JP5634410B2 (ja) | 2014-12-03 |
Family
ID=41718674
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011542416A Expired - Fee Related JP5634410B2 (ja) | 2008-12-19 | 2009-12-17 | 酵素糖化を促進させるためのバイオマスの有機溶剤前処理 |
Country Status (10)
| Country | Link |
|---|---|
| US (2) | US8241873B2 (https=) |
| EP (1) | EP2358886B1 (https=) |
| JP (1) | JP5634410B2 (https=) |
| CN (1) | CN102257151A (https=) |
| AU (1) | AU2009335804A1 (https=) |
| BR (1) | BRPI0916158A2 (https=) |
| CA (1) | CA2743450A1 (https=) |
| ES (1) | ES2401730T3 (https=) |
| MY (1) | MY151224A (https=) |
| WO (1) | WO2010080464A1 (https=) |
Families Citing this family (52)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5054177A (en) | 1988-03-10 | 1991-10-08 | B & J Manufacturing Company | Tire rasp blade |
| ES2447371T3 (es) | 2008-04-14 | 2014-03-11 | Bridgestone Corporation | Proceso para recuperar caucho a partir de látex de caucho natural |
| AU2009335866A1 (en) * | 2008-12-19 | 2010-07-15 | E. I. Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
| US8278070B2 (en) * | 2008-12-19 | 2012-10-02 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
| US8304213B2 (en) * | 2008-12-19 | 2012-11-06 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
| TWI676687B (zh) * | 2009-08-06 | 2019-11-11 | 奧地利商安尼基有限公司 | 用以由木質纖維素材料製造醣類裂解產物之方法 |
| US20110253326A1 (en) * | 2010-04-19 | 2011-10-20 | Savannah River Nuclear Solutions, Llc | Separation of Lignin From Lignocellulosic Materials |
| US8651403B2 (en) | 2010-07-21 | 2014-02-18 | E I Du Pont De Nemours And Company | Anhydrous ammonia treatment for improved milling of biomass |
| WO2012058293A1 (en) * | 2010-10-26 | 2012-05-03 | Novozymes North America, Inc. | Methods of saccharifying sugarcane trash |
| JP5621528B2 (ja) * | 2010-11-12 | 2014-11-12 | 王子ホールディングス株式会社 | リグノセルロース系原料の酵素糖化処理方法 |
| US20120125548A1 (en) * | 2010-11-23 | 2012-05-24 | E. I. Du Pont De Nemours And Company | Continuously fed biomass pretreatment process for a packed bed reactor |
| US20120125551A1 (en) * | 2010-11-23 | 2012-05-24 | E. I. Du Pont De Nemours And Company | Biomass pretreatment process for a packed bed reactor |
| CA2829207C (en) | 2011-03-07 | 2022-10-11 | Agrivida, Inc. | Consolidated pretreatment and hydrolysis of plant biomass expressing cell wall degrading enzymes |
| EP2597100A1 (de) * | 2011-11-28 | 2013-05-29 | Annikki GmbH | Verfahren zur Gewinnung von niedermolekularem Lignin (NML) |
| EP3216809B1 (en) | 2012-03-06 | 2018-11-14 | Bridgestone Corporation | Processes for recovering rubber from aged briquettes and aged briquettes containing plant matter from non-hevea plants |
| US12359004B2 (en) | 2012-03-06 | 2025-07-15 | Bridgestone Corporation | Processes for the removal of rubber from non-Hevea plants |
| MX2014012867A (es) * | 2012-04-26 | 2015-07-14 | Archer Daniels Midland Co | Separacion liquido / liquido de biomasa lignocelulosica para producir jarabes de azucar y fracciones de lignina. |
| AU2013262725B2 (en) | 2012-05-16 | 2016-10-06 | Bridgestone Corporation | Compositions containing purified non-Hevea rubber and related purification methods |
| SG11201408096SA (en) * | 2012-06-05 | 2015-03-30 | Mitsubishi Chem Corp | Polyester and polyurethane production method |
| EP2861627B1 (en) | 2012-06-18 | 2017-03-01 | Bridgestone Corporation | Methods for increasing the extractable rubber content of non-hevea plant matter |
| AU2013277335B2 (en) | 2012-06-18 | 2016-08-11 | Bridgestone Corporation | Systems and methods for the management of waste associated with processing guayule shrubs to extract rubber |
