JP2010005659A - Method of manufacturing magnesium sheet - Google Patents

Method of manufacturing magnesium sheet Download PDF

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JP2010005659A
JP2010005659A JP2008167509A JP2008167509A JP2010005659A JP 2010005659 A JP2010005659 A JP 2010005659A JP 2008167509 A JP2008167509 A JP 2008167509A JP 2008167509 A JP2008167509 A JP 2008167509A JP 2010005659 A JP2010005659 A JP 2010005659A
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rolling
temperature
sheet
plate
flatness
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Masayuki Nakamoto
将之 中本
Sukenori Nakaura
祐典 中浦
Jo Sugimoto
丈 杉本
Akira Watabe
晶 渡部
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MA Aluminum Corp
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Mitsubishi Aluminum Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method of manufacturing a magnesium sheet having excellent flatness. <P>SOLUTION: This invention relates to the method of manufacturing the magnesium sheet having excellent flatness by applying different circumferential speed rolling in the cold and at low temperature to the magnesium belt-like sheet, in the process in which a magnesium belt-like sheet is thinned by rolling in a coil shape, wherein in the final pass of the rolling, the upper and lower work rolls is made to have different circumferential speed, and in the range of 1.05-1.3 of a circumferential speed ratio, rolling in the cold and at low temperature is performed at the total draft of ≤25%. In this rolling, it is preferable that the temperature of a material is the room temperature to 180°C and the surface temperature of the work rolls is the room temperature to 180°C. Since shear deformation is generated in the vertical direction and the horizontal direction in the material and uniform stain is imparted to the full surface of the sheet, and the flatness is improved without bringing about the deterioration of characteristics by heating the material. <P>COPYRIGHT: (C)2010,JPO&INPIT

Description

優れた平坦度を有するMg板の製造方法に関する。   The present invention relates to a method for producing an Mg plate having excellent flatness.

Mgは六方最密構造であるため、室温でのすべり面が(0002)基底面のみであり、常温での塑性加工性が乏しく、圧延する際には高温に加熱する必要がある。また、圧延時のロールへの抜熱量を低下させるためにヒーターを内蔵した圧延ロールを用い、ロール自体を加熱し圧延する方法等が一般的に行なわれている。材料の加熱が不十分である場合、材料表面に微細割れやサイドクラックを生じやすく、最悪の場合は発生した割れやクラックが伝播し、材料の破断に起因することがある。しかし、材料を加熱して圧延する熱間圧延、温間圧延では材料温度の影響により材料形状に不良を生じ易い。例えば、コイル圧延時において加熱ロールのサーマルクラウンの影響や材料通板時の位置ズレ等により、材料にセンターベリーやサイドベリーが発生し、材料の形状精度を悪くする要因となっている。材料の形状精度は平坦度で示され、板材の場合、形状精度が良いことが寸法精度とともに精度の良い板の条件となる。平坦度不良は、製品の外観を損ね、加工精度の低下を招く。さらに加工の自動化高速化を図るためには、加工時のセットや送りの精度が正確でなければならず、このためにも高い平坦度が必要となっている。   Since Mg has a hexagonal close-packed structure, the sliding surface at room temperature is only the (0002) basal plane, the plastic workability at room temperature is poor, and it is necessary to heat to a high temperature when rolling. Moreover, in order to reduce the heat removal amount to the roll at the time of rolling, the method of heating and rolling the roll itself using the rolling roll which incorporated the heater is generally performed. If the heating of the material is insufficient, fine cracks and side cracks are likely to occur on the surface of the material, and in the worst case, the generated cracks and cracks propagate and may be caused by the fracture of the material. However, in hot rolling and warm rolling in which a material is heated and rolled, the shape of the material is likely to be defective due to the influence of the material temperature. For example, due to the influence of the thermal crown of the heating roll at the time of coil rolling, the position misalignment at the time of material feeding, etc., center berries and side berries are generated in the material, which is a factor that deteriorates the shape accuracy of the material. The shape accuracy of the material is indicated by flatness. In the case of a plate material, a good shape accuracy is a condition for a plate having a high accuracy as well as a dimensional accuracy. The poor flatness impairs the appearance of the product and causes a reduction in processing accuracy. Furthermore, in order to increase the speed of automation of processing, the accuracy of setting and feeding at the time of processing must be accurate, and for this reason, high flatness is required.

