JP2009095809A - Removing method and apparatus for deposited sludge in storage tank - Google Patents

Removing method and apparatus for deposited sludge in storage tank Download PDF

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JP2009095809A
JP2009095809A JP2007272344A JP2007272344A JP2009095809A JP 2009095809 A JP2009095809 A JP 2009095809A JP 2007272344 A JP2007272344 A JP 2007272344A JP 2007272344 A JP2007272344 A JP 2007272344A JP 2009095809 A JP2009095809 A JP 2009095809A
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storage tank
cleaning
sludge
liquid
tank
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Koji Sato
幸治 佐藤
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JFE Chemical Corp
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JFE Chemical Corp
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Abstract

<P>PROBLEM TO BE SOLVED: To remove sludge by preventing leakage of odor and vapor in a storage tank and low-boiling temperature components in sludge to the outside of the tank by removing the sludge in a sealed system in a cleaning process of deposited sludge in the storage tank. <P>SOLUTION: Cleaning pipes 4 having spray nozzles 6 near the tips are fixed at existing manholes 3 in a top plate 2 of the storage tank 1 in such a manner as to be sealed and turnable in the peripheral direction of the cleaning pipes. A storage liquid and/or a cleaning liquid 14 are/is jetted from the spray nozzles 6, the deposited sludge 13 in the storage tank 1 is suspended in the storage liquid and/or the cleaning liquid 14 to be extracted from the storage tank 1, and the extracted storage liquid and/or the cleaning liquid 14 is returned to the cleaning pipes 4. <P>COPYRIGHT: (C)2009,JPO&INPIT

Description

本発明は、コールタール、原油、重油等を貯蔵する貯蔵タンク内に堆積したスラッジの除去方法および装置に関するものである。   The present invention relates to a method and an apparatus for removing sludge accumulated in a storage tank for storing coal tar, crude oil, heavy oil and the like.

危険物貯蔵タンクのうち、1000キロリットルを超えるものは、消防法により10年に一度の開放点検が義務付けられている。
開放点検の際には、タンク底板まで検査するためタンク内の堆積スラッジの掃除が必要となる。タンク内の堆積スラッジは、重質油中に含有される重質物、ピッチ、石炭・コークス粉がタンク底部に沈降し、堆積したものである。
Of the hazardous material storage tanks, those exceeding 1000 kiloliters are required to be inspected once every 10 years under the Fire Service Act.
During open inspection, it is necessary to clean the accumulated sludge in the tank to inspect up to the tank bottom plate. The sediment sludge in the tank is a sediment in which heavy matter, pitch, and coal / coke powder contained in the heavy oil settle to the bottom of the tank.

従来、タンク内スラッジの掃除は、タンク内の液を抜出した後、タンク内下部の側板マンホールを開放して、人力で堆積スラッジをタンク外へ排出していた。また、堆積スラッジの高さが側板マンホールより高く、圧密されて硬くなっている場合は、蒸気配管をスラッジ内に差込み蒸気の圧力と熱で堆積スラッジを粉砕し、溶媒中へ懸濁させてタンク外へ排出し、側板マンホールが開放できる位置まで堆積スラッジの高さを下げていた。   Conventionally, in the cleaning of sludge in the tank, after draining the liquid in the tank, the side plate manhole in the lower part of the tank is opened, and the accumulated sludge is discharged manually from the tank. Also, if the height of the accumulated sludge is higher than the side plate manhole, and it is hardened by consolidation, the steam sludge is crushed with the pressure and heat of the steam, and suspended in the solvent. The height of the accumulated sludge was lowered to the position where the side plate manhole could be opened.

しかし、これらの方法では、開放系で実施するためにタンク外にタンク内の臭気やベーパーが漏洩するといった問題があった。また、タンク内の作業環境は、臭気やベーパーが充満し、夏場はタンク内の温度や湿度が高く、長時間のスラッジ排出作業は困難であった。人力に代わるタンク内堆積スラッジの処理方法として、タンク内の貯蔵液、洗浄油などの洗浄液を循環させることによって、スラッジを懸濁させて抜出す方法が行われているが、この方法では洗浄液を循環させる位置が一箇所に限定され、限られた範囲にある堆積スラッジのみの処理になるという問題がある。   However, since these methods are implemented in an open system, there is a problem that odors and vapor in the tank leak outside the tank. In addition, the working environment in the tank was filled with odors and vapors, and the temperature and humidity in the tank were high in summer, making it difficult to discharge sludge for a long time. As a method of treating accumulated sludge in tanks instead of human power, a method of suspending and removing sludge by circulating cleaning liquid such as storage liquid and cleaning oil in the tank is performed. There is a problem that the position to circulate is limited to one place, and only the deposited sludge in a limited range is processed.

