JP2009232750A - Frozen dessert and method for producing the same - Google Patents

Frozen dessert and method for producing the same Download PDF

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JP2009232750A
JP2009232750A JP2008083105A JP2008083105A JP2009232750A JP 2009232750 A JP2009232750 A JP 2009232750A JP 2008083105 A JP2008083105 A JP 2008083105A JP 2008083105 A JP2008083105 A JP 2008083105A JP 2009232750 A JP2009232750 A JP 2009232750A
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fat
frozen dessert
buttermilk
emulsion
frozen
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JP5185673B2 (en
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Keisuke Inoue
恵介 井上
Makiko Iwata
真樹子 岩田
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Morinaga Milk Industry Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a frozen dessert excellent in emulsification stability without using an emulsifier and a stabilizer as food additives, and having excellent flavor, and to provide a method for producing the same. <P>SOLUTION: The frozen dessert contains oil and fat, and butter milk. The method for producing the frozen dessert includes mixing a raw material liquid which contains oil and fat, and butter milk so as to obtain an emulsified liquid, and freezing the emulsified liquid. <P>COPYRIGHT: (C)2010,JPO&INPIT

Description

本発明は、冷菓およびその製造方法に関する。   The present invention relates to a frozen dessert and a method for producing the same.

近年、冷菓は年間を通じて食される代表的な嗜好食品となっている。冷菓は、例えば、乳脂肪、植物脂肪、又はこれらの混合物、無脂乳固形分、糖類、その他必要に応じ少量の安定剤、乳化剤、色素及び香料等を含む、殺菌した原料液より製造される。
氷結晶が細かく、組織が滑らかである優れた冷菓を製造するには、低温でのフリージングが効果的であると一般に知られている。しかし同時に、低温でのフリージングは、原料液の乳化状態を不安定にし、原料液中の脂肪球の凝集を促すため、風味や組織の劣化の一因となる脂肪粒を発生させてしまうことがある。
従来の冷菓では、この脂肪粒の発生を防ぎ、氷結晶が細かさ、組織の滑らかさ、風味などの品質を保持する為に、乳化剤および安定剤を使用している(非特許文献1参照)。
In recent years, frozen confectionery has become a typical favorite food eaten throughout the year. The frozen dessert is produced from a sterilized raw material liquid containing, for example, milk fat, vegetable fat, or a mixture thereof, non-fat milk solids, saccharides, and other small amounts of stabilizers, emulsifiers, pigments and fragrances as necessary. .
It is generally known that freezing at low temperature is effective for producing an excellent frozen dessert having fine ice crystals and a smooth structure. At the same time, however, freezing at a low temperature may cause the emulsion state of the raw material liquid to become unstable and promote the aggregation of fat globules in the raw material liquid. is there.
In conventional frozen desserts, emulsifiers and stabilizers are used in order to prevent the generation of fat particles and maintain the quality of ice crystals such as fineness, smoothness of the structure, and flavor (see Non-Patent Document 1). .

ところが、最近は健康志向から食品に対して様々な要望が寄せられるようになっており、要望の1つとして食品添加物を可能な限り含有しないことが望まれている。つまり、冷菓をはじめとして乳化の工程を有する多くの食品群において食品の品質を維持するために使用されている、食品添加物である乳化剤や安定剤の使用量を削減すること、あるいは不使用とすることが嘱望されている。
しかしながら、乳化剤及び安定剤を使用しない冷菓は、乳化剤及び安定剤を使用した従来の冷菓に比べて、脂肪粒が発生しやすい、氷結晶が大きい、組織が粗い、などの問題が生じやすく、風味の優れたものを得にくいという問題があった。
特に、冷菓を連続的に長時間製造する製造するメーカーが、乳化剤及びゼラチンなどの安定剤を使用せずに、氷結晶が細かく、組織が滑らかで、脂肪粒の発生がない、風味の優れた冷菓を連続的に製造することは困難であった。
Recently, however, various demands have been made on foods for health reasons, and as one of the demands, it is desired not to contain food additives as much as possible. In other words, reducing the amount of emulsifiers and stabilizers that are food additives used to maintain the quality of food in many food groups that have an emulsification process, including frozen desserts, or non-use It is envied to do.
However, frozen desserts that do not use emulsifiers and stabilizers are more prone to problems such as the formation of fat particles, large ice crystals, and coarser texture than conventional frozen desserts that use emulsifiers and stabilizers. There was a problem that it was difficult to obtain an excellent product.
In particular, manufacturers that produce frozen desserts continuously for a long time, without using emulsifiers and stabilizers such as gelatin, ice crystals are fine, the structure is smooth, fat particles are not generated, and the flavor is excellent It was difficult to produce frozen dessert continuously.