また、素材の平坦度は比較的良いにも関わらず、打抜きなどの加工後の形状がばらついたり、曲げ加工後のスプリングバックが不均一になってしまう場合があるが、これらは素材の残留応力の分布が原因であることが多い。材料の矯正の主な目的は形状不良をなくすことであるが、残留応力の分布を均一化して小さくすることも可能である。従って、材料の矯正は薄板の高精度化に不可欠の工程となり、連続的なコイル材の主な矯正法には、繰返し曲げを利用するローラレベラと、引張りを利用するテンションレベラに大別される。
特開2006−205173号公報(段落0020)
In addition, although the flatness of the material is relatively good, the shape after punching or other processing may vary, and the springback after bending may become uneven. Often due to the distribution of. The main purpose of correcting the material is to eliminate the defective shape, but it is also possible to make the distribution of residual stress uniform and to reduce it. Accordingly, the correction of the material is an indispensable process for increasing the accuracy of the thin plate, and the main correction methods for the continuous coil material are roughly classified into a roller leveler that uses repeated bending and a tension leveler that uses tension.
JP 2006-205173 A (paragraph 0020)

上記繰返し曲げ矯正では、ジグザグ状に並んだ平行ロールの間に材料を通して、逆向きの曲げを材料に交互に与えることにより矯正を行うが、Mg板は室温での加工性が悪いために大きな効果は得られにくい。また、引張矯正法は一対の張力付加装置により、連続的に引張力を与えるものであるが、Mg板の場合は中間に炉を設けるなど加熱処理しながら行う必要がある。加熱によって変形抵抗を減らし、矯正に必要な張力を小さくすることができるが、材料を再び加熱することとなり、熱影響で粒成長してしまい、材料特性の低下を招いてしまう。そのため、材料加熱による特性低下を招くことなく、材料の残留応力の分布を均一化し、平坦度を改善する方法が必要とされている。   In the above repeated bending straightening, straightening is performed by passing the material between the parallel rolls arranged in a zigzag shape alternately, and the bending is performed alternately. However, the Mg plate has a great effect because it has poor workability at room temperature. Is difficult to obtain. In addition, the tension straightening method is a method in which a tensile force is continuously applied by a pair of tension applying devices, but in the case of an Mg plate, it is necessary to carry out a heat treatment such as providing a furnace in the middle. Although the deformation resistance can be reduced by heating and the tension required for correction can be reduced, the material is heated again, resulting in grain growth under the influence of heat, leading to deterioration of material properties. Therefore, there is a need for a method for making the distribution of the residual stress of the material uniform and improving the flatness without causing deterioration of characteristics due to material heating.

本発明の課題は、上記問題点を改善するためになされたもので、優れた平坦度を有するMg板を製造することによる品質改善を行なうことを目的とする。   An object of the present invention is to improve the above-mentioned problems, and an object of the present invention is to improve quality by manufacturing an Mg plate having excellent flatness.

本願発明者らは、前記目標を達成するために、様々な検討を行なった結果、仕上げ圧延に異周速圧延を用いることにより、板の巾方向だけでなく板厚方向にまで均一に加工を加えることができ、本発明完成するに至ったものである。   The inventors of the present invention have conducted various studies to achieve the above-mentioned target, and as a result, by using different peripheral speed rolling for finish rolling, processing can be performed uniformly not only in the sheet width direction but also in the sheet thickness direction. The present invention can be completed.

すなわち、本発明のMg板の製造方法のうち、第1の本発明は、熱間圧延または温間圧延後のMg帯状板をコイル状で圧延加工により薄肉化する過程において、上下ワークロールを異なる周速度とし、周速比を1.05〜1.3の範囲で、総圧下率25%以下で冷間圧延することを特徴とする。   That is, among the manufacturing methods of the Mg plate of the present invention, the first present invention is different in the upper and lower work rolls in the process of thinning the Mg strip-like plate after hot rolling or warm rolling in a coil shape by rolling. The rolling speed is set to a peripheral speed, and the rolling speed ratio is in the range of 1.05 to 1.3, and cold rolling is performed at a total rolling reduction of 25% or less.