また、もう少し積極的な堆積スラッジの除去方法として、特許文献1では、タンクの側壁に所定間隔で進退自在に設置した洗浄管により、タンク内の共液または洗浄液を堆積スラッジに向けて近傍より噴出して、堆積スラッジを撹拌、分散、溶解させタンク外に抜出すことを提案している。
この方法では、使用しているタンクの側壁に複数個所、洗浄管を設置する孔を設ける必要があるが、危険物を貯蔵しているタンクを使用しながら、側壁に孔をあけることは、安全上、消防法上も難しい。また、タンク内堆積スラッジは、タンク壁面内側部にも堆積しているため、堆積スラッジの高さよりも低い部分の側壁に孔をあけることは現実的には難しい。
In addition, as a more aggressive method for removing the accumulated sludge, in Patent Document 1, the common liquid or the cleaning liquid in the tank is spouted from the vicinity toward the accumulated sludge by a cleaning pipe installed on the side wall of the tank so as to freely advance and retreat at predetermined intervals. Thus, it is proposed to stir, disperse and dissolve the deposited sludge and extract it out of the tank.
In this method, it is necessary to provide multiple holes on the side wall of the tank used to install cleaning pipes. However, it is safe to make a hole in the side wall while using a tank that stores hazardous materials. In addition, it is difficult under the Fire Service Law. In addition, since the accumulated sludge in the tank is also accumulated on the inner side of the tank wall surface, it is practically difficult to make a hole in the side wall of the portion lower than the height of the accumulated sludge.

仮に孔を空けて洗浄管を差し込んでも洗浄管設置部がタンク内液部であるため、シール部からの漏れ等、安全上問題がある。また、堆積スラッジの高さ方向全体に洗浄液を噴射するためには、洗浄管の設置孔をタンクの高さ方向、周方向に複数個設ける必要があり、安全上難しく、堆積スラッジの処理コストも高くなる。
また、洗浄管を他の孔へ抜き替える場合もタンクは開放系となる場合があり、液、タンク内臭気もしくはベーパーは漏洩する問題もある。
特開2001−276765号公報
Even if the cleaning pipe is inserted with a hole, the cleaning pipe installation part is the liquid part in the tank, so there are safety problems such as leakage from the seal part. In addition, in order to inject the cleaning liquid to the entire height direction of the accumulated sludge, it is necessary to provide a plurality of cleaning tube installation holes in the height direction and circumferential direction of the tank. Get higher.
In addition, when the cleaning pipe is replaced with another hole, the tank may be an open system, and there is a problem that liquid, odor in the tank or vapor leaks.
JP 2001-276765 A

本発明は、タンク内堆積スラッジの掃除過程において、密閉系でスラッジ除去を行い、タンク内の臭気やベーパーおよびスラッジ中の低沸点成分のタンク外への漏洩を防止することが可能なタンク内堆積スラッジの除去方法および装置を提供することを目的とする。   In the process of cleaning the sludge in the tank, the present invention removes sludge in a closed system, and prevents the odor in the tank and the leakage of low boiling point components in the vapor and sludge to the outside of the tank. An object is to provide a method and apparatus for removing sludge.