そこで、従来の乳化剤に代えて、卵黄を使用することが考えられる。実際、従来から乳化性やホイップ性を有する卵黄を使用した冷菓もある。しかし、卵に対してアレルギーを持つ場合に喫食することができないという問題があった。
一方、卵と乳化剤のいずれも使用せずに冷菓を得る方法として、乳化すべき原料とバターミルクパウダーとを水の存在下に混合して、冷菓の原料を乳化する方法がある(特許文献1参照)。
特開平4−346750号公報 湯山莊平監修、「アイスクリームの製造」、光琳(株)、1996年、p.19〜24
Therefore, it is conceivable to use egg yolk instead of the conventional emulsifier. In fact, there is a frozen dessert using egg yolk having emulsifying properties and whipping properties. However, there is a problem that if you are allergic to eggs, you cannot eat.
On the other hand, as a method of obtaining frozen confectionery without using either egg or emulsifier, there is a method of emulsifying the raw material of frozen confectionery by mixing the raw material to be emulsified and buttermilk powder in the presence of water (Patent Document 1). reference).
JP-A-4-346750 Supervised by Yuhei Yuyama, “Manufacture of ice cream”, Koso Co., Ltd., 1996, p. 19-24

しかしながら、特許文献1に記載の冷菓の製造方法においては、安定剤としてゼラチンを用いており、食品添加物である、乳化剤及び安定剤を共に使用せずに冷菓を製造することは、やはり困難であった。   However, in the method for producing frozen confection described in Patent Document 1, gelatin is used as a stabilizer, and it is still difficult to produce frozen confectionery without using an emulsifier and a stabilizer which are food additives. there were.

本発明は、上記事情を鑑みてなされたもので、卵や、食品添加物である乳化剤及び安定剤を用いることなく、風味の良い冷菓とその製造方法を提供することを目的とする。   This invention is made | formed in view of the said situation, and it aims at providing the frozen dessert with good flavor, and its manufacturing method, without using an egg and the emulsifier and stabilizer which are food additives.

本発明の冷菓は、油脂と、バターミルクとを含有することを特徴とする。
本発明の冷菓は、前記バターミルクを固形分で5.0〜10.0質量%含有することが好ましい。
本発明の冷菓の製造方法は、油脂とバターミルクとを含有する原料液を混合して乳化液を得た後、該乳化液をフリージングすることを特徴とする。
本発明の冷菓の製造方法においては、前記フリージングを、連続式フリーザーを用いて−6.5〜−7.5℃の範囲で行うことが好ましい。
The frozen dessert of the present invention is characterized by containing fats and oils and butter milk.
The frozen dessert of the present invention preferably contains 5.0 to 10.0% by mass of the buttermilk in solid content.
The method for producing a frozen dessert according to the present invention is characterized in that a raw material liquid containing fats and oils and buttermilk is mixed to obtain an emulsion, and then the emulsion is frozen.
In the manufacturing method of the frozen dessert of this invention, it is preferable to perform the said freezing in the range of -6.5 to -7.5 degreeC using a continuous freezer.

本発明によれば、卵や乳化剤及び安定剤等の食品添加物を用いることなく冷菓の原料液を乳化することができる。また、本発明の冷菓の製造方法によれば、卵や乳化剤及び安定剤等の食品添加物を用いることなく、製造中の脂肪粒の発生を抑えることができ、氷結晶が細かく、組織が滑らかな、風味の優れた冷菓を得ることができる。   According to the present invention, a frozen confectionery raw material liquid can be emulsified without using food additives such as eggs, emulsifiers and stabilizers. Further, according to the method for producing frozen confectionery of the present invention, the generation of fat particles during production can be suppressed without using food additives such as eggs, emulsifiers and stabilizers, ice crystals are fine, and the structure is smooth. In addition, a frozen dessert with excellent flavor can be obtained.

以下、本発明を詳細に説明する。
[冷菓]
本発明の冷菓は、油脂とバターミルクとを含有することを特徴とする。
本発明における冷菓とは、一般的な「冷菓」に分類されるものをいい、具体的には、アイスクリーム、アイスミルク、ラクトアイス、氷菓を挙げることができ、これらは、乳脂肪と無脂乳固形分の含量によって分類される。
Hereinafter, the present invention will be described in detail.
[Frozen dessert]
The frozen dessert of the present invention is characterized by containing fats and oils and butter milk.
The frozen dessert in the present invention refers to those classified as general “frozen desserts”, and specific examples include ice cream, ice milk, lact ice, and ice dessert. These include milk fat and non-fat milk. Classified by solids content.

