JP2011516748A - 鉱物繊維用のサイズ剤組成物および得られる製品 - Google Patents
鉱物繊維用のサイズ剤組成物および得られる製品 Download PDFInfo
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- JP2011516748A JP2011516748A JP2011503486A JP2011503486A JP2011516748A JP 2011516748 A JP2011516748 A JP 2011516748A JP 2011503486 A JP2011503486 A JP 2011503486A JP 2011503486 A JP2011503486 A JP 2011503486A JP 2011516748 A JP2011516748 A JP 2011516748A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/24—Coatings containing organic materials
- C03C25/26—Macromolecular compounds or prepolymers
- C03C25/32—Macromolecular compounds or prepolymers obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds
- C03C25/34—Condensation polymers of aldehydes, e.g. with phenols, ureas, melamines, amides or amines
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/24—Coatings containing organic materials
- C03C25/26—Macromolecular compounds or prepolymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/0405—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/0405—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres
- C08J5/043—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres with glass fibres
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09J161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09J161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
- C09J161/14—Modified phenol-aldehyde condensates
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/34—Condensation polymers of aldehydes or ketones with monomers covered by at least two of the groups C09J161/04, C09J161/18 and C09J161/20
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B1/00—Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2361/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers
- C08J2361/04—Condensation polymers of aldehydes or ketones with phenols only
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/15—Heterocyclic compounds having oxygen in the ring
- C08K5/151—Heterocyclic compounds having oxygen in the ring having one oxygen atom in the ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/17—Amines; Quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2666/00—Composition of polymers characterized by a further compound in the blend, being organic macromolecular compounds, natural resins, waxes or and bituminous materials, non-macromolecular organic substances, inorganic substances or characterized by their function in the composition
- C08L2666/02—Organic macromolecular compounds, natural resins, waxes or and bituminous materials
- C08L2666/26—Natural polymers, natural resins or derivatives thereof according to C08L1/00 - C08L5/00, C08L89/00, C08L93/00, C08L97/00 or C08L99/00
Abstract
【選択図】 なし
Description
−0ないし10部、好ましくは7部未満の重縮合触媒、たとえば硫酸アンモニウム;
−0ないし2部のシラン、特にアミノシラン;
−0ないし20部、好ましくは6ないし15部のオイル;および
−0ないし20部、好ましくは12部未満のアンモニア水溶液(20重量%溶液)。
頂部にコンデンサがあり、攪拌システムを備えた2リットルのリアクタに、378gのフェノール(4mol)、および37%の水溶液として809gのホルムアルデヒド(10mol)を導入し(2.5に等しいホルムアルデヒド/フェノールのモル比)、混合物を、攪拌しながら45℃に加熱した。
例1の条件下で液体樹脂を調製した。
−5/1に等しい圧縮比(見かけ厚さの圧縮下の厚さに対する比として定義される)による圧縮下で24時間後の厚さ回復性。この厚さ回復性は、測定された厚さの見かけ厚さに対する比であり、%で表される;これは製品の優れた寸法挙動を評価することを可能にする;および
−スタンピングによってインシュレーティング製品から切り取った試料に関するASTM C 686-71T規格に従った引張強さ。試料は、トーラス形状をしており、長さが122mm、幅が46mmであり、外縁での切片の曲率半径が38mmに等しく、内縁での切片の曲率半径が12.5mmに等しかった。
