JP2011505360A5 - - Google Patents
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- Publication number
- JP2011505360A5 JP2011505360A5 JP2010536085A JP2010536085A JP2011505360A5 JP 2011505360 A5 JP2011505360 A5 JP 2011505360A5 JP 2010536085 A JP2010536085 A JP 2010536085A JP 2010536085 A JP2010536085 A JP 2010536085A JP 2011505360 A5 JP2011505360 A5 JP 2011505360A5
- Authority
- JP
- Japan
- Prior art keywords
- diaminodinitropyridine
- diamino
- sulfonic acid
- stirring
- nitropyridine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- TXVNGKMUDSTDOD-UHFFFAOYSA-N 5,6-dinitropyridine-3,4-diamine Chemical compound NC1=CN=C([N+]([O-])=O)C([N+]([O-])=O)=C1N TXVNGKMUDSTDOD-UHFFFAOYSA-N 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 17
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 15
- 229910017604 nitric acid Inorganic materials 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 12
- XVDKITJPWVCWDA-UHFFFAOYSA-N 2,6-diamino-5-nitropyridine-3-sulfonic acid Chemical compound NC1=NC(N)=C(S(O)(=O)=O)C=C1[N+]([O-])=O XVDKITJPWVCWDA-UHFFFAOYSA-N 0.000 claims description 11
- ZZYXNRREDYWPLN-UHFFFAOYSA-N pyridine-2,3-diamine Chemical compound NC1=CC=CN=C1N ZZYXNRREDYWPLN-UHFFFAOYSA-N 0.000 claims description 10
- -1 2,6-diamino-3-nitropyridine-5-sulfonic acid Pyridine Chemical compound 0.000 claims description 4
- KJIPNHZXGLADPG-UHFFFAOYSA-L dipotassium;3,6-dicarboxybenzene-1,2-diolate Chemical compound [K+].[K+].OC(=O)C1=CC=C(C(O)=O)C([O-])=C1[O-] KJIPNHZXGLADPG-UHFFFAOYSA-L 0.000 claims description 4
- HOWDQPJMFFMJSR-UHFFFAOYSA-N pyridine-2,3,4,5-tetramine Chemical compound NC1=CN=C(N)C(N)=C1N HOWDQPJMFFMJSR-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- ZKBGGGWJGOHLDS-UHFFFAOYSA-N 4,5-diamino-3-nitropyridine-2-sulfonic acid Chemical compound NC1=CN=C(S(O)(=O)=O)C([N+]([O-])=O)=C1N ZKBGGGWJGOHLDS-UHFFFAOYSA-N 0.000 claims description 2
- 230000008878 coupling Effects 0.000 claims description 2
- 238000010168 coupling process Methods 0.000 claims description 2
- 238000005859 coupling reaction Methods 0.000 claims description 2
- 230000000379 polymerizing effect Effects 0.000 claims description 2
- RFSIFTKIXZLPHR-UHFFFAOYSA-N 3,5-dinitropyridine Chemical compound [O-][N+](=O)C1=CN=CC([N+]([O-])=O)=C1 RFSIFTKIXZLPHR-UHFFFAOYSA-N 0.000 claims 1
- 238000006396 nitration reaction Methods 0.000 claims 1
- YAXKSOWCKFOWDQ-UHFFFAOYSA-N 3,4-dinitrobenzene-1,2-diamine Chemical compound NC1=CC=C([N+]([O-])=O)C([N+]([O-])=O)=C1N YAXKSOWCKFOWDQ-UHFFFAOYSA-N 0.000 description 8
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 6
- ICTCBBIYOXTFLI-UHFFFAOYSA-N 2,4-diamino-5-nitrobenzenesulfonic acid Chemical compound NC1=CC(N)=C(S(O)(=O)=O)C=C1[N+]([O-])=O ICTCBBIYOXTFLI-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 150000003927 aminopyridines Chemical class 0.000 description 2
- KAMGOKSXKBHPHL-UHFFFAOYSA-N benzene-1,2,3,4-tetramine Chemical compound NC1=CC=C(N)C(N)=C1N KAMGOKSXKBHPHL-UHFFFAOYSA-N 0.000 description 2
- KMIOGTYSYXMZHB-UHFFFAOYSA-N 3,4-diamino-5-nitrobenzenesulfonic acid Chemical compound NC1=CC(S(O)(=O)=O)=CC([N+]([O-])=O)=C1N KMIOGTYSYXMZHB-UHFFFAOYSA-N 0.000 description 1
- ZBQONSWZWURUDA-UHFFFAOYSA-N 3,4-diaminopyridine-2-sulfonic acid Chemical compound NC1=CC=NC(S(O)(=O)=O)=C1N ZBQONSWZWURUDA-UHFFFAOYSA-N 0.000 description 1
- UVSUQUOUHQHYGW-UHFFFAOYSA-N 3-amino-2-nitrobenzenesulfonic acid Chemical compound NC1=CC=CC(S(O)(=O)=O)=C1[N+]([O-])=O UVSUQUOUHQHYGW-UHFFFAOYSA-N 0.000 description 1
- FHVMNJDMDQKUFK-UHFFFAOYSA-N 4-amino-3-nitropyridine-2-sulfonic acid Chemical compound NC1=CC=NC(S(O)(=O)=O)=C1[N+]([O-])=O FHVMNJDMDQKUFK-UHFFFAOYSA-N 0.000 description 1