バターミルクとは、クリームを攪拌(チャーニング)してバター粒を形成した際、形成されるバター粒から分離し排出される淡黄色の液体(山内邦男、横山健吉編集、「ミルク総合辞典」、朝倉書店(株)、1992年、p.357〜358)のことである。
本発明においては、バターミルクの代わりに、バターミルクを濃縮したバターミルク濃縮物および、さらに乾燥させたバターミルクパウダーも用いる事ができる。
バターミルクは、バターミルクの固形分中のリン脂質含量が高い事が知られおり、このリン脂質が、乳化の安定に寄与するため、バターミルクを油脂など冷菓の原料と共に用いると、乳化作用が得られると推測される。
尚、本発明において固形分とは、水分を除いた成分(総量から水分を減じた乾燥物量)を意味する。また、本発明における無脂乳固形分とは、固形分より脂質を除いた成分を意味する。
Buttermilk is a pale yellow liquid that is separated and discharged from the butter granules that are formed when the cream is stirred (charted) to form butter granules (Kunio Yamauchi, edited by Kenkichi Yokoyama, “Milk General Dictionary”, Asakura Shoten Co., Ltd., 1992, p.357-358).
In this invention, the buttermilk concentrate which concentrated buttermilk and the dried buttermilk powder can also be used instead of buttermilk.
Buttermilk is known to have a high phospholipid content in the solid content of buttermilk, and this phospholipid contributes to the stability of emulsification. Presumed to be obtained.
In the present invention, the solid content means a component excluding moisture (a dry matter amount obtained by subtracting moisture from the total amount). Moreover, the non-fat milk solid content in the present invention means a component obtained by removing lipid from the solid content.

本発明の冷菓において、バターミルクは固形分で5〜10質量%含有されていると好ましく、7〜10質量%含有されていることがより好ましい。
バターミルクの含有量が、固形分で5質量%以上であれば、低温のフリージング中でも脂肪球が凝集しにくい傾向にあり、10質量%以下であれば、冷菓の組成が変化しにくく、冷菓の風味に影響を与えにくい。
In the frozen dessert of the present invention, the buttermilk is preferably contained in a solid content of 5 to 10% by mass, and more preferably 7 to 10% by mass.
If the content of buttermilk is 5% by mass or more in terms of solid content, fat globules tend not to aggregate even during low-temperature freezing, and if it is 10% by mass or less, the composition of the frozen dessert is less likely to change. Hard to affect the flavor.

油脂としては、無塩バター、チーズ、バターオイル及びクリーム等の乳脂肪、植物油、ラード等が挙げられ、中でもクリームや無塩バター等を用いることが好ましい。
冷菓における油脂の含有量は特に限定しないが、固形分で3〜18質量%であることが好ましく、8〜18質量%であることがより好ましい。油脂の含有量が固形分で18質量%を超えると、脂っぽくなり、好ましい風味が得られない傾向にあり、3質量%未満であると、組織の緻密さとなめらかさが損なわれる傾向にある。
Examples of the fat include milk fat such as unsalted butter, cheese, butter oil and cream, vegetable oil, lard, etc. Among them, it is preferable to use cream and unsalted butter.
Although the content of fats and oils in frozen dessert is not specifically limited, it is preferable that it is 3-18 mass% in solid content, and it is more preferable that it is 8-18 mass%. When the content of fats and oils exceeds 18% by mass in solid content, it tends to be greasy and a preferable flavor tends not to be obtained, and when it is less than 3% by mass, the fineness and smoothness of the tissue tend to be impaired. .

また、本発明の冷菓は、バターミルクと油脂以外に、一般に冷菓の原料として用いられる原料を適宜選択して用いることができる。具体例としては、牛乳および乳製品、糖類および甘味料、酸味料、植物蛋白質、着香料、着色料、果汁および果肉、ジャム類、チョコレート類、各種食材等があげられる。また必要に応じて溶解水を用いる。溶解水とは、前記原料を溶解させる水のことである。   Moreover, the frozen confectionery of this invention can select and use suitably the raw material generally used as a raw material of frozen confectionery other than buttermilk and fats and oils. Specific examples include milk and dairy products, sugars and sweeteners, acidulants, plant proteins, flavoring agents, coloring agents, fruit juices and pulp, jams, chocolates, various foods, and the like. Dissolved water is used as necessary. Dissolved water is water that dissolves the raw material.

[冷菓の製造方法]
本発明の冷菓の製造方法は、油脂とバターミルクとを含有する原料液を混合して乳化液を得た後、該乳化液をフリージングすることを特徴とする。
[Method of manufacturing frozen confectionery]
The method for producing a frozen dessert according to the present invention is characterized in that a raw material liquid containing fats and oils and buttermilk is mixed to obtain an emulsion, and then the emulsion is frozen.