| CN105073862B (zh) * | 2012-06-18 | 2022-02-08 | 株式会社普利司通 | 用于渣滓脱溶剂的方法 |
| NZ743055A (en) * | 2013-03-08 | 2020-03-27 | Xyleco Inc | Equipment protecting enclosures |
| US20140326422A1 (en) * | 2013-05-03 | 2014-11-06 | Celanese International Corporation | Integrated Processes for Purifying a Cellulosic Material |
| WO2014179673A1 (en) * | 2013-05-03 | 2014-11-06 | Celanese International Corporation | Processes for purifying a cellulosic material |
| US20150041084A1 (en) * | 2013-08-06 | 2015-02-12 | Celanese International Corporation | Processes for Purifying a Cellulosic Material |
| WO2015038707A1 (en) | 2013-09-11 | 2015-03-19 | Bridgestone Corporation | Processes for the removal of rubber from tks plant matter |
| US20150087041A1 (en) | 2013-09-26 | 2015-03-26 | E I Du Pont De Nemours And Company | Production of ethanol with reduced contaminants in a cellulosic biomass based process |
| US20150087040A1 (en) | 2013-09-26 | 2015-03-26 | E I Du Pont De Nemours And Company | Production of ethanol and recycle water in a cellulosic fermentation process |
| US20150147786A1 (en) | 2013-11-24 | 2015-05-28 | E I Du Pont De Nemours And Company | High force and high stress destructuring for starch biomass processing |
| WO2016023563A1 (en) * | 2014-08-14 | 2016-02-18 | Inbicon A/S | Fluid composition comprising lignin |
| BR112017006700B1 (pt) * | 2014-10-01 | 2022-06-07 | Ptt Global Chemical Public Company Limited | Processo de pré-tratamento da biomassa lignocelulósica |
| CN104561183B (zh) * | 2015-01-16 | 2019-01-22 | 天津大学 | 一种玉米秸秆的预处理方法 |
| MX2017012913A (es) | 2015-04-10 | 2018-06-06 | Comet Biorefining Inc | Metodos y composiciones para el tratamiento de biomasa celulosica y productos producidos por estos. |
| KR101709328B1 (ko) * | 2015-07-09 | 2017-03-08 | 한국에너지기술연구원 | 2세대 바이오 매스의 5탄당을 이용한 저등급 석탄의 고품위화 방법 |
| JP5982549B1 (ja) * | 2015-10-01 | 2016-08-31 | 新日鉄住金エンジニアリング株式会社 | リグノセルロース系バイオマスの前処理方法及び前処理装置 |
| CN105352782B (zh) * | 2015-11-23 | 2018-07-31 | 中国科学院南京地理与湖泊研究所 | 一种沉积物中硫醚类致臭物质的测定前处理方法 |
| WO2017108055A1 (en) * | 2015-12-21 | 2017-06-29 | Inbicon A/S | Fluid composition comprising lignin and vinasse |
| ES2850355T3 (es) | 2016-02-19 | 2021-08-27 | Intercontinental Great Brands Llc | Procesos para crear corrientes de múltiples valores de fuentes de biomasa |
| CN107179259B (zh) * | 2016-03-10 | 2020-02-11 | 贵州茅台酒股份有限公司 | 一种快速简便评判酒醅堆积发酵质量的方法 |
| CN117587552A (zh) | 2018-01-12 | 2024-02-23 | 希尔科公司 | 从废弃纺织品中回收棉纤维和聚酯纤维的方法 |
| AU2019265921B2 (en) | 2018-05-10 | 2024-12-19 | Comet Biorefining Inc. | Compositions comprising glucose and hemicellulose and their use |
| CN109181270B (zh) * | 2018-07-02 | 2020-11-27 | 仲恺农业工程学院 | 一种超吸水性半纤维素气凝胶及其制备方法 |
| US10775105B2 (en) | 2018-11-19 | 2020-09-15 | Bridgestone Corporation | Methods for the desolventization of bagasse |
| US12202852B2 (en) | 2018-11-26 | 2025-01-21 | Board Of Trustees Of Michigan State University | Lignin extraction with volatile trialkylamines |
| WO2020132236A1 (en) | 2018-12-21 | 2020-06-25 | Bridgestone Corporation | Processes for increasing the molecular weight of guayule natural rubber |
| AU2020276774B2 (en) | 2019-05-10 | 2025-11-27 | Comet Biorefining Inc. | Materials and methods for producing arabinoxylan compositions |
| CN111534556B (zh) * | 2020-04-30 | 2023-04-25 | 南京林业大学 | 一种利用杨木酶法制备高浓度单糖溶液的方法 |
| CN112209975A (zh) * | 2020-09-28 | 2021-01-12 | 中国科学院广州能源研究所 | 一种催化木质纤维素一步制备芳香物和小分子醇类的方法 |
| CN114426330A (zh) * | 2020-10-29 | 2022-05-03 | 中国环境科学研究院 | 一种水-甲醇-碱体系制备稳态强化脱氮缓释碳源填料的方法 |