本発明は、貯蔵タンクに堆積したスラッジの除去方法であって、該貯蔵タンクのタンク天板の既存マンホールに、先端近傍に噴出ノズルを有する洗浄用管を密閉かつ該洗浄用管の周方向に回動可能に固定し、前記噴出ノズルから貯蔵液および/または洗浄液を噴出させ、前記スラッジを貯蔵液および/または洗浄液に懸濁させて、該貯蔵タンク内から抜出しするとともに、抜出した貯蔵液および/または洗浄液を前記洗浄用管へ返送することを特徴とする貯蔵タンク内堆積スラッジの除去方法である。   The present invention is a method for removing sludge accumulated in a storage tank, wherein a cleaning pipe having a jet nozzle near the tip is sealed in a circumferential direction of the cleaning pipe in an existing manhole on a tank top plate of the storage tank. The storage liquid and / or the cleaning liquid are ejected from the ejection nozzle, the sludge is suspended in the storage liquid and / or the cleaning liquid, and is extracted from the storage tank, and the extracted storage liquid and A method of removing accumulated sludge in a storage tank, wherein the cleaning liquid is returned to the cleaning pipe.

また、本発明は、貯蔵タンクに堆積したスラッジの除去装置であって、先端に噴出ノズルを有し、前記貯蔵タンクのタンク天板の既存マンホールに密閉かつ周方向に回動可能に固定された洗浄用管と、前記貯蔵タンクの底部近傍に接続されて貯蔵液および/または洗浄液を抜き出しする抜出管と、吸込み側が前記抜出管と接続され、吐出側が接続配管に接続されて抜出された貯蔵液および/または洗浄液を前記洗浄用管へ返送する循環ポンプと、該循環ポンプの吐出側で前記接続配管と切換可能に接続されて前記貯蔵タンク内の貯蔵液および/または洗浄液を前記貯蔵タンク外へ排出する排出管と、を有することを特徴とする貯蔵タンク内堆積スラッジの除去装置である。   Further, the present invention is a device for removing sludge accumulated in a storage tank, having a jet nozzle at the tip, and being fixed to an existing manhole on the tank top plate of the storage tank so as to be capable of rotating in a circumferential direction. A cleaning pipe, an extraction pipe connected to the vicinity of the bottom of the storage tank and extracting the storage liquid and / or cleaning liquid, a suction side connected to the extraction pipe, and a discharge side connected to a connection pipe and extracted. A circulating pump for returning the stored liquid and / or the cleaning liquid to the cleaning pipe, and the storage liquid and / or the cleaning liquid in the storage tank connected to the connection pipe on the discharge side of the circulating pump in a switchable manner. An apparatus for removing accumulated sludge in a storage tank, comprising: a discharge pipe that discharges outside the tank.

本発明によれば、密閉系で安全かつ容易にタンク内の堆積スラッジに対して貯蔵液および/または洗浄液を高流速で噴出し、堆積スラッジを粉砕し、懸濁させ、抜出し処理することが可能となる。   According to the present invention, the storage liquid and / or the cleaning liquid can be ejected at high flow rate against the accumulated sludge in the tank safely and easily in a closed system, and the accumulated sludge can be pulverized, suspended, and extracted. It becomes.

本発明の実施例を図1に基づいて説明する。図1は、本発明によるタンク内堆積スラッジの除去装置の一例を示すフロー図であり、図2は、図1のA部を拡大して示す説明図である。
図1において、貯蔵タンク1のタンク天板2に設けられているマンホール(既設)3に洗浄用管4を立設する。洗浄用管4はマンホール3との接続部でスイベルジョイント5を介して設置されており、360度回動可能となっている。
An embodiment of the present invention will be described with reference to FIG. FIG. 1 is a flow chart showing an example of a tank sludge removal apparatus according to the present invention, and FIG. 2 is an explanatory diagram showing an enlarged view of part A in FIG.
In FIG. 1, a cleaning pipe 4 is erected in a manhole (existing) 3 provided on a tank top plate 2 of a storage tank 1. The cleaning tube 4 is installed through a swivel joint 5 at the connection with the manhole 3 and can be rotated 360 degrees.