第2の本発明のMg板の製造方法は、前記第1の本発明において、上記冷間圧延工程において、前記ワークロールの表面温度を室温〜180℃とし、材料温度を室温〜180℃とすることを特徴とする。   In the manufacturing method of the Mg plate of the second aspect of the present invention, in the first aspect of the present invention, in the cold rolling step, the surface temperature of the work roll is set to room temperature to 180 ° C, and the material temperature is set to room temperature to 180 ° C. It is characterized by that.

なお、本発明の製造方法で規定する条件について以下に説明する。
周速比:1.05〜1.3
仕上げ圧延として異周速圧延を行うことで、材料に上下方向及び水平方向にせん断変形を付与して平坦度を向上させることができる。ここで、周速比が1.05未満であると、十分な効果を得ることができず、一方、1.3を超えた周速比で異周速圧延を行うと、加工力が高すぎるため板材に割れを生じさせる。
In addition, the conditions prescribed | regulated with the manufacturing method of this invention are demonstrated below.
Peripheral speed ratio: 1.05-1.3
By performing different peripheral speed rolling as finish rolling, it is possible to improve the flatness by imparting shear deformation to the material in the vertical direction and the horizontal direction. Here, when the peripheral speed ratio is less than 1.05, a sufficient effect cannot be obtained. On the other hand, when different peripheral speed rolling is performed at a peripheral speed ratio exceeding 1.3, the processing force is too high. Therefore, the plate material is cracked.

総圧下率:25%以下
上記異周速圧延での総圧下率が25%を超える仕上げ圧延を行うと、強加工が複数回繰り返し行われるため、材料端部からの割れが大きくなり、健全なMg板材を得ることができない。下限は好ましくは3%以上でないと効果がない。
Total rolling reduction: 25% or less When finishing rolling in which the total rolling reduction in the above-mentioned peripheral rolling is over 25%, strong work is repeatedly performed a plurality of times, so that cracks from the end of the material become large and sound. Mg plate cannot be obtained. The lower limit is preferably 3% or more, and there is no effect.

ワークロール表面温度:室温〜180℃
ワークロールの表面温度が180℃を超えるとロールクラウン形状の影響が大きくなりすぎるため、Mg板の形状が制御できず、センターベリーを生じてしまう。
Work roll surface temperature: room temperature to 180 ° C
If the surface temperature of the work roll exceeds 180 ° C., the influence of the roll crown shape becomes too large, so that the shape of the Mg plate cannot be controlled and a center berry is produced.

材料温度:室温〜180℃
材料の温度が180℃を超えると、強度に影響が出る。温度が高すぎると、複数回の加熱により結晶粒が粗大化し、強度低下の原因に繋がる。
Material temperature: Room temperature to 180 ° C
When the temperature of the material exceeds 180 ° C., the strength is affected. If the temperature is too high, the crystal grains are coarsened by heating a plurality of times, leading to a decrease in strength.

すなわち、本発明のMg板の製造方法によれば、熱間圧延または温間圧延後のMg帯状板をコイル状で圧延加工により薄肉化する過程において、上下ワークロールを異なる周速度とし、周速比を1.05〜1.3の範囲で、総圧下率25%以下で冷間圧延するので、冷間および低温における圧延で加工される板材は、コイル状で薄肉化する工程において、周速度の異なる上下のワークロールを通過する際に上下方向の圧下だけでなく、水平方向にせん断変形が生じるため、板全面に均一なひずみが付与される。この結果、板材とロールとの接触面は加工度が均一となるため優れた平坦度のMg板が得られる。   That is, according to the manufacturing method of the Mg plate of the present invention, the upper and lower work rolls have different peripheral speeds in the process of thinning the Mg strip-like sheet after hot rolling or warm rolling in a coil shape by rolling. Since cold rolling is performed at a ratio of 1.05 to 1.3 and a total rolling reduction of 25% or less, the plate material processed by rolling at cold and low temperatures is a peripheral speed in the process of thinning in a coil shape. When passing through different upper and lower work rolls, not only the vertical reduction but also the horizontal shearing deformation occurs, so that a uniform strain is applied to the entire plate surface. As a result, the contact surface between the plate material and the roll has a uniform degree of processing, so an Mg plate with excellent flatness can be obtained.

