JP2009297684A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2009297684A5 JP2009297684A5 JP2008157706A JP2008157706A JP2009297684A5 JP 2009297684 A5 JP2009297684 A5 JP 2009297684A5 JP 2008157706 A JP2008157706 A JP 2008157706A JP 2008157706 A JP2008157706 A JP 2008157706A JP 2009297684 A5 JP2009297684 A5 JP 2009297684A5
- Authority
- JP
- Japan
- Prior art keywords
- gas
- liquid
- reaction
- separation method
- reaction vessel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007788 liquid Substances 0.000 claims 48
- 239000012495 reaction gas Substances 0.000 claims 17
- 238000000926 separation method Methods 0.000 claims 13
- 239000007789 gas Substances 0.000 claims 11
- 239000011344 liquid material Substances 0.000 claims 11
- 239000000463 material Substances 0.000 claims 2
- 238000005259 measurement Methods 0.000 claims 2
- 239000000758 substrate Substances 0.000 claims 2
- 238000007599 discharging Methods 0.000 claims 1
- 238000007789 sealing Methods 0.000 claims 1
Claims (15)
気体透過性材料で形成され、加圧された状態で未反応の前記反応気体及び前記生成物が流通する気体透過性管体と、
前記気体透過性管体の周囲を囲んで内部に収容する収容体と、
前記反応容器と前記気体透過性管体との間に設けられ、前記反応気体を密封した状態で、前記反応容器で生成された前記生成物を前記気体透過性管体に排出する生成物排出装置と、
を有することを特徴とする気液反応装置。 A gas-liquid reactor having a reaction vessel in which a product is produced by reaction between a liquid material containing a reaction substrate and a reaction gas under pressure,
A gas permeable tube formed of a gas permeable material and through which the unreacted reaction gas and the product flow in a pressurized state;
A container that encloses and surrounds the gas permeable tubular body ;
A product discharge device that is provided between the reaction vessel and the gas permeable tube and discharges the product generated in the reaction vessel to the gas permeable tube in a state where the reaction gas is sealed. When,
A gas-liquid reactor characterized by comprising:
前記生成物排出装置は、
内部に液溜空間を有し、天部において第１排出管を介して前記反応容器と接続され、底部において第２排出管を介して前記気体透過性管体と接続される液溜部と、
前記第２排出管を開閉するバルブと、
前記液溜空間に溜められた前記生成物の液面の位置を計測する液面計と、
前記液面の位置が所定位置に達したときに前記バルブを開き、前記液面の位置が所定位置に達していないときに前記バルブを閉じるように制御する排出制御器と、
を備えることを特徴とする気液反応装置。 The gas-liquid reactor according to claim 1,
The product discharge device comprises:
A liquid storage part having a liquid storage space inside, connected to the reaction vessel via a first discharge pipe at the top, and connected to the gas permeable tubular body via a second discharge pipe at the bottom;
A valve for opening and closing the second discharge pipe;
A level gauge for measuring the position of the liquid level of the product stored in the liquid storage space;
A discharge controller for controlling to open the valve when the position of the liquid level reaches a predetermined position and to close the valve when the position of the liquid level does not reach the predetermined position;
Gas-liquid reaction apparatus comprising: a.
前記収容体の内部を真空吸引する吸引装置を有することを特徴とする気液反応装置。 The gas-liquid reactor according to claim 1 or 2 ,
A gas-liquid reaction device comprising a suction device for vacuum suction of the inside of the container.
前記収容体の内部の気圧を計測する計測装置と、
前記計測装置の計測結果に基づいて前記吸引装置の駆動を制御する制御装置とを有することを特徴とする気液反応装置。 The gas-liquid reactor according to claim 3 ,
A measuring device for measuring the pressure inside the container;
A gas-liquid reaction device comprising: a control device that controls driving of the suction device based on a measurement result of the measurement device.
前記気体透過性管体は、前記収容体の内部で螺旋状に巻回されて配置されることを特徴とする気液反応装置。 In the gas-liquid reaction device according to any one of claims 1 to 4 ,
The gas-liquid reaction apparatus is characterized in that the gas permeable tube is spirally wound inside the container.
前記液体材料と前記反応気体とを加圧下で反応させる反応容器を有し、
前記液体材料と前記反応気体とは、前記反応容器内に連続的に供給されて反応することを特徴とする気液反応装置。 In the gas-liquid reactor according to any one of claims 1 to 5 ,
Having a reaction vessel for reacting the liquid material and the reaction gas under pressure;
The gas-liquid reaction apparatus, wherein the liquid material and the reaction gas are continuously supplied and reacted in the reaction vessel.