洗浄用管4の口径は、マンホール径以下であればいくらでもよいが、100〜200mm以下が取り扱い易い。また、洗浄用管の設置数は、タンクの大きさ(径)や堆積スラッジの量により決定するが、2〜3本を均等に設置するのが好ましい。
洗浄用管4のタンク内先端近傍には、貯蔵液および/または洗浄液14の噴出流速を上げ、効果的に堆積スラッジを粉砕、懸濁するため噴出ノズル6を設置する。噴出ノズル6の装着は、溶接、ねじ込みまたはボルト固定とし、図2に示すように堆積スラッジの高さに合わせて3〜4個設置する。噴出ノズル6の先端はキャップで封止できる構造とし、使用している噴出ノズルの流速を上げるようにしてもよい。
The diameter of the cleaning tube 4 is not limited as long as it is equal to or smaller than the manhole diameter, but is easily handled at 100 to 200 mm. The number of cleaning pipes is determined by the size (diameter) of the tank and the amount of accumulated sludge, but it is preferable that two or three pipes are installed equally.
In the vicinity of the front end of the cleaning pipe 4 in the tank, an ejection nozzle 6 is installed to increase the ejection flow rate of the storage liquid and / or the cleaning liquid 14 and effectively pulverize and suspend the accumulated sludge. The ejection nozzle 6 is attached by welding, screwing or bolt fixing, and 3 to 4 nozzles are installed according to the height of the accumulated sludge as shown in FIG. The tip of the ejection nozzle 6 may be sealed with a cap, and the flow velocity of the ejection nozzle being used may be increased.

噴出ノズル6のサイズは、洗浄用管4の直径より小さければいくらでもよいが、より噴出効果を上げるには50mm以下とするのが好ましい。また、噴出角度は、洗浄用管4の長さ方向に対して90度程度が望ましい。
洗浄用管4は、フレキシブルホース7、接続配管8を介して、加温器9、循環ポンプ10の吐出側に接続されている。循環ポンプ10の吸込み側は、貯蔵タンク1に既存の抜出管11に接続され、吐出側は、接続配管8と、あるいは切換弁16を介して排出管15と接続されており、切換弁16の操作で循環している貯蔵液および/または洗浄液14を、洗浄用管4あるいは排出管15のいずれか一方に供給できるように構成している。
The size of the ejection nozzle 6 may be any size as long as it is smaller than the diameter of the cleaning tube 4, but is preferably 50 mm or less in order to further increase the ejection effect. The ejection angle is preferably about 90 degrees with respect to the length direction of the cleaning tube 4.
The cleaning pipe 4 is connected to the discharge side of the warmer 9 and the circulation pump 10 via a flexible hose 7 and a connection pipe 8. The suction side of the circulation pump 10 is connected to the existing extraction pipe 11 in the storage tank 1, and the discharge side is connected to the connection pipe 8 or the discharge pipe 15 via the switching valve 16. The storage liquid and / or the cleaning liquid 14 circulated by the above operation can be supplied to either the cleaning pipe 4 or the discharge pipe 15.

接続管8の途中に設けた加温器9は、加熱源として蒸気12を使用し、堆積スラッジ13の粉砕、懸濁に最適温度で循環するように貯蔵液および/または洗浄液14を加温する構成としている。
貯蔵タンク1内の堆積スラッジ13の処理に際しては、洗浄用管4をタンク天板2のマンホール3から貯蔵タンク1内に降ろしながら堆積スラッジ13内に装入し、タンク底板に立設する。
A heater 9 provided in the middle of the connecting pipe 8 uses steam 12 as a heating source, and heats the storage liquid and / or the cleaning liquid 14 so as to circulate at an optimum temperature for pulverization and suspension of the accumulated sludge 13. It is configured.
When processing the accumulated sludge 13 in the storage tank 1, the cleaning pipe 4 is loaded into the accumulated sludge 13 while being lowered into the storage tank 1 from the manhole 3 of the tank top plate 2 and is erected on the tank bottom plate.