具体的には、例えば、まず油脂とバターミルクとを含む原料液を、65℃〜80℃で混合して乳化液を得る。混合には、粉物溶解機、高速攪拌機等の混合機を使用できる。
次に、乳化液を濾過する。乳化液を濾過することで、不純物を除去し、より滑らかな冷菓を得ることが可能となる。
次に、濾過した乳化液を50℃〜90℃、5〜20MPaの条件で均質化する。ここで、均質化を行うことにより、乳化がより良好となる。均質化には、ホモゲナイザー等を使用できる。
次に、均質化した乳化液を65℃〜150℃で殺菌する。殺菌には、プレート殺菌機、チューブラー殺菌機、インフュージョン殺菌機、インジェクション殺菌機、バッチ式殺菌機等を使用できる。
更に、殺菌した乳化液を0〜10℃に冷却し、4〜24時間程度エージングさせる。エージングとは、乳化液中の脂肪球を結晶化し、乳化被膜を安定化させることであり、ここで、エージングを行うと乳化液の物性が安定化する傾向にある。
Specifically, for example, first, a raw material liquid containing fats and oils and buttermilk is mixed at 65 ° C. to 80 ° C. to obtain an emulsion. For mixing, a mixer such as a powder dissolver or a high-speed stirrer can be used.
Next, the emulsion is filtered. By filtering the emulsified liquid, impurities can be removed and a smoother frozen dessert can be obtained.
Next, the filtered emulsion is homogenized at 50 to 90 ° C. and 5 to 20 MPa. Here, emulsification becomes better by homogenization. For homogenization, a homogenizer or the like can be used.
Next, the homogenized emulsion is sterilized at 65 ° C to 150 ° C. For sterilization, a plate sterilizer, a tubular sterilizer, an infusion sterilizer, an injection sterilizer, a batch sterilizer, or the like can be used.
Further, the sterilized emulsion is cooled to 0 to 10 ° C. and aged for about 4 to 24 hours. Aging is to crystallize fat globules in the emulsion and stabilize the emulsion film. When aging is performed here, the physical properties of the emulsion tend to be stabilized.

上記過程を経た、乳化液を、連続式フリーザーを用いてフリージングし、半凍結液を得る。
連続式フリーザーとは、連続的に冷却と攪拌を行い、アイスクリームを製造するフリーザーのことをいう。
また、フリージングとは、乳化液を冷却すると同時に適量の空気を混入して、気泡や氷の粒を乳化液中に分散させることをいう。乳化液をフリージングすることで、適度な空気と微細な氷結晶を有する半凍結液を得ることができる。
本発明の冷菓を製造するにあたり、フリージングの際の温度は−6.5〜−7.5℃であると好ましい。
フリージングの温度がこの範囲内であれば、氷結晶が微細で滑らかな組織を有する冷菓が得られる傾向にある。対して、フリージングの温度が−6.5℃を超えると、氷結晶が粗大で組織の粗い冷菓になりやすく、−7.5℃未満であると、乳化液が硬くなりすぎ、製造上の不備が生じやすくなる。
The emulsion that has undergone the above process is frozen using a continuous freezer to obtain a semi-frozen solution.
A continuous freezer refers to a freezer that produces ice cream by continuously cooling and stirring.
Freezing means that an appropriate amount of air is mixed at the same time that the emulsion is cooled to disperse bubbles and ice particles in the emulsion. By freezing the emulsion, a semi-frozen solution having appropriate air and fine ice crystals can be obtained.
In producing the frozen dessert of the present invention, the temperature during freezing is preferably −6.5 to −7.5 ° C.
If the freezing temperature is within this range, a frozen dessert having fine and smooth ice crystals tends to be obtained. On the other hand, if the freezing temperature exceeds −6.5 ° C., the ice crystals are coarse and tend to become a frozen dessert with a coarse structure, and if it is less than −7.5 ° C., the emulsified liquid becomes too hard, resulting in manufacturing defects. Is likely to occur.

以上のようにして得られた半凍結液を、容器に充填し、包装した後硬化させると本発明の冷菓を得ることができる。   The frozen dessert of the present invention can be obtained by filling the semi-frozen solution obtained as described above into a container, packaging, and curing.

以上のように本発明の冷菓はバターミルクを含有しており、これが乳化作用を示すため、卵や食品添加物である乳化剤を添加しなくてもよい。
また、本発明の冷菓の製造方法では、バターミルクを含有させた乳化液をフリージングするため、乳化剤及び安定剤等の食品添加物を用いなくても、脂肪球が凝集しにくく、脂肪粒が発生し難い。更に、フリージング温度が所定の範囲であることより、乳化剤及び安定剤等の食品添加物を用いなくても、微細な氷結晶や滑らかな組織を有した風味のよい冷菓を得ることができる。
As described above, the frozen dessert of the present invention contains buttermilk, which exhibits an emulsifying action, so that it is not necessary to add an emulsifier which is an egg or a food additive.
Further, in the method for producing frozen confectionery of the present invention, since the emulsion containing buttermilk is frozen, fat globules are hardly aggregated and fat granules are generated without using food additives such as emulsifiers and stabilizers. It is hard to do. Furthermore, since the freezing temperature is in a predetermined range, a tasty frozen dessert having fine ice crystals and a smooth structure can be obtained without using food additives such as emulsifiers and stabilizers.

以下、本発明を試験例により具体的に説明するが、本発明はこれらに限定されるものではない。   EXAMPLES Hereinafter, although this invention is demonstrated concretely by a test example, this invention is not limited to these.

[試験1]
本試験は、従来の乳化安定剤に代えてバターミルクを添加したアイスクリームと乳化安定剤を配合しないアイスクリームとを連続式フリーザーで製造し、乳化安定性を比較検討した。
[Test 1]
In this test, ice cream with buttermilk added in place of the conventional emulsion stabilizer and ice cream with no emulsion stabilizer were produced in a continuous freezer, and the emulsion stability was compared.