前記液体材料と前記反応気体とを加圧下で反応させる反応容器を有し、
前記液体材料と前記反応気体とは、前記反応容器内に間欠的に供給されて反応することを特徴とする気液反応装置。 In the gas-liquid reactor according to any one of claims 1 to 5 ,
Having a reaction vessel for reacting the liquid material and the reaction gas under pressure;
The gas-liquid reaction apparatus characterized in that the liquid material and the reaction gas are intermittently supplied into the reaction vessel to react.
前記液体材料と前記反応気体とを加圧下で反応させる反応容器を有し、
前記反応気体は、前記反応容器内に供給されて密封され、
前記液体材料は、前記反応容器内に連続的に供給されて前記反応気体と反応することを特徴とする気液反応装置。 In the gas-liquid reactor according to any one of claims 1 to 5 ,
Having a reaction vessel for reacting the liquid material and the reaction gas under pressure;
The reaction gas is supplied and sealed in the reaction vessel,
The gas-liquid reaction apparatus, wherein the liquid material is continuously supplied into the reaction vessel and reacts with the reaction gas.
気体透過性材料で形成され、収容体の内部に周囲を囲まれて収容された気体透過性管体に、加圧された状態で未反応の前記反応気体及び前記生成物を流通させる工程と、
前記反応気体を密封した状態で、前記反応容器で生成された前記生成物を前記気体透過性管体に排出する工程と、
を有することを特徴とする気液反応装置の気液分離方法。 A gas-liquid separation method of a gas-liquid reactor in which a product is generated by reacting a liquid material containing a reaction substrate with a reaction gas under pressure in a reaction vessel,
Flowing the unreacted reaction gas and the product in a pressurized state through a gas permeable tube formed of a gas permeable material and surrounded and enclosed inside the container;
Discharging the product produced in the reaction vessel to the gas permeable tube while the reaction gas is sealed;
A gas-liquid separation method for a gas-liquid reactor characterized by comprising:
前記収容体の内部を真空吸引する吸引工程を有することを特徴とする気液反応装置の気液分離方法。 In the gas-liquid separation method of the gas-liquid reactor according to claim 9 ,
A gas-liquid separation method for a gas-liquid reaction apparatus, comprising: a suction step for vacuum suction of the inside of the container.
前記収容体の内部の気圧を計測する工程と、
計測した気圧に基づいて前記真空吸引の駆動を制御する工程とを有することを特徴とする気液反応装置の気液分離方法。 In the gas-liquid separation method of the gas-liquid reaction device according to claim 10 ,
Measuring the atmospheric pressure inside the container;
And a step of controlling the driving of the vacuum suction based on the measured atmospheric pressure.
前記気体透過性管体は、前記収容体の内部で螺旋状に巻回されて配置されることを特徴とする気液反応装置の気液分離方法。 In the gas-liquid separation method of the gas-liquid reaction device according to any one of claims 9 to 11 ,
The gas-liquid separation method of a gas-liquid reaction apparatus, wherein the gas permeable tubular body is spirally wound inside the container.
前記液体材料と前記反応気体とを、前記反応容器内に連続的に供給して反応させることを特徴とする気液反応装置の気液分離方法。 In the gas-liquid separation method of the gas-liquid reaction device according to any one of claims 9 to 12 ,
A gas-liquid separation method for a gas-liquid reaction apparatus, wherein the liquid material and the reaction gas are continuously supplied into the reaction vessel to cause a reaction.
前記液体材料と前記反応気体とを、密閉された前記反応容器内に間欠的に供給して反応させることを特徴とする気液反応装置の気液分離方法。 In the gas-liquid separation method of the gas-liquid reaction device according to any one of claims 9 to 12 ,
A gas-liquid separation method for a gas-liquid reaction apparatus, wherein the liquid material and the reaction gas are intermittently supplied into the sealed reaction vessel to be reacted.