その後、循環ポンプ10によって貯蔵タンク1内から貯蔵液および/または洗浄液14を抜出し、加温器9で加温後、洗浄用管4を介して、噴出ノズル6から高流速で貯蔵液および/または洗浄液14を堆積スラッジ13に向けて噴出し、堆積スラッジ13を粉砕し、懸濁させる。次いで、洗浄用管4を回動させて角度を変えて先端部の噴出ノズル6の噴出方向を変更することにより、貯蔵タンク1内の堆積スラッジ13を満遍なく粉砕し、懸濁させることができる。この操作を繰り返して行い、貯蔵液および/または洗浄液14中のスラッジ濃度が高くなったとき、貯蔵液および/または洗浄液14は切換弁16の操作で排出管15から貯蔵タンク1外に排出される。   Thereafter, the storage liquid and / or the cleaning liquid 14 is extracted from the storage tank 1 by the circulation pump 10, heated by the heater 9, and then stored at a high flow rate from the ejection nozzle 6 through the cleaning pipe 4. The cleaning liquid 14 is ejected toward the accumulated sludge 13, and the accumulated sludge 13 is pulverized and suspended. Next, the cleaning sludge 13 in the storage tank 1 can be uniformly pulverized and suspended by rotating the cleaning tube 4 and changing the angle to change the ejection direction of the ejection nozzle 6 at the tip. When this operation is repeated and the sludge concentration in the storage liquid and / or the cleaning liquid 14 becomes high, the storage liquid and / or the cleaning liquid 14 is discharged out of the storage tank 1 from the discharge pipe 15 by the operation of the switching valve 16. .

なお、洗浄用管4を複数個所に設置した場合には、噴出ノズル6の噴出方向を一定とすることによって貯蔵タンク1内に旋回流を発生させ、堆積スラッジの懸濁をより効果的に促進することもできる。また、洗浄用管4を自重で堆積スラッジ13内に装入できない場合は一旦堆積スラッジ13上に載置させておき、貯蔵液および/または洗浄液14の噴出で生じる貯蔵タンク1内の旋回流で堆積スラッジ13を徐々に粉砕、懸濁させることでタンク底板まで降下させることができる。   In addition, when the cleaning pipes 4 are installed at a plurality of locations, a swirling flow is generated in the storage tank 1 by making the ejection direction of the ejection nozzle 6 constant, and the suspension of the accumulated sludge is more effectively promoted. You can also Further, when the cleaning pipe 4 cannot be charged into the sedimentation sludge 13 by its own weight, it is temporarily placed on the sedimentation sludge 13, and the swirling flow in the storage tank 1 generated by the ejection of the storage liquid and / or the cleaning liquid 14 is used. The accumulated sludge 13 can be lowered to the tank bottom plate by gradually pulverizing and suspending it.

内径21.2m、高さ9.8m、容量3000キロリットルのコールタール用貯蔵タンク1のタンク天板2に既存するマンホール3のうちの三箇所に洗浄用管4を設置した。
貯蔵タンク1内に堆積し、圧密したコールタールスラッジに対して加温器9で常温〜100℃に加温した貯蔵液および/または洗浄液を、洗浄用管4の噴出ノズル6から噴出流速10〜30m/Sで噴出し、堆積するコールタールスラッジを粉砕、懸濁させて循環ポンプ10によって貯蔵タンク1外に排出した。その結果、貯蔵タンク1に堆積するスラッジの全量を除去することができた。
Cleaning pipes 4 were installed in three of the existing manholes 3 on the tank top plate 2 of the coal tar storage tank 1 having an inner diameter of 21.2 m, a height of 9.8 m, and a capacity of 3000 kiloliters.
The storage liquid and / or cleaning liquid deposited in the storage tank 1 and heated to normal temperature to 100 ° C. by the heater 9 against the compacted coal tar sludge is discharged from the discharge nozzle 6 of the cleaning pipe 4 at a flow velocity of 10 to The coal tar sludge ejected at 30 m / S and accumulated was pulverized, suspended, and discharged out of the storage tank 1 by the circulation pump 10. As a result, the entire amount of sludge accumulated in the storage tank 1 could be removed.

本発明によるタンク内堆積スラッジの除去装置の一例を示すフロー図である。It is a flowchart which shows an example of the removal apparatus of the accumulation sludge in a tank by this invention. 図1のA部を拡大して示す説明図である。It is explanatory drawing which expands and shows the A section of FIG.