(1)試験試料の調製
<配合1>
アイスクリームの調製は、常法の手順に基づいて行った。
すなわち、まず原料である、脱脂粉乳(森永脱脂粉乳、森永乳業(株)製)、無塩バター(森永バター、森永乳業(株)製)、グラニュー糖(MEグラニュー、大日本明治製糖製)、異性化液糖(FS−551、三和澱粉工業製)及び水飴(K−SPD−M、昭和産業(株)製)を表1に記載の配合にて、70℃に加温した溶解水に混合溶解し、二段均質機(サンマル社製)を使用して、温度70℃、2次圧:5MPa、全圧:15MPaで均質化した。
次に、均質化した原料を、連続式プレート殺菌機(MD−Plate Exchanger、森永エンジニアリング社製)にて、85℃−15秒の条件で殺菌し、その後、5℃で24時間エージングし、配合1の乳化液を得た。
<配合2>
原料として、バターミルクパウダー(SM−2powder、固形分96.75質量%、無脂乳固形分81.78質量%、CORMAN製)を配合した他は配合1と同様にして、配合2の乳化液を得た。なお、配合2の乳化液中には乳リン脂質が0.45質量%含まれていた。
なお、乳リン脂質は、フローインジェクション分析法(FIA法)を使用して測定した。
(1) Preparation of test sample <Formulation 1>
Ice cream was prepared based on a conventional procedure.
That is, first of all, the raw materials are skim milk powder (Morinaga skim milk powder, Morinaga Milk Co., Ltd.), salt-free butter (Morinaga butter, Morinaga Milk Co., Ltd.), granulated sugar (ME granulated, manufactured by Dainippon Meiji Sugar Co., Ltd.), Isomerized liquid sugar (FS-551, manufactured by Sanwa Starch Kogyo Co., Ltd.) and Minamata (K-SPD-M, manufactured by Showa Sangyo Co., Ltd.) were added to the dissolved water heated to 70 ° C. with the formulation shown in Table 1. The mixture was dissolved and homogenized at a temperature of 70 ° C., a secondary pressure of 5 MPa, and a total pressure of 15 MPa using a two-stage homogenizer (manufactured by Sanmaru).
Next, the homogenized raw material is sterilized under conditions of 85 ° C. to 15 seconds with a continuous plate sterilizer (MD-Plate Exchanger, manufactured by Morinaga Engineering Co., Ltd.), and then aged at 5 ° C. for 24 hours, and blended 1 emulsion was obtained.
<Formulation 2>
Emulsion of Formulation 2 in the same manner as Formulation 1 except that buttermilk powder (SM-2 powder, solid content 96.75% by mass, nonfat milk solid content 81.78% by mass, manufactured by CORMAN) was used as a raw material Got. In addition, 0.45% by mass of milk phospholipid was contained in the emulsion of Formulation 2.
Milk phospholipids were measured using a flow injection analysis method (FIA method).

Figure 2009232750
Figure 2009232750

<試験試料1〜4>
配合1の乳化液を用い、連続式フリーザーCS−200(SEREN社製)を用いて、−4.5℃、−5.5℃、−6.5℃及び−7.5℃でそれぞれフリージングした。なお、フリージング条件は、乳化液流量70L/h、オーバーラン100%、ダッシャー回転数222rpm、シリンダー内圧400barとした。
このようにしてフリージングしたものをそれぞれ130mlのカップに入れ、−35℃の急速冷凍庫で硬化させて試験試料1〜4のアイスクリームを得た。
得られた試験試料1〜4のアイスクリームの組成は、いずれも乳脂肪分9.5質量%、無脂乳固形分9.8質量%、全固形分37.3質量%であった。
<Test samples 1 to 4>
Using the emulsified liquid of Formulation 1, it was subjected to freezing at −4.5 ° C., −5.5 ° C., −6.5 ° C. and −7.5 ° C. using a continuous freezer CS-200 (manufactured by SEREN). . The freezing conditions were an emulsion flow rate of 70 L / h, an overrun of 100%, a dasher rotation speed of 222 rpm, and a cylinder internal pressure of 400 bar.
Each of the freezing pieces thus obtained was put into a 130 ml cup and cured in a quick freezer at -35 ° C. to obtain ice creams of test samples 1 to 4.
The composition of the ice creams of the obtained test samples 1 to 4 each had a milk fat content of 9.5% by mass, a non-fat milk solid content of 9.8% by mass, and a total solid content of 37.3% by mass.

<試験試料5〜8>
配合2の乳化液を用い、試験試料1〜4と同様にして試験試料5〜8のアイスクリームを得た。
得られた試験試料5〜8のアイスクリームの組成は、いずれも乳脂肪分9.5質量%、無脂乳固形分9.8質量%、全固形分37.3質量%であった。
<Test samples 5 to 8>
Using the emulsion of Formulation 2, ice creams of Test Samples 5 to 8 were obtained in the same manner as Test Samples 1 to 4.
The compositions of the obtained ice creams of test samples 5 to 8 each had a milk fat content of 9.5% by mass, a nonfat milk solid content of 9.8% by mass, and a total solid content of 37.3% by mass.