サイズ剤組成物を例2の条件下で調製したが、コーンスターチから得られたデキストリンをダイズ蛋白質水解物(Herculesから販売されているSoyad(登録商標) 12UT)で置換するように変更した。
Claims (16)
- 鉱物繊維、特にガラス繊維または岩石繊維用のサイズ剤組成物であって、液体の総重量に対して表わされる遊離ホルムアルデヒド含有量が0.1%以下である液体フェノール樹脂と増量剤とを含有する組成物。
- 前記液体フェノール樹脂が、フェノール−ホルムアルデヒドおよびフェノール−ホルムアルデヒド−アミンの縮合物で主に構成されていることを特徴とする請求項1に記載の組成物。
- 液体の総重量に対して表わされる遊離フェノール含有量が0.5%以下、好ましくは0.4以下であることを特徴とする請求項1または2に記載の組成物。
- 前記アミンが、アルカノールアミンまたは環状アミンであることを特徴とする請求項1ないし3の何れか1項に記載の組成物。
- 前記アミンが、モノエタノールアミンまたはジエタノールアミンであることを特徴とする請求項4に記載の組成物。
- 前記樹脂は、遊離ホルムアルデヒド含有量が0.1%以下であり、遊離フェノール含有量が0.4%以下であり、20℃での水希釈性が1000%以上、好ましくは2000%以上であることを特徴とする請求項1ないし5の何れか1項に記載の組成物。
- 前記増量剤が、炭水化物、リグニン誘導体、特にリグノスルホン酸アンモニウム(ALS)またはリグノスルホン酸ナトリウムなどのリグノスルホン酸塩、および動物性または植物性の蛋白質、特にダイズ蛋白質から選択されることを特徴とする請求項1ないし6の何れか1項に記載の組成物。
- 前記炭水化物が、エリトロース、トレオース、リボース、アラビノース、キシロース、リキソース、グルコース、アロース、アルトロース、マンノース、グロース、イドース、ガラクトース、タロース、プシコース、フルクトース、ソルボースおよびタガトースなどの単糖類、ラクトース、マルトース、スクロース、セロビオース、トレハロース、ラフィノース、ゲンチアノース、メリビオースおよびスタキオースなどの少糖類、ならびに、加工または未加工の澱粉、セルロース、グアーガムおよびキサンタンガムなどのガム、アルギナートおよびペクチンなどの多糖類から選択されることを特徴とする請求項7に記載の組成物。
- 更に、100乾燥重量部の、樹脂および尿素によって構成される混合物当たり、0ないし40部の尿素を含むことを特徴とする請求項1ないし8の何れか1項に記載の組成物。
- 増量剤の含有量は100乾燥重量部の液体樹脂当たり0.1ないし40部で変化し、好ましくは20部以下、たとえば3ないし20部であり、特に15部以下であることを特徴とする請求項1ないし9の何れか1項に記載の組成物。
- 100乾燥重量部の、液体樹脂および適切な場合には尿素当たり、以下の添加剤を更に含むことを特徴とする請求項1ないし10の何れか1項に記載の組成物:
−0ないし10部、好ましくは7部未満の触媒、たとえば硫酸アンモニウム;
−0ないし2部のシラン、特にアミノシラン;
−0ないし20部、好ましくは6ないし15部のオイル;および
−0ないし20部、好ましくは12部未満のアンモニア水溶液(20重量%溶液)。 - 液体の総重量に対して表される遊離ホルムアルデヒド含有量が0.1%以下である液体フェノール樹脂と増量剤とを含有する樹脂組成物。
- 請求項1ないし11の何れか1項に記載されたサイズ剤組成物によってサイジングされた鉱物繊維を含むインシュレーション製品、特に断熱および/防音製品。
- 前記繊維がガラス繊維または岩石繊維であることを特徴とする請求項13に記載の製品。
- 請求項12に記載の樹脂組成物の使用であって、鉱物繊維、特にガラス繊維または岩石繊維をベースとしたインシュレーティング製品の製造のために意図されたサイズ剤組成物の製造のための使用。
- 請求項1ないし11の何れか1項に記載のサイズ剤組成物の使用であって、鉱物繊維、特にガラス繊維または岩石繊維をベースとしたインシュレーティング製品の製造のための使用。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0802017A FR2929953B1 (fr) | 2008-04-11 | 2008-04-11 | Composition d'encollage pour fibres minerales et produits resultants |
FR08/02017 | 2008-04-11 | ||
PCT/FR2009/050654 WO2009136106A2 (fr) | 2008-04-11 | 2009-04-10 | Composition d'encollage pour fibres minerales et produits resultants |
Publications (2)
Publication Number | Publication Date |
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JP2011516748A true JP2011516748A (ja) | 2011-05-26 |
JP5562937B2 JP5562937B2 (ja) | 2014-07-30 |
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Application Number | Title | Priority Date | Filing Date |
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JP2011503486A Active JP5562937B2 (ja) | 2008-04-11 | 2009-04-10 | 鉱物繊維用のサイズ剤組成物および得られる製品 |
Country Status (14)
Country | Link |
---|---|
US (3) | US20110101260A1 (ja) |
EP (1) | EP2268590B1 (ja) |
JP (1) | JP5562937B2 (ja) |
AU (1) | AU2009245532B2 (ja) |
CA (1) | CA2720924C (ja) |
DK (1) | DK2268590T3 (ja) |
ES (1) | ES2693277T3 (ja) |
FR (1) | FR2929953B1 (ja) |
HR (1) | HRP20181476T1 (ja) |
LT (1) | LT2268590T (ja) |
PL (1) | PL2268590T4 (ja) |
RU (1) | RU2501825C2 (ja) |
SI (1) | SI2268590T1 (ja) |
WO (1) | WO2009136106A2 (ja) |
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FR2968008B1 (fr) * | 2010-11-30 | 2014-01-31 | Saint Gobain Isover | Composition d'encollage pour fibres, notamment minerales, comprenant un sucre non reducteur et un sel d'ammonium d'acide inorganique, et produits resultants. |