符号の説明Explanation of symbols

1 貯蔵タンク
2 タンク天板
3 マンホール(既存)
4 洗浄用管
5 スイベルジョイント
6 噴出ノズル
7 フレキシブルホース
8 接続配管
9 加温器
10 循環ポンプ
11 抜出管
12 蒸気
13 堆積スラッジ
14 貯蔵液および/または洗浄液
15 排出管
16 切換弁
1 Storage tank 2 Tank top 3 Manhole (existing)
4 Washing pipe 5 Swivel joint 6 Jet nozzle 7 Flexible hose 8 Connection pipe 9 Heater
10 Circulation pump
11 Extraction pipe
12 steam
13 Sediment sludge
14 Stock solution and / or cleaning solution
15 discharge pipe
16 Switching valve

Claims (2)

貯蔵タンクに堆積したスラッジの除去方法であって、該貯蔵タンクのタンク天板の既存マンホールに、先端近傍に噴出ノズルを有する洗浄用管を密閉かつ該洗浄用管の周方向に回動可能に固定し、前記噴出ノズルから貯蔵液および/または洗浄液を噴出させ、前記スラッジを貯蔵液および/または洗浄液に懸濁させて、該貯蔵タンク内から抜出しするとともに、抜出した貯蔵液および/または洗浄液を前記洗浄用管へ返送することを特徴とする貯蔵タンク内堆積スラッジの除去方法。   A method for removing sludge accumulated in a storage tank, wherein a cleaning pipe having a jet nozzle in the vicinity of the tip is sealed in an existing manhole on the tank top plate of the storage tank and is rotatable in the circumferential direction of the cleaning pipe The storage liquid and / or the cleaning liquid is ejected from the ejection nozzle, the sludge is suspended in the storage liquid and / or the cleaning liquid, and the storage liquid and / or the cleaning liquid extracted are discharged from the storage tank. Returning to the said washing | cleaning pipe | tube, The removal method of the accumulation sludge in a storage tank characterized by the above-mentioned. 貯蔵タンクに堆積したスラッジの除去装置であって、先端に噴出ノズルを有し、前記貯蔵タンクのタンク天板の既存マンホールに密閉かつ周方向に回動可能に固定された洗浄用管と、前記貯蔵タンクの底部近傍に接続されて貯蔵液および/または洗浄液を抜き出しする抜出管と、吸込み側が前記抜出管と接続され、吐出側が接続配管に接続されて抜出された貯蔵液および/または洗浄液を前記洗浄用管へ返送する循環ポンプと、該循環ポンプの吐出側で前記接続配管と切換可能に接続されて前記貯蔵タンク内の貯蔵液および/または洗浄液を前記貯蔵タンク外へ排出する排出管と、を有することを特徴とする貯蔵タンク内堆積スラッジの除去装置。   A device for removing sludge accumulated in a storage tank, having a jet nozzle at the tip, and a washing tube fixed to an existing manhole on the tank top plate of the storage tank and rotatably pivoted in the circumferential direction, An extraction pipe connected to the vicinity of the bottom of the storage tank to extract the storage liquid and / or cleaning liquid, and a storage liquid extracted from the suction side connected to the extraction pipe and a discharge side connected to the connection pipe and / or A circulation pump that returns the cleaning liquid to the cleaning pipe, and a discharge that is switchably connected to the connection pipe on the discharge side of the circulation pump and discharges the storage liquid and / or the cleaning liquid in the storage tank to the outside of the storage tank. A device for removing accumulated sludge in a storage tank.
JP2007272344A 2007-10-19 2007-10-19 Removing method and apparatus for deposited sludge in storage tank Pending JP2009095809A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013233533A (en) * 2012-05-02 2013-11-21 M & F System Kk Stick type fixed cleaning device
CN103420054A (en) * 2013-09-02 2013-12-04 四川郎酒集团有限责任公司 Wine tank and cleaning method of wine tank
CN103817120A (en) * 2014-02-27 2014-05-28 神华集团有限责任公司 Method for cleaning sticky wall of high pressure polyethylene tubular reactor
JP2015045775A (en) * 2013-08-29 2015-03-12 日本碍子株式会社 Method and apparatus for discharging deposit from inside jacket

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013233533A (en) * 2012-05-02 2013-11-21 M & F System Kk Stick type fixed cleaning device
JP2015045775A (en) * 2013-08-29 2015-03-12 日本碍子株式会社 Method and apparatus for discharging deposit from inside jacket
CN103420054A (en) * 2013-09-02 2013-12-04 四川郎酒集团有限责任公司 Wine tank and cleaning method of wine tank
CN103817120A (en) * 2014-02-27 2014-05-28 神华集团有限责任公司 Method for cleaning sticky wall of high pressure polyethylene tubular reactor

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