(2)試験方法
<粒度分布測定>
粒度分布測定装置LA−500(HORIBA社製)を用いて測定を行った。すなわち、試験試料1〜8それぞれ3gを15℃のイオン交換水を用いて10倍に希釈した後、一昼夜静置して気泡を脱気させる。その後、さらにそれぞれの試料をさらにイオン交換水を用いて100倍から5000倍に希釈し、測定器に供して脂肪球の粒子径を測定し、50μm以上の脂肪球が発生の有無について調べた。結果を表2及び表3に示す。
(2) Test method <Particle size distribution measurement>
Measurement was performed using a particle size distribution measuring apparatus LA-500 (manufactured by HORIBA). That is, 3 g of each of the test samples 1 to 8 was diluted 10 times with ion-exchanged water at 15 ° C., and then left to stand overnight to degas bubbles. Thereafter, each sample was further diluted 100-fold to 5000-fold with ion-exchanged water and subjected to a measuring device to measure the fat globule particle size, and the presence or absence of 50 μm or more fat globules was examined. The results are shown in Tables 2 and 3.

<セジメントテスト>
試験試料1〜8それぞれ1gを50g(15℃)のイオン交換水に溶解したものを、MILK SEDIMENT DISK 1026−B(ADVANTEC社製)を用いてろ過し、ろ紙に残った脂肪粒の残渣の有無について調べた。結果を表2及び表3に示す。
<Sediment Test>
1 g of each of test samples 1 to 8 was dissolved in 50 g (15 ° C.) of ion-exchanged water, filtered using MILK SEDIMENT DISK 1026-B (manufactured by ADVANTEC), and presence or absence of residue of fat particles remaining on the filter paper Investigated about. The results are shown in Tables 2 and 3.

Figure 2009232750
Figure 2009232750

Figure 2009232750
Figure 2009232750

(3)試験結果
表2及び表3における粒度分布測定の結果を比較すると、バターミルクを添加しない配合1を用いた試験試料1〜4では、フリージング温度が低温である試験試料3および4で直径50μm以上の脂肪球が発生していた。対して、バターミルクを添加した配合2を用いた試験試料5〜8では、試験試料5及び6は勿論、フリージング温度が低温である試験試料7および8でも直径50μm以上の脂肪球は確認されなかった。
また、表2及び表3におけるセジメントテストの結果を比較すると、バターミルクを添加しない配合1を用いた試験試料1〜4では、フリージング温度が低温である試験試料3および4で脂肪粒の残滓が確認された。対して、バターミルクを添加した配合2を用いた試験試料5〜8では、試験試料5及び6は勿論、フリージング温度が低温である試験試料7および8でも脂肪粒の残滓が確認されなかった。
以上の粒度分布及びセジメントテストの結果より、バターミルクを添加すると、油脂が乳化されて細かい脂肪球となり、−6.5℃や−7.5℃の低温でフリージングを行っても、製品中に脂肪粒が発生しにくくなるということがわかった。つまり、バターミルクは、製品の乳化安定性に寄与すると考えられる。
(3) Test results Comparing the results of particle size distribution measurement in Table 2 and Table 3, in Test Samples 1 to 4 using Formulation 1 to which no buttermilk was added, the diameters of Test Samples 3 and 4 having a low freezing temperature Fat globules of 50 μm or more were generated. On the other hand, in test samples 5 to 8 using Formulation 2 to which buttermilk was added, not only test samples 5 and 6, but also test samples 7 and 8 having a low freezing temperature, fat globules having a diameter of 50 μm or more were not confirmed. It was.
Moreover, when the results of the segment test in Table 2 and Table 3 are compared, in Test Samples 1 to 4 using Formulation 1 in which buttermilk is not added, the residue of fat granules is found in Test Samples 3 and 4 having a low freezing temperature. confirmed. On the other hand, in the test samples 5 to 8 using the formulation 2 to which buttermilk was added, not only the test samples 5 and 6, but also the test samples 7 and 8 having a low freezing temperature, no fat granule residue was confirmed.
From the results of the particle size distribution and the sediment test, when buttermilk is added, the fats and oils are emulsified into fine fat globules. Even if freezing is performed at a low temperature of -6.5 ° C or -7.5 ° C, It was found that fat particles are less likely to occur. That is, buttermilk is thought to contribute to the emulsion stability of the product.

[試験2]
本試験は、バターミルクが乳化安定剤不使用のアイスクリーム組織に、好ましい組織と風味を与えることができる適用範囲を確認することを目的とする。
[Test 2]
The purpose of this test is to confirm the application range in which buttermilk can give a preferable structure and flavor to an ice cream structure not using an emulsion stabilizer.