以下に、本発明の一実施形態を説明する。
本発明では、熱間圧延または温間圧延を経たMg帯状板が用いられる。このMg帯状板に用いるMg材料としては、特に組成が限定されるものではなく、適宜組成のものを選定することができる。また、Mg帯状板も熱間圧延または温間圧延を経たものであればよく、その前工程での製造方法は特に限定されるものではない。例えばビレットを熱間圧延してその後、熱間圧延または温間圧延を行うものでもよく、また、連続鋳造によって直接熱間圧延または温間圧延前のMg板を製造するものであってもよい。
Hereinafter, an embodiment of the present invention will be described.
In the present invention, an Mg strip that has been subjected to hot rolling or warm rolling is used. The Mg material used for the Mg strip is not particularly limited in composition, and an appropriate material can be selected. Moreover, the Mg strip | belt-shaped board should just pass hot rolling or warm rolling, and the manufacturing method in the front process is not specifically limited. For example, the billet may be hot-rolled and then hot-rolled or warm-rolled, or may be a direct hot casting or an Mg plate before hot-rolling manufactured by continuous casting.

Mg帯状板を得る熱間圧延または温間圧延の製造条件は特に限定されるものではなく、その圧延パスに異周速圧延を含むものであってもよい。なお、温間圧延は、材料温度を180℃超〜300℃とする圧延工程として示すことができる。   The production conditions for hot rolling or warm rolling to obtain the Mg strip are not particularly limited, and the rolling pass may include different circumferential speed rolling. In addition, warm rolling can be shown as a rolling process which makes material temperature more than 180 degreeC-300 degreeC.

上記熱間圧延または温間圧延後に行う本願発明の冷間圧延では、周速比1.05〜1.3の範囲内で異周速圧延を行う。該異周速圧延での総圧下率は25%以下とする。この圧下率内であれば、パス数が特に限定されるものではない。
なお、当該異周速圧延では、材料温度を180℃以下にして、同様にワークロールの表面温度を180℃以下とする。
当該異周速圧延によって、材料は上下方向および水平方向にせん断変形が生じ、板全面に均一な歪みが付与されて、材料加熱による特性低下を招くことなく平坦度が向上する。
In the cold rolling of the present invention performed after the hot rolling or the warm rolling, different circumferential speed rolling is performed within a circumferential speed ratio of 1.05 to 1.3. The total rolling reduction in the different peripheral speed rolling is 25% or less. The number of passes is not particularly limited as long as it is within the rolling reduction.
In the different peripheral speed rolling, the material temperature is set to 180 ° C. or lower, and similarly, the surface temperature of the work roll is set to 180 ° C. or lower.
By the different peripheral speed rolling, the material undergoes shear deformation in the vertical direction and the horizontal direction, a uniform strain is given to the entire surface of the plate, and the flatness is improved without causing deterioration of characteristics due to material heating.

以下に、本発明の実施例を説明する。
JIS AZ31合金からなる元板厚5.4〜5.7mmのMg帯状板を熱間圧延して板厚2.0mmまで薄肉化し、400℃×16hの均質化処理を行なった。その後、温間圧延で薄肉化し、さらに、その後、Mg帯状板を適切なパススケジュールにて仕上げ圧延し、該圧延の条件を変量しつつ、板厚0.6mmまで薄肉化した。なお、仕上げ圧延時の冷間圧延は、材料温度を室温、ワークロール表面温度60℃に設定し、仕上げ圧延時の温間圧延では、材料温度250℃、ワークロール表面温度250℃に設定した。
Examples of the present invention will be described below.
A Mg strip-shaped plate made of JIS AZ31 alloy having a thickness of 5.4 to 5.7 mm was hot-rolled to a thickness of 2.0 mm, and homogenized at 400 ° C. for 16 hours. Thereafter, the thickness was reduced by warm rolling, and then the Mg strip was finish-rolled by an appropriate pass schedule, and the thickness was reduced to 0.6 mm while varying the rolling conditions. In the cold rolling during finish rolling, the material temperature was set to room temperature and the work roll surface temperature was 60 ° C. In the warm rolling during finish rolling, the material temperature was set to 250 ° C and the work roll surface temperature was 250 ° C.