| CN112794932A (zh) * | 2020-12-31 | 2021-05-14 | 江南大学 | 一种通过预处理提高木质纤维素生物质可酶解性的方法 |
| EP4402202A4 (en) | 2021-09-16 | 2025-07-09 | Circ Llc | PROCESS FOR FORMING A POLYESTER FROM A REGENERATED DIACID FORMED FROM THE DEPOLYMERIZATION OF A WASTE MATERIAL |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1817525A (en) * | 1929-03-12 | 1931-08-04 | Brown Co | Production of chemical wood pulp |
| US1891337A (en) * | 1930-01-09 | 1932-12-20 | Du Pont | Process of producing cellulose |
| GB925524A (en) | 1958-10-22 | 1963-05-08 | Durel Inc | Methods of making a lignocellulose product and products resulting therefrom |
| US3033695A (en) * | 1958-10-22 | 1962-05-08 | Caradco Inc | Methods of making a lignocellulose product and products resulting therefrom |
| US3490994A (en) | 1966-12-30 | 1970-01-20 | Owens Illinois Inc | Treatment of lignocellulosic material with organomercaptan |
| US3490993A (en) * | 1966-12-30 | 1970-01-20 | Owens Illinois Inc | Process of treating lignocellulosic material with organomercaptan |
| US4329200A (en) * | 1980-06-02 | 1982-05-11 | Board Of Reagents, University Of Washington | Method and system for selective alkaline defiberization and delignification |
| US4470851A (en) * | 1981-03-26 | 1984-09-11 | Laszlo Paszner | High efficiency organosolv saccharification process |
| US4597830A (en) * | 1983-06-20 | 1986-07-01 | The University Of Alabama | Method and pulping composition for the selective delignification of lignocellulosic materials with an aqueous amine-alcohol mixture in the presence of a catalyst |
| US5171592A (en) * | 1990-03-02 | 1992-12-15 | Afex Corporation | Biomass refining process |
| US6555350B2 (en) * | 2000-02-17 | 2003-04-29 | Forskningscenter Riso | Method for processing lignocellulosic material |
| EP1869194A2 (en) * | 2005-04-12 | 2007-12-26 | E.I.Du pont de nemours and company | Treatment of biomass to obtain a target chemical |
| US20070029252A1 (en) * | 2005-04-12 | 2007-02-08 | Dunson James B Jr | System and process for biomass treatment |
| US7781191B2 (en) * | 2005-04-12 | 2010-08-24 | E. I. Du Pont De Nemours And Company | Treatment of biomass to obtain a target chemical |
| BRPI0505212A (pt) * | 2005-11-01 | 2007-08-07 | Dedini Sa Ind De Base | aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise |
| UA95795C2 (ru) * | 2006-01-27 | 2011-09-12 | Юниверсити Оф Массачусетс | Способ изготовления продукта из биомассы и установка по производству топлива из биомассы |
| US8278070B2 (en) * | 2008-12-19 | 2012-10-02 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
| US8304213B2 (en) * | 2008-12-19 | 2012-11-06 | E I Du Pont De Nemours And Company | Organic solvent pretreatment of biomass to enhance enzymatic saccharification |
-
2009
- 2009-12-16 US US12/639,059 patent/US8241873B2/en active Active
- 2009-12-17 BR BRPI0916158-9A patent/BRPI0916158A2/pt not_active IP Right Cessation
- 2009-12-17 WO PCT/US2009/068373 patent/WO2010080464A1/en not_active Ceased
- 2009-12-17 CA CA2743450A patent/CA2743450A1/en not_active Abandoned
- 2009-12-17 ES ES09775490T patent/ES2401730T3/es active Active
- 2009-12-17 MY MYPI20112123 patent/MY151224A/en unknown
- 2009-12-17 CN CN2009801511285A patent/CN102257151A/zh active Pending
- 2009-12-17 EP EP09775490A patent/EP2358886B1/en not_active Not-in-force
- 2009-12-17 JP JP2011542416A patent/JP5634410B2/ja not_active Expired - Fee Related
- 2009-12-17 AU AU2009335804A patent/AU2009335804A1/en not_active Abandoned
-
2012
- 2012-07-02 US US13/539,696 patent/US8460898B2/en not_active Expired - Fee Related
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