(1)試験試料の調製
<配合3>
表4に記載の配合の、脱脂粉乳、無塩バター、グラニュー糖、異性化液糖及び水飴に溶解水を加えて攪拌しながら湯せんで85℃まで昇温した後、二段均質機(サンマル社製)を使用して、温度:85℃、2次圧:5MPa、全圧:15MPaで均質化した。これを、5℃で24時間エージングし配合3の乳化液を得た。
なお、配合3の乳化液中には乳リン脂質が0.5質量%含まれていた。
(1) Preparation of test sample <Formulation 3>
After adding dissolved water to skim milk powder, unsalted butter, granulated sugar, isomerized liquid sugar and chickenpox with the composition shown in Table 4, the temperature was raised to 85 ° C. with a water bath while stirring, and then a two-stage homogenizer (Sanmaru Corporation) The pressure was homogenized at a temperature of 85 ° C., a secondary pressure of 5 MPa, and a total pressure of 15 MPa. This was aged at 5 ° C. for 24 hours to obtain an emulsion of Formulation 3.
The emulsion 3 contained 0.5% by mass of milk phospholipid.

<配合4〜8>
表4に記載の配合に従い、配合3と同様にして、配合4〜8の乳化液を得た。
なお、配合4の乳化液中には乳リン脂質が0.4質量%含まれていた。配合5の乳化液中には乳リン脂質が0.3質量%含まれていた。配合6の乳化液中には乳リン脂質が0.1質量%含まれていた。配合7の乳化液中には乳リン脂質が0.05質量%含まれていた。配合8の乳化液中には乳リン脂質が0.03質量%含まれていた。
<Formulation 4-8>
According to the formulation shown in Table 4, in the same manner as in formulation 3, emulsions of formulations 4 to 8 were obtained.
In addition, 0.4 mass% of milk phospholipid was contained in the emulsion of Formulation 4. The emulsion of Formulation 5 contained 0.3% by mass of milk phospholipid. The emulsion of Formulation 6 contained 0.1% by mass of milk phospholipid. The emulsion of Formulation 7 contained 0.05% by mass of milk phospholipid. The emulsion of Formulation 8 contained 0.03% by mass of milk phospholipid.

Figure 2009232750
Figure 2009232750

<試験試料9〜16>
表5に記載のとおり、配合3〜8及び配合1の乳化液をそれぞれ、連続式フリーザーCS−200を用いて、−7.5℃でフリージングした。
なお、フリージング条件は、乳化液流量70L/h、オーバーラン100%、ダッシャー回転数222rpm、シリンダー内圧400barとした。
フリージングしたものをそれぞれ130mlのカップに入れ、−35℃の急速冷凍庫で硬化させて試験試料9〜16のアイスクリームを得た。
得られた試験試料9〜16のアイスクリームの組成は、いずれも乳脂肪分9.5質量%、無脂乳固形分9.8質量%、全固形分37.3質量%であった。
<Test samples 9 to 16>
As shown in Table 5, each of the emulsions of Formulations 3 to 8 and Formulation 1 was frozen at -7.5 ° C using a continuous freezer CS-200.
The freezing conditions were an emulsion flow rate of 70 L / h, an overrun of 100%, a dasher rotation speed of 222 rpm, and a cylinder internal pressure of 400 bar.
Each of the frozen items was placed in a 130 ml cup and cured in a quick freezer at −35 ° C. to obtain ice creams of test samples 9 to 16.
As for the composition of the ice cream of the obtained test samples 9-16, all were milk fat content 9.5 mass%, non-fat milk solid content 9.8 mass%, and total solid content 37.3 mass%.

(2)試験方法
<粒度分布測定>
粒度分布測定装置LA−500(HORIBA社製)を用いて測定を行った。すなわち、試験試料9〜16それぞれ3gを15℃のイオン交換水を用いて10倍に希釈した後、一昼夜静置して気泡を脱気させる。その後、さらにそれぞれの試料をさらにイオン交換水を用いて100倍から5000倍に希釈し、測定器に供して脂肪球の粒子径を測定し、50μm以上の脂肪球及び30μm以上の脂肪球が発生しているか否かについて調べた。結果を表5に示す。
(2) Test method <Particle size distribution measurement>
Measurement was performed using a particle size distribution measuring apparatus LA-500 (manufactured by HORIBA). That is, 3 g of each of the test samples 9 to 16 was diluted 10 times with ion-exchanged water at 15 ° C., and then allowed to stand overnight to degas bubbles. After that, each sample is further diluted 100-fold to 5000-fold with ion-exchanged water, and the particle size of fat globules is measured by using a measuring device, and 50 μm or more fat globules and 30 μm or more fat globules are generated. I investigated whether or not. The results are shown in Table 5.