得られたMg板について、定盤の上に置いて目視で平坦度の評価を行った。該平坦度の評価は、下記基準で行い、その結果を表1に示した。
AA:フラット
A :横から見てわずかに山がある
B :上から見ても山がわかる
C :上から見ても山がわかる程度が大きくなっている
D :製品として全く使用できないほどの山谷がある
The obtained Mg plate was placed on a surface plate and visually evaluated for flatness. The flatness was evaluated according to the following criteria, and the results are shown in Table 1.
A: Flat A: There are a few peaks when viewed from the side B: Mountains can be seen from above C: Mountains are large enough to be seen from above D: Mountain valleys that cannot be used as a product at all Is

Figure 2010005659
Figure 2010005659

表1に示すように周速比が1.15で冷間圧延異周速したものが最も良好な平坦度が得られた。一方、異周速圧延を行わなかった比較例では、仕上げ圧延を冷間圧延、温間圧延のいずれで行っても平坦度はCまたはDであった。また、仕上げ圧延時の周速比が1.3を超えると、平坦度はBまたはCであった。
さらに、周速比を適切にした冷間圧延によっても、総圧下率が25%を超えると材料が割れた。
As shown in Table 1, the best flatness was obtained when the peripheral speed ratio was 1.15 and the cold peripheral rolling speed was different. On the other hand, in the comparative example in which the different peripheral speed rolling was not performed, the flatness was C or D regardless of whether the finish rolling was performed by cold rolling or warm rolling. Moreover, when the peripheral speed ratio at the time of finish rolling exceeded 1.3, the flatness was B or C.
Furthermore, even by cold rolling with an appropriate peripheral speed ratio, the material cracked when the total rolling reduction exceeded 25%.

Claims (2)

熱間圧延または温間圧延後のMg帯状板をコイル状で圧延加工により薄肉化する過程において、上下ワークロールを異なる周速度とし、周速比を1.05〜1.3の範囲で、総圧下率25%以下で冷間圧延することを特徴とするMg板の製造方法。   In the process of thinning the Mg strip after hot rolling or warm rolling in a coil shape by rolling, the upper and lower work rolls have different peripheral speeds, and the peripheral speed ratio is in the range of 1.05 to 1.3. A method for producing an Mg plate, comprising cold rolling at a rolling reduction of 25% or less. 上記冷間圧延工程において、前記ワークロールの表面温度を室温〜180℃とし、材料温度を室温〜180℃とすることを特徴とする請求項1記載のMg板の製造方法。   In the said cold rolling process, the surface temperature of the said work roll shall be room temperature-180 degreeC, and material temperature shall be room temperature-180 degreeC, The manufacturing method of the Mg plate of Claim 1 characterized by the above-mentioned.
JP2008167509A 2008-06-26 2008-06-26 Method of manufacturing magnesium sheet Pending JP2010005659A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016525012A (en) * 2013-12-12 2016-08-22 ヘルムホルツ−ツェントルム ゲーストハハト ツェントルム フュアー マテリアル ウント キュステンフォルシュンク ゲーエムベーハー Method and apparatus for producing a magnesium sheet
CN114226461A (en) * 2021-12-20 2022-03-25 哈尔滨工业大学(威海) Magnesium alloy plate strip different-temperature different-speed coordinated rolling device and application

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016525012A (en) * 2013-12-12 2016-08-22 ヘルムホルツ−ツェントルム ゲーストハハト ツェントルム フュアー マテリアル ウント キュステンフォルシュンク ゲーエムベーハー Method and apparatus for producing a magnesium sheet
CN114226461A (en) * 2021-12-20 2022-03-25 哈尔滨工业大学(威海) Magnesium alloy plate strip different-temperature different-speed coordinated rolling device and application
CN114226461B (en) * 2021-12-20 2023-12-01 哈尔滨工业大学(威海) Magnesium alloy plate strip different-temperature different-speed coordinated rolling device and application

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