- FXNSAHVFCAEFGU-UHFFFAOYSA-L [K+].[K+].NC1=CC=C(N)C(N)=C1N.OC(=O)C1=CC=C(C(O)=O)C([O-])=C1[O-] Chemical compound [K+].[K+].NC1=CC=C(N)C(N)=C1N.OC(=O)C1=CC=C(C(O)=O)C([O-])=C1[O-] FXNSAHVFCAEFGU-UHFFFAOYSA-L 0.000 description 1
- RRDBXTBGGXLZHD-UHFFFAOYSA-N benzene-1,4-dicarboperoxoic acid Chemical compound OOC(=O)C1=CC=C(C(=O)OO)C=C1 RRDBXTBGGXLZHD-UHFFFAOYSA-N 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/986,877 US8115007B2 (en) | 2007-11-27 | 2007-11-27 | Synthesis of diaminodinitropyridine |
| PCT/US2008/084459 WO2009070515A2 (en) | 2007-11-27 | 2008-11-24 | Synthesis of diaminodinitropyridine and diaminodinitrobenzene |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2011505360A JP2011505360A (ja) | 2011-02-24 |
| JP2011505360A5 true JP2011505360A5 (https=) | 2012-01-19 |
Family
ID=40336707
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010536085A Withdrawn JP2011505360A (ja) | 2007-11-27 | 2008-11-24 | ジアミノジニトロピリジンおよびジアミノジニトロベンゼンの合成 |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US8115007B2 (https=) |
| EP (1) | EP2217570B1 (https=) |
| JP (1) | JP2011505360A (https=) |
| KR (1) | KR20100092963A (https=) |
| WO (1) | WO2009070515A2 (https=) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102964596B (zh) * | 2012-11-14 | 2014-11-12 | 常州大学 | 聚2,6-二氨基吡啶及其合成方法 |
| CN113574701A (zh) | 2018-10-29 | 2021-10-29 | 株式会社Lg新能源 | 负极活性材料和包含其的锂二次电池 |
| HUE072593T2 (hu) | 2018-11-19 | 2025-11-28 | Lg Energy Solution Ltd | Anód aktív anyag és az azt tartalmazó lítium szekunder akkumulátor |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3740410A (en) | 1970-11-23 | 1973-06-19 | Horizons Inc | Acid addition salts of 2,3,5,6-tetraaminopyridine and a process for their preparation |
| US3838154A (en) | 1970-11-23 | 1974-09-24 | Horizons Inc | 2,6-diamino-3,5-dinitropyridines and derivatives thereof |
| US4022793A (en) | 1974-01-31 | 1977-05-10 | Horizons Research Incorporated | Triamino pyridine compounds |
| SU1066992A1 (ru) | 1982-10-05 | 1984-01-15 | Казанский Ордена Трудового Красного Знамени Химико-Технологический Институт Им.С.М.Кирова | Способ получени 2-нитрамино-3,5-динитропиридина |
| DE3727297A1 (de) | 1987-08-17 | 1989-03-02 | Wella Ag | Herstellungsverfahren fuer 2,5-diamino-6-nitro-pyridinderivate, ihre verwendung in haarfaerbemitteln sowie neue 2,5-diamino-6-nitro-pyridinderivate |
| DE3920336C2 (de) | 1989-06-21 | 1997-01-09 | Deutsch Franz Forsch Inst | Sprengstoffmasse mit geringer Empfindlichkeit |
| DE69412250T2 (de) | 1993-04-28 | 1999-02-11 | Akzo Nobel N.V., Arnheim/Arnhem | Pyridobismidazole enthaltendes rigid-rod-Polymer |
| US5945537A (en) | 1995-09-19 | 1999-08-31 | Akzo Nobel N.V. | Nitration of pyridine-2, 6-diamines |
| WO2006105227A1 (en) | 2005-03-28 | 2006-10-05 | E. I. Du Pont De Nemours And Company | Thermal processes for increasing polyareneazole inherent viscosities |
| WO2006105080A1 (en) | 2005-03-28 | 2006-10-05 | E.I. Du Pont De Nemours And Company | Processes for increasing polymer inherent viscosity |
-
2007
- 2007-11-27 US US11/986,877 patent/US8115007B2/en not_active Expired - Fee Related
-
2008
- 2008-11-24 WO PCT/US2008/084459 patent/WO2009070515A2/en not_active Ceased
- 2008-11-24 JP JP2010536085A patent/JP2011505360A/ja not_active Withdrawn
- 2008-11-24 EP EP08853164A patent/EP2217570B1/en not_active Not-in-force
- 2008-11-24 KR KR1020107014061A patent/KR20100092963A/ko not_active Withdrawn
-
2012
- 2012-01-09 US US13/345,996 patent/US20120116046A1/en not_active Abandoned
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