前記反応気体を、前記反応容器内に供給して密封し、
前記液体材料を、前記反応容器内に連続的に供給して前記反応気体と反応させることを特徴とする気液反応装置の気液分離方法。 In the gas-liquid separation method of the gas-liquid reaction device according to any one of claims 9 to 12 ,
Supplying and sealing the reaction gas into the reaction vessel;
A gas-liquid separation method for a gas-liquid reaction apparatus, wherein the liquid material is continuously supplied into the reaction vessel to react with the reaction gas.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2008157706A JP5219133B2 (en) | 2008-06-17 | 2008-06-17 | Gas-liquid reactor and gas-liquid separation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2008157706A JP5219133B2 (en) | 2008-06-17 | 2008-06-17 | Gas-liquid reactor and gas-liquid separation method thereof |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009297684A JP2009297684A (en) | 2009-12-24 |
| JP2009297684A5 true JP2009297684A5 (en) | 2011-07-14 |
| JP5219133B2 JP5219133B2 (en) | 2013-06-26 |
Family
ID=41545141
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008157706A Expired - Fee Related JP5219133B2 (en) | 2008-06-17 | 2008-06-17 | Gas-liquid reactor and gas-liquid separation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP5219133B2 (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013039967A1 (en) * | 2011-09-12 | 2013-03-21 | Idex Health & Science Llc | Supersaturated fluid degassing |
| US20200101400A1 (en) * | 2016-08-08 | 2020-04-02 | Taiyo Nippon Sanso Corporation | Gas-liquid separating device |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS531177A (en) * | 1976-06-24 | 1978-01-07 | Mitsui Eng & Shipbuild Co Ltd | Gas-liquid contact reaction apparatus |
| GB8304067D0 (en) * | 1983-02-14 | 1983-03-16 | Ici Plc | Gas treatment |
| JP2574734B2 (en) * | 1993-01-20 | 1997-01-22 | 和泉電気株式会社 | Gas-liquid pressurized mixing equipment |
| JP3770638B2 (en) * | 1995-10-02 | 2006-04-26 | 修三 松村 | Gas-liquid contact reactor |
| JP2000279750A (en) * | 1999-03-31 | 2000-10-10 | Chiyoda Corp | Mounting structure of tube of shell-and-tube type gas- liquid contact device and shell-and-tube type gas-liquid contact device |
| JP4538604B2 (en) * | 2004-09-21 | 2010-09-08 | 独立行政法人産業技術総合研究所 | Photoreaction tube built-in photoreaction apparatus and water quality monitoring apparatus using the same |
| JP2007105668A (en) * | 2005-10-14 | 2007-04-26 | Mitsubishi Chemicals Corp | Gas-liquid reaction method and apparatus therefor |
-
2008
- 2008-06-17 JP JP2008157706A patent/JP5219133B2/en not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5698456B2 (en) | Liquid distribution system including gas removal | |
| KR101936536B1 (en) | Fluid processing systems and methods | |
| JP5186583B2 (en) | Method and system for liquid dispensing with headspace degassing | |
| JP2009539606A5 (en) | ||
| US4936877A (en) | Dopant delivery system for semiconductor manufacture | |
| JP2007532433A5 (en) | ||
| WO2007139106A1 (en) | Pressurized tank, device for feeding powder to transportation pipe and its feeding method, and method of determining feeding interval of powder to transportation pipe | |
| US20160377469A1 (en) | Method and Apparatus for Measuring Gas Flow | |
| WO2008125917A3 (en) | System and method for packaging | |
| JP2009297684A5 (en) | ||
| KR100933481B1 (en) | Leakage tester | |
| CN208758195U (en) | Equipment raw material rinse device and its preform production equipment | |
| RU2009102818A (en) | INDICATOR PACKING | |
| JP6901303B2 (en) | Synthesizer | |
| RU2011104104A (en) | EMERGENCY DEVICE FOR EXPOSURE TO LEAKAGE OF HAZARDOUS CHEMICALS | |
| ITGE20130010A1 (en) | DEVICE FOR PROTECTING A LIQUID FROM OXIDATION | |
| CN208470643U (en) | Oil storage tank with pressure control device | |
| CN109630893A (en) | A kind of continuous-stable liquid-supplying system | |
| CN201815294U (en) | Device for adding powdered material in reactor | |
| KR20110068389A (en) | Apparatus for supplying chemical | |
| KR20120060083A (en) | Method of determining the relations of hydrogen-absorbing alloys | |
| JP2009287944A (en) | Internal pressure testing machine and internal pressure testing method | |
| KR100540186B1 (en) | Measuring method and device for pressure changed in plastic-bottle | |
| CN208394052U (en) | A kind of wet tank | |
| US1045567A (en) | Machine for bottling liquids under pressure. |