Figure 2009232750
Figure 2009232750

(3)試験結果
表5における粒度分布測定の結果を比較すると、バターミルクの配合割合が固形分で5.0質量%未満の試験試料13〜16では、バターミルクの配合量が多いほど脂肪球の発生が抑制される傾向はあるものの、直径50μm以上の脂肪球の発生が見られた。対して、バターミルクが固形分で5.0質量%以上含有されている配合では、直径50μm以上の脂肪球は見られなかった。
以上より、バターミルクが固形分で5.0質量%以上含有されていると、フリージング中の脂肪球の凝集を制御し、より脂肪粒の発生を抑えられるといえる。
一方、試験試料9〜16においては、脱脂粉乳や無塩バターの量を調整することにより、試験試料全体の乳脂肪分、無脂乳固形分及び固形分の組成を同一とすることができた。従ってこれらの組成を変更させずに、バターミルクを配合するには、バターミルクを固形分で10質量%以下とすることが好ましい。バターミルクの配合量が固形分で10質量%を超えると、脱脂粉乳や無塩バターの量を調整しても、試験試料全体の乳脂肪分、無脂乳固形分及び固形分の組成を同一とすることが難しくなる。
従って、脂肪粒の発生による組織の劣化を防ぎ、安定的にフリージングを行うには、バターミルクの配合割合が固形分で5.0%以上かつ10質量%以下であることが望ましい。
更に、バターミルクの配合割合が固形分で7.0質量%以上であると、直径30μm以上の脂肪球の発生が見られない。これにより、バターミルクの配合割合は、固形分で7.0質量%以上かつ10.0質量%以下であることが特に望ましい。
(3) Test results Comparing the results of the particle size distribution measurement in Table 5, in test samples 13 to 16 in which the blending ratio of buttermilk is less than 5.0% by mass in solid content, the more buttermilk is blended, the more fat globule Although there is a tendency to suppress the generation of fat, the generation of fat globules with a diameter of 50 μm or more was observed. On the other hand, fat globules with a diameter of 50 μm or more were not observed in the blend containing buttermilk in a solid content of 5.0% by mass or more.
From the above, it can be said that when the buttermilk is contained in a solid content of 5.0% by mass or more, aggregation of fat globules during freezing can be controlled and generation of fat particles can be further suppressed.
On the other hand, in test samples 9-16, the composition of milk fat content, non-fat milk solid content, and solid content of the whole test sample could be made the same by adjusting the amount of skim milk powder and salt-free butter. . Therefore, in order to mix buttermilk without changing these compositions, it is preferable that the buttermilk is 10% by mass or less in terms of solid content. If the amount of buttermilk blended exceeds 10% by mass, the composition of milk fat, nonfat milk solids and solids in the entire test sample will be the same even if the amount of skim milk powder or unsalted butter is adjusted. It becomes difficult to do.
Therefore, in order to prevent tissue deterioration due to the generation of fat particles and to perform freezing stably, it is desirable that the blending ratio of butter milk is 5.0% or more and 10% by mass or less in terms of solid content.
Furthermore, when the blending ratio of butter milk is 7.0% by mass or more in terms of solid content, generation of fat globules having a diameter of 30 μm or more is not observed. Thereby, as for the mixture ratio of buttermilk, it is especially desirable that it is 7.0 mass% or more and 10.0 mass% or less by solid content.

本発明の冷菓は、食品添加物である乳化剤及び安定剤を使用しない健康志向に沿いながら良好な組織をもった冷菓として好適である。   The frozen dessert according to the present invention is suitable as a frozen dessert having a good structure while keeping the health orientation without using an emulsifier and a stabilizer which are food additives.

Claims (4)

油脂と、バターミルクとを含有する冷菓。   A frozen dessert containing fat and buttermilk. 前記バターミルクを固形分で5.0〜10.0質量%含有する請求項1に記載の冷菓。   The frozen dessert according to claim 1, containing 5.0 to 10.0% by mass of the buttermilk in solid content. 油脂とバターミルクとを含有する原料液を混合して乳化液を得た後、該乳化液をフリージングする冷菓の製造方法。   A method for producing a frozen dessert, wherein an emulsion is obtained by mixing raw material liquids containing fats and fats and buttermilk, and then the emulsion is frozen. 前記フリージングを、連続式フリーザーを用いて−6.5〜−7.5℃の範囲で行う、請求項3記載の冷菓の製造方法。   The manufacturing method of the frozen dessert of Claim 3 which performs the said freezing in the range of -6.5 to -7.5 degreeC using a continuous freezer.
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Publication number Priority date Publication date Assignee Title
CN113365504A (en) * 2019-04-04 2021-09-07 罗蒂株式会社 Frozen dessert and method for enriching the flavour of a frozen dessert

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60186251A (en) * 1984-02-07 1985-09-21 ルケツト・フレール Sugarless ice cream and its production
JPH04144646A (en) * 1990-10-03 1992-05-19 Nissei Kk Soft ice cream
JPH04346750A (en) * 1991-05-21 1992-12-02 Shimizu Kagaku Kk Method for emulsifying raw material in production of processed food

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60186251A (en) * 1984-02-07 1985-09-21 ルケツト・フレール Sugarless ice cream and its production
JPH04144646A (en) * 1990-10-03 1992-05-19 Nissei Kk Soft ice cream
JPH04346750A (en) * 1991-05-21 1992-12-02 Shimizu Kagaku Kk Method for emulsifying raw material in production of processed food

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113365504A (en) * 2019-04-04 2021-09-07 罗蒂株式会社 Frozen dessert and method for enriching the flavour of a frozen dessert

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