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FR2976585B1 (fr) * | 2011-06-17 | 2013-06-07 | Saint Gobain Adfors | Liant pour mat de fibres minerales et/ou organiques et produits obtenus. |
GB201120137D0 (en) * | 2011-11-22 | 2012-01-04 | Dynea Oy | Modified binder compositions |
CN103160230B (zh) * | 2013-03-01 | 2015-03-04 | 北京中铁润海科技有限公司 | 一种制备高温滤料的复合浸渍胶及其使用方法 |
CN103173169B (zh) * | 2013-03-01 | 2015-04-08 | 北京中铁润海科技有限公司 | 一种制备防火保温板的复合浸渍胶及其使用方法 |
FR3015472A1 (fr) | 2013-12-23 | 2015-06-26 | Rockwool Int | Methode pour reduire les emissions de formaldehyde et de composes organiques volatils (cov) dans un produit a base de fibres minerales |
CN103911104B (zh) * | 2014-01-06 | 2015-09-23 | 河北金源建材科技有限公司 | 木质素岩棉酚醛树脂粘结剂及其制备和使用方法 |
US9492961B2 (en) | 2014-08-01 | 2016-11-15 | Usg Interiors, Llc | Acoustic ceiling tiles with anti-sagging properties and methods of making same |
US20180290922A1 (en) * | 2014-10-30 | 2018-10-11 | Ppg Industries Ohio, Inc. | Amino Acid-Containing Sizing Compositions For Glass Fibers And Sized Fiber Glass Products |
PL3237350T3 (pl) * | 2014-12-23 | 2020-03-31 | Rockwool International A/S | Ulepszony środek wiążący |
EP3037393A1 (en) * | 2014-12-23 | 2016-06-29 | Rockwool International A/S | Improved Biobinder |
US11274444B2 (en) | 2014-12-23 | 2022-03-15 | Rockwool International A/S | Binder |
EA034416B1 (ru) * | 2015-01-30 | 2020-02-05 | Сэн-Гобэн Изовер | Изоляционный продукт |
EP3135647A1 (en) * | 2015-08-28 | 2017-03-01 | Rockwool International A/S | Solid state binder |
CN107236500A (zh) * | 2016-03-29 | 2017-10-10 | 中国林业科学研究院林产化学工业研究所 | 木质素磺酸盐改性尿素-酚醛树脂的制备方法 |
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- 2009-04-10 SI SI200931879T patent/SI2268590T1/sl unknown
- 2009-04-10 RU RU2010145927/05A patent/RU2501825C2/ru active
- 2009-04-10 DK DK09742304.0T patent/DK2268590T3/en active
- 2009-04-10 EP EP09742304.0A patent/EP2268590B1/fr active Active
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JP2014148422A (ja) * | 2011-09-27 | 2014-08-21 | Gunei-Chemical Industry Co Ltd | 無機繊維製品製造用バインダー、無機繊維製品の製造方法 |
Also Published As
Publication number | Publication date |
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JP5562937B2 (ja) | 2014-07-30 |
DK2268590T3 (en) | 2018-10-08 |
EP2268590A2 (fr) | 2011-01-05 |
AU2009245532B2 (en) | 2014-08-07 |
FR2929953B1 (fr) | 2011-02-11 |
EP2268590B1 (fr) | 2018-06-13 |
AU2009245532A1 (en) | 2009-11-12 |
PL2268590T3 (pl) | 2019-02-28 |
US20210309568A1 (en) | 2021-10-07 |
SI2268590T1 (sl) | 2018-12-31 |
FR2929953A1 (fr) | 2009-10-16 |
CA2720924C (fr) | 2017-04-18 |
RU2501825C2 (ru) | 2013-12-20 |
US20110101260A1 (en) | 2011-05-05 |
US20170334776A1 (en) | 2017-11-23 |
ES2693277T3 (es) | 2018-12-10 |
WO2009136106A3 (fr) | 2010-01-07 |
CA2720924A1 (fr) | 2009-11-12 |
PL2268590T4 (pl) | 2019-02-28 |
RU2010145927A (ru) | 2012-05-20 |
LT2268590T (lt) | 2018-10-10 |
WO2009136106A2 (fr) | 2009-11-12 |
US10961150B2 (en) | 2021-03-30 |
HRP20181476T1 (hr) | 2018-11-02 |
US11912616B2 (en) | 2024-02-27 |
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